IP Library Granted Patent US 12,500,232
Granted Patent B2
US 12,500,232 · App. 17/570,050 · Granted Dec 16, 2025

Cathode active material

Inventors: Yong-Mook Kang (Seoul, KR); Suwon Lee (Seoul, KR); Youngju Choi (Seoul, KR); Gi-Hyeok Lee (Cheonan-si, KR)
Assignee: KOREA UNIVERSITY RESEARCH AND BUSINESS FOUNDATION
H01M4/505H01M10/052
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,500,232
App. No.
17/570,050
Granted
Dec 16, 2025
Kind
B2
Abstract

The inventive concept discloses a cathode active material containing crystal water and a manganese-based metal oxide.

Claims (15)

1 . A cathode active material containing:

crystal water and a manganese-based metal oxide,

wherein the cathode active material includes a first crystal phase having a two-dimensional crystal structure and a second crystal phase having a three-dimensional crystal structure,

wherein the first crystal phase is a thermodynamically stable two-dimensional layered crystal structure where a unit lattice structure composed of the manganese-based metal oxide, and having manganese filling octahedral sites of a unit lattice where manganese and oxygen are bonded to each other is two-dimensionally extended,

wherein the second crystal phase is a thermodynamically metastable three-dimensional crystal structure where, as some manganese in the manganese-based metal oxide forming the layered structure is chemically bonded to oxygen in the crystal water, a unit lattice structure having manganese filling octahedral sites of a unit lattice and a unit lattice structure having manganese filling tetrahedral sites are mixed,

wherein the two-dimensional crystal structure includes two or more unit layers composed of a manganese oxide, and contains a first metal element and a second metal element disposed between the two or more unit layers,

wherein the first metal element is at least one metal element selected from a group consisting of an alkali metal element and an alkaline earth metal element, and the second metal element is at least one metal element selected from a group consisting of a post-transition metal element.

2 . The cathode active material of claim 1 , wherein the cathode active material is expressed by a following [Chemical Formula 1]

Me x Do y MnO 2 ·z H 2 O  [Chemical Formula 1]

in Chemical Formula 1, the Me is the first metal element,

the dopant (Do) is the second metal element, and

0.23≤x≤1, 0.01≤y≤1, and 0.01≤z≤0.5.

3 . The cathode active material of claim 2 , wherein the Me is at least one element selected from Li, Na, and K.

4 . The cathode active material of claim 2 , wherein the dopant is at least one element selected from Al, Mg, Cu, Zn, and Fe.

5 . The cathode active material of claim 2 , wherein the Me and the dopant are composed of different elements.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 7, 2022
From: KANG, YONG-MOOK; LEE, SUWON; CHOI, YOUNGJU; LEE, GI-HYEOK
To: KOREA UNIVERSITY RESEARCH AND BUSINESS FOUNDATION
Reel/Frame 058582/0440 →
Priority Claims (1)
KR 10-2021-0002501 · Jan 8, 2021 · national
Continuity (1)
Related Publication 20220223858A1 · Jul 14, 2022
References Cited (34)
US 20110311846A1 · Whitacre · 2011 [cited by examiner]
US 20120064388A1 · Whitacre · 2012 [cited by examiner]
US 20140037996A1 · Whitacre · 2014 [cited by examiner]
US 20150147628A1 · Whitacre · 2015 [cited by examiner]
US 20170110765A1 · Yadav · 2017 [cited by examiner]
US 20200227739A1 · Yadav · 2020 [cited by examiner]
US 20230344014A1 · Yadav · 2023 [cited by examiner]
CN 108793254A · 2018 [cited by applicant]
CN 110615480A · 2019 [cited by applicant]
JP 2003502256A · 2003 [cited by applicant]
KR 1020110017850A · 2011 [cited by applicant]
KR 1020130098224A · 2013 [cited by applicant]
KR 1020140108807A · 2014 [cited by applicant]
KR 1020160022103A · 2016 [cited by applicant]
KR 20160022103 · 2016 [cited by examiner]
KR 1020180089030A · 2018 [cited by applicant]
KR 1020200013200A · 2020 [cited by applicant]
KR 102112405B1 · 2020 [cited by applicant]
KR 1020200065626A · 2020 [cited by applicant]
KR 102120272B1 · 2020 [cited by applicant]
KR 1020200083825A · 2020 [cited by applicant]
English translation of KR 2016/0022103 (Year: 2016). [cited by examiner]
Zhang et al, Manganese-Based Oxide Cathode Materials for Aqueous Zinc-Ion Batteries: Materials, Mechanism, Challenges, and Strategies, vol. 1 Iss.2 Chem & Bio Engr, pp. 113-132 (Year: 2024). [cited by examiner]
Zhang et al, Challenges and Perspectives for Doping Strategy for Manganese-Based Zinc-ion Battery Cathode, 15 Energies 4698 (Year: 2022). [cited by examiner]
Zhai et al, Layered Birnessite Cathode with a Displacement/ Intercalation Mechanism for High-Performance Aqueous Zinc-Ion Batteries, Nano-Micro Letters (Year: 2020). [cited by examiner]
Triggered reversible phase transformation between layered and spinel structure in manganese-based layered compounds, Nature Communications (Year: 2019). [cited by examiner]
Qiu et al, Low-cost birnessite as a promising cathode for high-performance aqueous rechargeable batteries, vol. 272 10 Electrochimica Acta, pp. 154-160 (Year: 2018). [cited by examiner]
Song et al, Recent advances in Zn-ion batteries, Nanyang Technology University (Year: 2018). [cited by examiner]
Xia et al , A monoclinic polymorph of sodium birnessite for ultrafast and ultrastable sodium ion storage, Nature Communications (Year: 2018). [cited by examiner]
Yadav et al, Regenerable Cu-intercalated MnO2 layered cathode for highly cyclable energy dense batteries, Nature Communications (Year: 2017). [cited by examiner]
Nam et al, The High Performance of Crystal Water Containing Manganese Birnessite Cathodes for Magnesium Batteries, vol. 15 Nano Letters pp. 4071-4079 (Year: 2015). [cited by examiner]
Aronson et al, Synthesis, Characterization, and Electrochemical Properties of Magnesium Birnessite and Zinc Chalcophanite Prepared by a Low-Temperature Route, vol. 4 Iss.4 Chemistry of Materials pp. 949-957 (Year: 1999). [cited by examiner]
Mi Ru Jo et al., “Triggered reversible phase transformation between layered and spinel structure in manganese-based layered compounds,” Nature Communications, Sep. 2, 2019, vol. 10, Article No. 3385. [cited by applicant]
Korean Written Decision of Registration dated Jul. 5, 2023 for corresponding Korean Patent Application No. 10-2021-0002501, 6 pages, English Machine Translation. [cited by applicant]