IP Library Granted Patent US 12,735,365
Granted Patent B2
US 12,735,365 · App. 18/134,970 · Granted Sep 15, 2026

Environmental barrier coating and method of applying the same

Inventors: James T. Beals (West Hartford, CT); Xia Tang (West Hartford, CT); Richard Wesley Jackson, III (Mystic, CT); Andrew Spaeth (Holden, MA)
Assignee: RTX CORPORATION
C04B41/52C04B41/87C04B41/89C09D1/00C09D5/002C09D5/08C09D5/18F01D5/288C23C16/401C23C16/403C23C16/405C23C16/45529Y10T428/24521Y10T428/249957Y10T428/24999
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Quick Facts
Patent No.
US 12,735,365
App. No.
18/134,970
Granted
Sep 15, 2026
Kind
B2
Abstract

An article includes a substrate, a barrier layer disposed on the substrate, and an oxide-based ceramic material topcoat disposed on the barrier layer. The topcoat includes at least one crack. The article also includes a filler layer disposed on the topcoat and in the at least one crack. A method of applying a coating to an article and an article are also disclosed.

Claims (36)

1 . An article, comprising:

a substrate;

a barrier layer disposed on the substrate;

an oxide-based ceramic material topcoat disposed on the barrier layer, the topcoat including at least one crack; and

a filler layer disposed on the topcoat and in the at least one crack,

wherein an overall density of the filler layer is higher than an overall density of the topcoat,

wherein the at least one crack has a width less than about 100 nm.

2 . The article of claim 1 , wherein the barrier layer is a composite material, the composite material including a matrix, diffusive particles dispersed in the matrix, and gettering particles dispersed in the matrix.

3 . The article of claim 1 , wherein the barrier layer is a monolithic layer.

4 . The article of claim 1 , wherein the filler layer has a coefficient of thermal expansion less than about 6×10 −6 K −1 .

5 . The article of claim 1 , wherein the filler layer has a thickness of between about 1 and about 2 microns.

6 . The article of claim 1 , wherein the crack has an aspect ratio of at least about 100:1.

7 . The article of claim 1 , wherein the at least one crack is a through-thickness crack that extends in a direction approximately parallel to a thickness dimension of the topcoat.

8 . The article of claim 7 , wherein the through-thickness crack extends through the entire thickness dimension.

9 . The article of claim 1 , wherein the topcoat includes a ytterbium-based oxide.

10 . The article of claim 1 , wherein the filler layer includes HfO 2 .

11 . The article of claim 1 , wherein the filler layer includes Al 2 O 3 .

12 . The article of claim 1 , wherein the filler layer has a modulus of elasticity less than about 200 GPa.

13 . An article, comprising:

a substrate;

an oxide-based ceramic material topcoat disposed on the substrate, the topcoat including at least one crack; and

a filler layer disposed on the topcoat and in the at least one crack,

wherein an overall density of the filler layer is higher than an overall density of the topcoat, and

wherein the at least one crack has a width less than about 100 nm.

14 . The article of claim 13 , wherein the at least one crack is a through-thickness crack that extends in a direction approximately parallel to a thickness dimension of the topcoat.

15 . The article of claim 14 , wherein the through-thickness crack extends through the entire thickness dimension.

16 . A method of applying a coating to an article, comprising:

disposing a barrier layer on a substrate;

disposing an oxide-based ceramic material topcoat on the barrier layer, the topcoat including at least one crack; and

disposing a filler layer on the topcoat and in the at least one crack,

wherein the at least one crack has a width less than about 100 nm, and

wherein an overall density of the filler layer is higher than an overall density of the topcoat.

17 . The method of claim 16 , wherein the barrier layer is a monolithic layer.

18 . The method of claim 16 , wherein the filler layer is disposed on the topcoat by atomic layer deposition.

19 . The method of claim 16 , wherein the filler layer is disposed on the topcoat by slurry coating.

20 . The method of claim 16 , wherein the filler layer is disposed on the topcoat by chemical vapor deposition.

Assignments (2)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064402/0837 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 23, 2023
From: BEALS, JAMES T.; TANG, XIA; JACKSON, RICHARD WESLEY, III; SPAETH, ANDREW
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 063730/0331 →
Continuity (1)
Related Publication 20240343917A1 · Oct 17, 2024
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