IP Library Granted Patent US 11,610,807
Granted Patent B2
US 11,610,807 · App. 17/227,354 · Granted Mar 21, 2023

Methods and apparatus for cleaving of semiconductor substrates

Inventors: Felix Deng (Singapore, SG); Yueh Sheng Ow (Singapore, SG); Tuck Foong Koh (Singapore, SG); Nuno Yen-Chu Chen (Singapore, SG); Yuichi Wada (Chiba, JP); Sree Rangasai V. Kesapragada (Union City, CA); Clinton Goh (Singapore, SG)
Assignee: APPLIED MATERIALS, INC.
H01L21/76254H01L21/67017H01L21/67115H01L21/67253
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Quick Facts
Patent No.
US 11,610,807
App. No.
17/227,354
Granted
Mar 21, 2023
Kind
B2
Abstract

Methods and apparatus for cleaving a substrate in a semiconductor chamber. The semiconductor chamber pressure is adjusted to a process pressure, a substrate is then heated to a nucleation temperature of ions implanted in the substrate, the temperature of the substrate is then adjusted below the nucleation temperature of the ions, and the temperature is maintained until cleaving of the substrate occurs. Microwaves may be used to provide heating of the substrate for the processes. A cleaving sensor may be used for detection of successful cleaving by detecting pressure changes, acoustic emissions, changes within the substrate, and/or residual gases given off by the implanted ions when the cleaving occurs.

Claims (52)

1. A method of cleaving a substrate in a chamber, comprising:

adjusting a pressure of the chamber to a process pressure;

adjusting a temperature of the substrate to a nucleation temperature of ions implanted in the substrate;

adjusting the temperature of the substrate below the nucleation temperature of ions implanted in the substrate;

maintaining the temperature of the substrate at a soak temperature; and

detecting when cleaving of the substrate has occurred.

2. The method of claim 1 , further comprising:

adjusting the temperature of the substrate using microwaves at a fixed power level.

3. The method of claim 1 , further comprising:

adjusting the temperature of the substrate using microwaves controlled by a proportional-integral-derivative (PID) controller interfacing with an infrared sensor.

4. The method of claim 1 , further comprising:

adjusting the temperature of the substrate using microwaves with a power level adjusted before, after, or in parallel with a change of the process pressure in the chamber.

5. The method of claim 4 , wherein the power level of the microwaves is in a range of greater than zero watts to approximately 1600 watts.

6. The method of claim 1 , further comprising:

adjusting the temperature of the substrate using microwaves with a single frequency between 2 GHz and 8 GHz or a sweeping frequency at a rate of approximately 750 microseconds between frequencies to approximately 25 microseconds between frequencies.

7. The method of claim 6 , wherein the sweeping frequency has a range of approximately 2 GHz to approximately 8 GHz.

8. The method of claim 6 , wherein the sweeping frequency has a range of approximately 5.85 GHz to approximately 6.65 GHz.

9. The method of claim 1 , further comprising:

adjusting the temperature of the substrate to the nucleation temperature of ions with a ramping rate of approximately 0.01 degrees Celsius to approximately 15 degrees Celsius.

10. The method of claim 1 , further comprising:

pulsing the soak temperature while maintaining the process pressure in the chamber to promote cleaving of the substrate.

11. The method of claim 1 , further comprising:

pulsing the process pressure in the chamber while maintaining the soak temperature to promote cleaving of the substrate.

12. The method of claim 1 , further comprising:

adjusting the process pressure of the chamber to a range of greater than zero Torr to approximately 770 Torr.

13. The method of claim 1 , wherein ions implanted in the substrate include hydrogen, helium, nitrogen, oxygen, or argon.

14. An apparatus for cleaving a substrate, comprising:

a chamber having a multi-faceted microwave cavity for processing the substrate;

a microwave power source coupled to the multi-faceted microwave cavity for heating the substrate during processing;

a controller with proportional-integral-derivative (PID) control for adjusting the microwave power source, process temperature, and process pressure within the chamber, the controller configured to perform a substrate cleaving process including;

adjusting a pressure of the chamber to a process pressure;

adjusting a temperature of the substrate to a nucleation temperature of ions implanted in the substrate;

adjusting the temperature of the substrate below the nucleation temperature of ions implanted in the substrate;

maintaining the temperature of the substrate at a soak temperature; and

detecting when cleaving of the substrate has occurred;

a vacuum source with pulsing capabilities to pulse the process pressure within the chamber; and

a contactless temperature sensor that reads a temperature of the substrate during processing and relays the temperature to the PID controls.

15. The apparatus of claim 14 , further comprising:

a cleaving sensor for detecting when a cleaving of the substrate has occurred.

16. The apparatus of claim 15 , wherein the cleaving sensor includes an acoustic emission sensor, a residual gas analyzer, or a pressure sensor.

17. An apparatus for cleaving a substrate, comprising:

a chamber having a multi-faceted microwave cavity configured to support a substrate to be cleaved therein;

a microwave power source coupled to the multi-faceted microwave cavity, the microwave power source configured to heat the substrate during processing with microwaves of a single frequency or of a sweeping frequency in a range of approximately 2 GHz to approximately 8 GHz;

a vacuum source with pulsing capabilities configured to pulse a process pressure within the chamber;

a contactless temperature sensor that reads a temperature of the substrate during processing and relays the temperature to a controller having proportional-integral-derivative (PID) control configured to adjust the temperature of the substrate with the microwave power source and adjust the process pressure within the chamber with the vacuum source, the controller configured to perform a substrate cleaving process including:

adjusting the process pressure within the chamber;

adjusting the temperature of the substrate to a nucleation temperature of ions implanted in the substrate;

adjusting the temperature of the substrate below the nucleation temperature of ions implanted in the substrate; and

maintaining the temperature of the substrate at a soak temperature until cleaving of the substrate occurs.

18. The apparatus of claim 17 , further comprising:

a cleaving sensor coupled to the controller and configured to detect when a cleaving of the substrate has occurred.

19. The apparatus of claim 18 , wherein the cleaving sensor includes an acoustic emission sensor, a residual gas analyzer, or a pressure sensor.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 7, 2021
From: APPLIED MATERIALS SINGAPORE TECHNOLOGY PTE. LTD.
To: APPLIED MATERIALS, INC.
Reel/Frame 057726/0648 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2021
From: WADA, YUICHI; KESAPRAGADA, SREE RANGASAI V
To: APPLIED MATERIALS, INC.
Reel/Frame 055899/0610 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2021
From: DENG, FELIX; OW, YUEH SHENG; KOH, TUCK FOONG; CHEN, NUNO YEN-CHU; GOH, CLINTON
To: APPLIED MATERIALS SINGAPORE TECHNOLOGY PTE. LTD.
Reel/Frame 055899/0705 →
Continuity (4)
Continuation 17217179 · Mar 30, 2021
Continuation 16403796 · May 6, 2019
Provisional Application 62671535 · May 15, 2018
Related Publication 20210233802A1 · Jul 29, 2021