IP Library Granted Patent US 10,466,588
Granted Patent B2
US 10,466,588 · App. 15/332,340 · Granted Nov 5, 2019

Sulfonyl photoacid generators and photoresists comprising same

Inventors: Cong Liu (Marlborough, MA); Cheng-Bai Xu (Marlborough, MA)
Assignee: Rohm and Haas Electronic Materials LLC
G03F7/0045C07C309/17C07C311/48C07C313/04C07C321/28C07C381/12G03F7/0046G03F7/0382G03F7/0392G03F7/162G03F7/20G03F7/30G03F7/322C07C2603/74
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,466,588
App. No.
15/332,340
Granted
Nov 5, 2019
Kind
B2
Abstract

New bis(sulfonyl)imide and tri(sulfonyl)methide photoacid generator compounds (“PAGs”) are provided as well as photoresist compositions that comprise such PAG compounds.

Claims (40)

1. A photoacid generator compound of the following Formula I:

wherein W, Y are each independently hydrogen, fluorine, optionally substituted fluoroalkyl;

optionally substituted fluoroalkoxy; or optionally substituted fluorocarbocyclic aryl;

W′, Y′ are each independently the same as defined for W and Y;

W″, Y″ are each independently the same as defined for W and Y;

n, n′ and n″ are each the same or different and are each a positive integer;

U, U′ and U″ are each the same or different and are each a linker; and

R, R′ and R″ are each the same or different and are each an optionally substituted carboalicyclic, optionally substituted heteroalicyclic, optionally substituted carbocyclic aryl, or optionally substituted heteroaromatic group;

X + is a sulfonium or iodonium group.

2. A photoacid generator compound of the following Formula II:

wherein W, Y are each independently hydrogen, fluorine, optionally substituted fluoroalkyl;

optionally substituted fluoroalkoxy; or optionally substituted fluorocarbocyclic aryl;

W′, Y′ are each independently the same as defined for W and Y;

n and n′ are each the same or different and are each a positive integer;

U and U′ are each the same or different and are each a linker; and

R and R′ are each the same or different and are each an optionally substituted carboalicyclic, optionally substituted heteroalicyclic, optionally substituted carbocyclic aryl, or optionally substituted heteroaromatic group;

X + is a sulfonium or iodonium group.

3. A photoacid generator of claim 1 wherein X + is of either of the following formulae:

where R 1 to R 5 each independently represents C 1-30 optionally substituted alkyl group or a substituted or unsubstituted carbocyclic aryl group, or any two or more of R 1 , R 2 and R 3 may bond together to form a ring with the sulfur ring.

4. A photoacid generator compound of claim 1 wherein X + is any of the following groups:

wherein in those formulae P 1 , P 2 , P 3 , P 4 , P 5 , P 6 , and P 7 each independently represent hydrogen or one to five non-hydrogen substituents.

5. A photoresist composition comprising a photoacid generator compound of claim 1 .

6. A method for forming a photoresist relief image comprising:

a) applying a coating layer of a photoresist composition of claim 5 on a substrate;

b) exposing the photoresist coating layer to patterned activating radiation and developing the exposed photoresist layer to provide a relief image.

7. A photoresist composition comprising a photoacid generator compound of claim 3 .

8. A method for forming a photoresist relief image comprising:

a) applying a coating layer of a photoresist composition of claim 7 on a substrate;

b) exposing the photoresist coating layer to patterned activating radiation and

developing the exposed photoresist layer to provide a relief image.

9. A photoresist composition comprising a photoacid generator compound of claim 4 .

10. A method for forming a photoresist relief image comprising:

a) applying a coating layer of a photoresist composition of claim 9 on a substrate;

b) exposing the photoresist coating layer to patterned activating radiation and

developing the exposed photoresist layer to provide a relief image.

11. A photoacid generator of claim 2 wherein X + is a sulfonium compound.

12. A photoacid generator of claim 2 wherein X + is of either of the following formulae:

where R 1 to R 5 each independently represents C 1-30 optionally substituted alkyl group or a substituted or unsubstituted carbocyclic aryl group, or any two or more of R 1 , R 2 and R 3 may bond together to form a ring with the sulfur ring.

13. A photoacid generator compound of claim 1 wherein X + is any of the following groups:

wherein in those formulae P 1 , P 2 , P 3 , P 4 , P 5 , P 6 , and P 7 each independently represent hydrogen or one to five non-hydrogen substituents.

Assignments (4)
SECURITY INTEREST Recorded Nov 3, 2025
From: QNITY ELECTRONICS, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 073515/0243 →
SECURITY INTEREST Recorded Nov 3, 2025
From: QNITY ELECTRONICS, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 073517/0298 →
CHANGE OF NAME Recorded Oct 29, 2024
From: ROHM & HAAS ELECTRONIC MATERIALS LLC
To: DUPONT ELECTRONIC MATERIALS INTERNATIONAL, LLC
Reel/Frame 069272/0383 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 15, 2019
From: LIU, CONG; XU, CHENG-BAI
To: ROHM AND HAAS ELECTRONIC MATERIALS LLC
Reel/Frame 049751/0820 →
Continuity (3)
Division 12968130 · Dec 10, 2010
Provisional Application 61286197 · Dec 14, 2009
Related Publication 20170153542A1 · Jun 1, 2017