IP Library Granted Patent US 9,640,386
Granted Patent B2
US 9,640,386 · App. 14/571,943 · Granted May 2, 2017

Precursors for CVD silicon carbo-nitride films

Inventors: Manchao Xiao (San Diego, CA); Arthur Kenneth Hochberg (Solana Beach, CA)
Assignee: VERSUM MATERIALS US, LLC
H01L21/02211C07F7/025C09D5/00C23C16/36H01L21/0228H01L21/02167H01L21/02219H01L21/02222H01L21/02271H01L21/02274
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Quick Facts
Patent No.
US 9,640,386
App. No.
14/571,943
Granted
May 2, 2017
Kind
B2
Abstract

Classes of liquid aminosilanes have been found which allow for the production of silicon carbo-nitride films of the general formula Si x C y N z . These aminosilanes, in contrast, to some of the precursors employed heretofore, are liquid at room temperature and pressure allowing for convenient handling. In addition, the invention relates to a process for producing such films. The classes of compounds are generally represented by the formulas: and mixtures thereof, wherein R and R 1 in the formulas represent aliphatic groups typically having from 2 to about 10 carbon atoms, e.g., alkyl, cycloalkyl with R and R 1 in formula A also being combinable into a cyclic group, and R 2 representing a single bond, (CH 2 ) n , a ring, or SiH 2 .

Claims (22)

1. An aminosilane compound selected from the group having the following formulas:

2. The aminosilane of claim 1 comprising:

3. A composition comprising:

and at least one member selected from the group consisting of nitrogen, ammonia, hydrazine, and dimethylhydrazine.

4. The aminosilane of claim 1 comprising:

5. The aminosilane of claim 1 comprising:

6. The aminosilane of claim 1 comprising:

7. A composition comprising the compound of claim 1 and at least one aminosilane compound selected from the group consisting of:

and where n is 4 or 5.

8. The composition of claim 7 comprising:

9. The composition of claim 7 comprising:

10. The composition of claim 7 comprising:

11. The composition of claim 7 comprising:

wherein n is 4 or 5.

12. A composition comprising the compound of claim 1 and at least one member selected from the group consisting of:

13. The composition of claim 12 comprising:

14. The composition of claim 12 comprising:

15. The composition of claim 12 comprising:

16. A composition comprising at least one aminosilane selected from the group consisting of:

and at least one member selected from the group consisting of nitrogen, ammonia, hydrazine, and dimethylhydrazine.

17. A composition comprising the compound of claim 1 and at least one member selected from the group consisting of bis-tert-butylaminosilane, tris-iso-propylaminosilane, bis-diethylaminosilane, tris-dimethylaminosilane, and bis-iso-propylaminosilane.

18. A composition comprising the compound of claim 1 and at least one member selected from the group consisting of nitrogen, ammonia, hydrazine, and dimethylhydrazine.

Assignments (4)
RELEASE OF SECURITY INTEREST Recorded Oct 7, 2019
From: CITIBANK, N.A., AS AGENT
To: VERSUM MATERIALS US, LLC
Reel/Frame 050647/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 20, 2017
From: AIR PRODUCTS AND CHEMICALS, INC.
To: VERSUM MATERIALS US, LLC
Reel/Frame 041772/0733 →
PATENT SECURITY AGREEMENT Recorded Oct 27, 2016
From: VERSUM MATERIALS US, LLC
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 040503/0442 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 8, 2015
From: XIAO, MANCHAO; HOCHBERG, ARTHUR KENNETH
To: AIR PRODUCTS AND CHEMICALS, INC.
Reel/Frame 035360/0468 →
Continuity (4)
Division 13051591 · Mar 18, 2011
Continuation 12267790 · Nov 10, 2008
Division 11129862 · May 16, 2005
Related Publication 20150147893A1 · May 28, 2015