IP Library Granted Patent US 9,890,452
Granted Patent B2
US 9,890,452 · App. 14/384,749 · Granted Feb 13, 2018

Tantalum sputtering target, method for manufacturing same, and barrier film for semiconductor wiring formed by using target

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Quick Facts
Patent No.
US 9,890,452
App. No.
14/384,749
Granted
Feb 13, 2018
Kind
B2
Abstract

Provided is a tantalum sputtering target, which is characterized that an average crystal grain size of the target is 50 μm or more and 200 μm or less, and variation of a crystal grain size in the target plane is 40% or higher and 60% or less. This invention aims to provide a tantalum sputtering target capable of improving the uniformity of the film thickness and reducing the variation of the resistance value (sheet resistance).

Claims (2)

1. A tantalum sputtering target, wherein an average crystal grain size of the target is 50 μm or more and 200 μm or less, and variation of a crystal grain size in the target plane is 40% or higher and 50% or less on a surface of the target, wherein the variation is defined as a ratio of standard deviation to an average of five average crystal grain sizes measured at five different locations selected on the surface of the sputtering target.

2. A method of producing a tantalum sputtering target wherein an ingot or a billet obtained by subjecting a tantalum raw material to electron beam melting and casting is heat treated at a temperature of 900° C. or higher and 1400° C. lower, subsequently subjected to cold forging processing consisting of upset forging and extend forging by a total amount of true strain of 3.0 or more and 5.0 or less, thereafter heat-treated at 850° C. or higher and 1100° C. lower subsequently rolled at a rolling reduction of 80% or higher and 90% or less, thereafter heat-treated at 750° C. or higher and 1000° C. lower, and additionally subject to finish processing to obtain a target, wherein an average crystal grain size of the target is 50 micrometers or more and 200 micrometers or less, and a variation of crystal grain size in a target plane is 40% or higher and 50% or less on a surface of the target, wherein the variation is defined as a ratio of standard deviation to an average of five average crystal grain sizes measured at five different locations selected on the surface of the sputtering target.

Assignments (3)
CHANGE OF ADDRESS Recorded Aug 11, 2021
From: JX NIPPON MINING & METALS CORPORATION
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 057453/0937 →
CHANGE OF ADDRESS Recorded Aug 11, 2021
From: JX NIPPON MINING & METALS CORPORATION
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 057160/0114 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 10, 2014
From: NAGATSU, KOTARO; SENDA, SHINICHIRO
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 033931/0748 →