Method for manufacturing semiconductor device
It is an object to provide a highly reliable semiconductor device which includes a thin film transistor having stable electric characteristics. It is another object to manufacture a highly reliable semiconductor device at lower cost with high productivity. In a method for manufacturing a semiconductor device which includes a thin film transistor where a semiconductor layer having a channel formation region, a source region, and a drain region are formed using an oxide semiconductor layer, heat treatment (heat treatment for dehydration or dehydrogenation) is performed so as to improve the purity of the oxide semiconductor layer and reduce impurities such as moisture. Moreover, the oxide semiconductor layer subjected to the heat treatment is slowly cooled under an oxygen atmosphere.
1. A method for manufacturing a semiconductor device comprising the steps of:
forming a first oxide semiconductor layer;
forming a second oxide semiconductor layer over the first oxide semiconductor layer;
performing a first heat treatment on the first oxide semiconductor layer and the second oxide semiconductor layer under an atmosphere containing nitrogen;
forming an oxide insulating layer over and in contact with the first oxide semiconductor layer and the second oxide semiconductor layer; and
performing a second heat treatment on the oxide insulating layer,
wherein the first oxide semiconductor layer has a carrier density of less than 1×10 18 /cm 3 after the second heat treatment.
2. The method for manufacturing a semiconductor device according to claim 1 , wherein the first heat treatment is performed at 400° C. or higher.
3. The method for manufacturing a semiconductor device according to claim 1 , wherein a crystallinity of the second oxide semiconductor layer is higher than a crystallinity of the first oxide semiconductor layer.
4. The method for manufacturing a semiconductor device according to claim 1 , wherein at least one of the first oxide semiconductor layer and the second oxide semiconductor layer comprises indium, gallium, and zinc.
5. The method for manufacturing a semiconductor device according to claim 1 , wherein at least one of the first oxide semiconductor layer and the second oxide semiconductor layer comprises indium, tin, and zinc.
6. The method for manufacturing a semiconductor device according to claim 1 , wherein the oxide insulating layer is in contact with a side surface of the second oxide semiconductor layer.
7. A method for manufacturing a semiconductor device comprising the steps of:
forming a first oxide semiconductor layer;
forming a second oxide semiconductor layer over the first oxide semiconductor layer;
performing a first heat treatment on the first oxide semiconductor layer and the second oxide semiconductor layer for dehydration or dehydrogenation;
forming an oxide insulating layer over and in contact with the first oxide semiconductor layer and the second oxide semiconductor layer; and
performing a second heat treatment on the oxide insulating layer,
wherein the first oxide semiconductor layer has a carrier density of less than 1×10 18 /cm 3 after the second heat treatment.
8. The method for manufacturing a semiconductor device according to claim 7 , wherein the first heat treatment is performed at 400° C. or higher.
9. The method for manufacturing a semiconductor device according to claim 7 , wherein a crystallinity of the second oxide semiconductor layer is higher than a crystallinity of the first oxide semiconductor layer.
10. The method for manufacturing a semiconductor device according to claim 7 , wherein at least one of the first oxide semiconductor layer and the second oxide semiconductor layer comprises indium, gallium, and zinc.
11. The method for manufacturing a semiconductor device according to claim 7 , wherein at least one of the first oxide semiconductor layer and the second oxide semiconductor layer comprises indium, tin, and zinc.
12. The method for manufacturing a semiconductor device according to claim 7 , wherein the oxide insulating layer is in contact with a side surface of the second oxide semiconductor layer.
13. A method for manufacturing a semiconductor device comprising the steps of:
forming a first oxide semiconductor layer;
forming a second oxide semiconductor layer over the first oxide semiconductor layer;
performing a first heat treatment on the first oxide semiconductor layer and the second oxide semiconductor layer under an atmosphere containing nitrogen;
cooling the first oxide semiconductor layer and the second oxide semiconductor layer in an atmosphere containing oxygen;
forming an oxide insulating layer over and in contact with the first oxide semiconductor layer and the second oxide semiconductor layer; and
performing a second heat treatment on the oxide insulating layer,
wherein the first oxide semiconductor layer has a carrier density of less than 1×10 18 /cm 3 after the second heat treatment.
14. The method for manufacturing a semiconductor device according to claim 13 , wherein the first heat treatment is performed at 400° C. or higher.
15. The method for manufacturing a semiconductor device according to claim 13 , wherein a crystallinity of the second oxide semiconductor layer is higher than a crystallinity of the first oxide semiconductor layer.
16. The method for manufacturing a semiconductor device according to claim 13 , wherein at least one of the first oxide semiconductor layer and the second oxide semiconductor layer comprises indium, gallium, and zinc.
17. The method for manufacturing a semiconductor device according to claim 13 , wherein at least one of the first oxide semiconductor layer and the second oxide semiconductor layer comprises indium, tin, and zinc.
18. The method for manufacturing a semiconductor device according to claim 13 , wherein the oxide insulating layer is in contact with a side surface of the second oxide semiconductor layer.