IP Library Granted Patent US 11,781,199
Granted Patent B2
US 11,781,199 · App. 18/173,158 · Granted Oct 10, 2023

Method for producing nanoparticles and the nanoparticles produced therefrom

Inventors: Michele Viola Manuel (Gainesville, FL); Hunter B. Henderson (Gainesville, FL); Orlando Rios (Oak Ridge, TN); Gerard M. Ludtka (Oak Ridge, TN)
Assignees: University of Florida Research Foundation, Inc.; UT-BATTELLE, LLC
C22C1/1084B22F1/00B22F1/054B22F1/07B22F1/12B22F9/06C25D1/00C25D15/00H01F1/047H01F1/442H05B6/367B22F2009/042B22F2202/01B22F2202/07B22F2301/058B22F2302/10B22F2302/20B22F2998/10B22F2999/00H01F1/0036
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Quick Facts
Patent No.
US 11,781,199
App. No.
18/173,158
Granted
Oct 10, 2023
Kind
B2
Abstract

Disclosed herein is a method comprising disposing a container containing a metal and/or ferromagnetic solid and abrasive particles in a static magnetic field; where the container is surrounded by an induction coil; activating the induction coil with an electrical current, to heat up the metallic or ferromagnetic solid to form a fluid; generating sonic energy to produce acoustic cavitation and abrasion between the abrasive particles and the container; and producing nanoparticles that comprise elements from the container, the metal and/or the ferromagnetic solid and the abrasive particles. Disclosed herein too is a composition comprising first metal or a first ceramic; and particles comprising carbides and/or nitrides dispersed therein. Disclosed herein too is a composition comprising nanoparticles comprising chromium carbide, iron carbide, nickel carbide, γ-Fe and magnesium nitride.

Claims (18)

1. A composition comprising:

a conductive material;

a plurality of first abrasive particles comprising an abrasive particle; and

a plurality of second particles comprising a reaction product of the conductive material and an article material, a reaction product of the first abrasive particles and the article material, or a combination thereof.

2. The composition of claim 1 , wherein the conductive material comprises a metallic material, a ferromagnetic material, or any combination thereof.

3. The composition of claim 1 , wherein the conductive material has a melting point temperature that is lower than a melting point temperature of the article material.

4. The composition of claim 1 , wherein the conductive material is a solid at room temperature.

5. The composition of claim 1 , wherein the conductive material comprises magnesium, tin, lead, antimony, manganese, chromium, mercury, cadmium, silver, zinc, zirconium, silicon, or any combination thereof.

6. The composition of claim 1 , wherein the plurality of first abrasive particles comprises diamonds, cubic boron nitride, steel abrasive, emery, silicon carbide, aluminum oxide, or any combination thereof.

7. The composition of claim 1 , wherein the plurality of first abrasive particles comprises one or more carbonaceous particles.

8. The composition of claim 7 , wherein the one or more carbonaceous particles comprise carbon black, carbon nanotubes, carbon fibers, graphite flakes or lumps, crystalline flake graphite, amorphous graphite, vein graphite, or any combination thereof.

9. The composition of claim 1 , wherein the plurality of first abrasive particles has an average particle size of 1 nanometer to 10 micrometers.

10. The composition of claim 1 , wherein the plurality of second particles has an average particle size of from 1 nanometer to 1000 nanometers.

11. The composition of claim 1 , wherein the plurality of second particles has an average particle size of from 1 micrometer to 1000 micrometers.

12. The composition of claim 1 , wherein the composition further comprises a plurality of third non-abrasive particles comprising carbon, and a plurality of nanoparticles comprises one or more alloys comprising a reaction product of the non-abrasive particles and the article material.

13. The composition of claim 12 , wherein the third non-abrasive particles comprise iron carbides, silicon carbides, tungsten carbides, or any combination thereof.

14. The composition of claim 1 , wherein the second particles comprise chromium carbide (Cr 7 C 3 ), iron carbide (Fe 3 C), nickel carbide (Ni 3 C), (FeCr) 3 C, or any combination thereof.

15. The composition of claim 1 , wherein the second particles comprise magnesium nickel (MgNi 2 ).

Assignments (2)
CONFIRMATORY LICENSE Recorded Feb 10, 2025
From: UNIVERSITY OF FLORIDA
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 070161/0910 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 23, 2023
From: MANUEL, MICHELE VIOLA; HENDERSON, HUNTER B.; RIOS, ORLANDO; LUDTKA, GERARD M.
To: UNIVERSITY OF FLORIDA RESEARCH FOUNDATION, INC.; UTBATTELLE, LLC
Reel/Frame 062788/0055 →
Continuity (6)
Continuation 17664165 · May 19, 2022
Continuation 16692439 · Nov 22, 2019
Continuation 16394531 · Apr 25, 2019
Division 15123172
Provisional Application 61947603 · Mar 4, 2014
Related Publication 20230227944A1 · Jul 20, 2023