IP Library Granted Patent US 12,590,250
Granted Patent B2
US 12,590,250 · App. 18/192,320 · Granted Mar 31, 2026

System and method for separating bitumen from shingle powder

Inventors: William Lovell Lawrence (Louisville, KY); Edward Merrel Brownlee (Louisville, KY); Alexander Bennett Hoekstra (Louisville, KY); Michael Thomas Earl (Jeffersonville, IN); Jonathon Daniel Horton (Barrington, RI)
Assignee: Redivius, Inc.
C10C3/08B01D3/00B01D11/028B01D11/0288
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Quick Facts
Patent No.
US 12,590,250
App. No.
18/192,320
Granted
Mar 31, 2026
Kind
B2
Abstract

A system for separating bitumen from shingle powder includes: a blender; a solvent tank in fluid communication with the blender; a water tank in fluid communication with the blender; a decanting tank in fluid communication with the blender; a distillation tank in fluid communication with the decanting tank; and a plurality of pumps for pumping fluids between various components of the system or out of the system. When the system is in use, the blender receives and mixes solvent from the solvent tank with shingle powder containing bitumen to produce a bitumen-infused solvent. Water is supplied to the blender from the water tank to wash an interior of the blender. Bitumen-infused solvent received in the decanting tank from the blender is separated from excess water. Bitumen within the bitumen-infused solvent is isolated within the distillation tank.

Claims (62)

1 . A system for separating bitumen from shingle powder, comprising:

a blender configured to receive and mix a solvent and shingle powder containing bitumen and one or more non-bitumen constituents to separate the bitumen from the one or more non-bitumen constituents and produce a bitumen-infused solvent;

a plurality of tanks, including

a solvent tank in fluid communication with the blender, the solvent tank supplying the solvent to the blender,

a water tank in fluid communication with the blender, the water tank supplying water to wash an interior of the blender in which the solvent and the shingle powder is mixed,

a decanting tank in fluid communication with the blender, the decanting tank configured to receive the bitumen-infused solvent from the blender and to separate the bitumen-infused solvent from the water, and

a distillation tank in fluid communication with the decanting tank, wherein the distillation tank is configured to vaporize the solvent of the bitumen-infused solvent to isolate bitumen from the bitumen-infused solvent received from the decanting tank, resulting in an isolated bitumen in the distillation tank; and

a plurality of pumps, with each pump of the plurality of pumps configured to either (i) pump fluid from one tank of the plurality of tanks to one of the blender and another tank of the plurality of tanks or (ii) pump fluid from the blender to one of the plurality of tanks.

2 . The system according to claim 1 , and further comprising a filter in fluid communication with the decanting tank, such that the bitumen-infused solvent passes through the filter prior to reaching the distillation tank.

3 . The system according to claim 1 , and further comprising a membrane in fluid communication with the water tank, such that the water supplied to the blender by the water tank passes through the membrane prior to reaching the blender.

4 . The system according to claim 1 , and further comprising an inert gas source in fluid communication with at least one of the blender, the water tank, the decanting tank, and the distillation tank.

5 . The system according to claim 4 , wherein the inert gas source is configured to supply nitrogen gas to the at least one of the blender, the water tank, the decanting tank, and the distillation tank.

6 . The system according to claim 4 , wherein the inert gas source is in fluid communication with the blender, the decanting tank, and the distillation tank.

7 . The system according to claim 1 , wherein the distillation tank includes a vacuum distillation vessel in which the solvent of the bitumen-infused solvent is evaporated and the isolated bitumen is liquefied.

8 . The system according to claim 1 , and further comprising a heat and solvent recovery subsystem in fluid communication with the distillation tank and the solvent tank and configured to condense solvent vapor from the distillation tank to a distillate solvent, the heat and solvent recovery subsystem including:

at least one of (a) one or more heat exchangers and (b) a condenser to condense solvent vapor received from the distillation tank to the distillate solvent; and

a pump positioned downstream of the at least one of the (a) one or more heat exchangers and (b) the condenser and configured to pump the distillate solvent to the solvent tank.

9 . The system according to claim 8 ,

wherein the heat and solvent recovery subsystem includes the one or more heat exchangers, with the one or more heat exchangers including a heat exchanger that is in fluid communication with the solvent tank, and is configured to receive the solvent vapor from one of the distillation tank and another heat exchanger of the solvent recovery subsystem; and

wherein solvent from the solvent tank is circulated through the heat exchanger in fluid communication with the solvent tank and heated by solvent vapor within the heat exchanger in fluid communication with the solvent tank when the system is in use.

10 . The system according to claim 1 , and further comprising a heat and solvent recovery subsystem, which includes:

one or more heat exchangers;

a condenser; and

a pump;

wherein the condenser is positioned downstream of the one or more heat exchangers, and the pump is positioned downstream of the condenser.

11 . The system according to claim 1 , and further comprising a collection tank in fluid communication with the distillation tank and configured to receive the isolated bitumen from the distillation tank.

12 . The system according to claim 11 , wherein the collection tank includes a heater for maintaining the isolated bitumen received from the distillation tank in a liquefied state.

13 . The system according to claim 1 , wherein the solvent is limonene, n-Propyl Bromide (nPB), a fluorinated solvent, toluene, hexane, 1,2-trans-dichloroethylene, or a combination thereof.

14 . A system for separating bitumen from shingle powder, comprising:

a blender configured to receive and mix a solvent and shingle powder containing bitumen;

a plurality of tanks, including

a solvent tank in fluid communication with the blender, the solvent tank supplying the solvent to the blender,

a water tank in fluid communication with the blender, the water tank supplying water to wash an interior of the blender in which the solvent and the shingle powder is mixed,

a decanting tank in fluid communication with the blender, the decanting tank configured to receive bitumen-infused solvent from the blender, and

a distillation tank in fluid communication with the decanting tank, wherein the distillation tank is configured to vaporize the solvent of the bitumen-infused solvent to isolate bitumen from the bitumen-infused solvent received from the decanting tank, resulting in an isolated bitumen in the distillation tank;

a plurality of pumps, with each pump of the plurality of pumps configured to either (i) pump fluid from one tank of the plurality of tanks to one of the blender and another tank of the plurality of tanks or (ii) pump fluid from the blender to one of the plurality of tanks; and

a heat and solvent recovery subsystem, which includes:

a first heat exchanger in fluid communication with the water tank and the distillation tank, such that solvent vapor from the distillation tank is passed through the first heat exchanger while water from the water tank is simultaneously circulated through the first heat exchanger when the system is in use,

a second heat exchanger in fluid communication with the first heat exchanger and the solvent tank, such that solvent vapor from the first heat exchanger can be passed through the second heat exchanger while the solvent from the solvent tank is simultaneously circulated through the second heat exchanger, and

a condenser, wherein the condenser is in fluid communication with the second heat exchanger and is configured to form a distillate solvent.

15 . A method for separating bitumen from shingle powder, comprising steps of:

mixing, in a blender, shingle powder containing bitumen and one or more non-bitumen constituents with a solvent to separate bitumen from the one or more non-bitumen constituents and produce a bitumen-infused solvent;

decanting the bitumen-infused solvent from the blender into a first tank;

washing, within the blender, the one or more non-bitumen constituents with water to produce additional bitumen-infused solvent;

decanting the additional bitumen-infused solvent from the blender into the first tank;

separating, within the first tank, the bitumen-infused solvent and the additional bitumen-infused solvent from water present in the first tank;

transferring, subsequent to separation of the bitumen-infused solvent and the additional bitumen-infused solvent from water within the first tank, the bitumen-infused solvent and the additional bitumen-infused solvent within the first tank into a second tank; and

vaporizing, in the second tank, the solvent from the bitumen-infused solvent and the additional bitumen-infused solvent, resulting in an isolated bitumen in the second tank.

16 . The method according to claim 15 , and further comprising a step of filtering the bitumen-infused solvent and the additional bitumen-infused solvent.

17 . The method according to claim 15 , and further comprising a step of injecting an inert gas into at least one of the blender, the first tank, and the second tank.

18 . The method according to claim 17 , wherein the inert gas is injected into the blender, the first tank, and the second tank.

19 . The method according to claim 15 , and further comprising a step of liquefying, in the second tank, the isolated bitumen.

20 . The method according to claim 19 , and further comprising steps of:

transferring the liquefied isolated bitumen from the second tank into a third tank; and

heating, in the third tank, the liquefied isolated bitumen.

21 . The method according to claim 15 , and further comprising steps of:

condensing solvent vapor from the second tank to form a distillate solvent; and

transferring the distillate solvent to a solvent supply source in fluid communication with the blender.

22 . The method according to claim 15 , and further comprising a step of:

passing solvent vapor from the second tank through a heat exchanger in fluid communication with a solvent supply source as solvent from the solvent supply source is simultaneously circulated through the heat exchanger.

23 . The method according to claim 15 , wherein, in the step of transferring the bitumen-infused solvent and the additional bitumen-infused within the first tank into the second tank, the bitumen-infused solvent and the additional bitumen-infused solvent is transferred in discrete batches.

24 . The method according to claim 15 , wherein the solvent is limonene, n-Propyl Bromide (nPB), a fluorinated solvent, toluene, hexane, and 1,2-trans-dichloroethylene, or a combination thereof.

Assignments (5)
CHANGE OF NAME Recorded Aug 21, 2025
From: REDIVIUS, LLC
To: REDIVIUS, INC.
Reel/Frame 072516/0037 →
SECURITY INTEREST Recorded Sep 27, 2024
From: REDIVIUS, LLC
To: OWENS CORNING VENTURE INVESTMENTS, LLC
Reel/Frame 068729/0782 →
NUNC PRO TUNC ASSIGNMENT Recorded Aug 21, 2024
From: CRS-SPV INC.
To: REDIVIUS, LLC
Reel/Frame 068352/0385 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 19, 2024
From: HORTON, JONATHON DANIEL
To: CRS-SPV INC.
Reel/Frame 066491/0130 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 19, 2024
From: LAWRENCE, WILLIAM LOVELL; BROWNLEE, EDWARD MERREL; HOEKSTRA, ALEXANDER BENNETT; EARL, MICHAEL THOMAS
To: CRS-SPV INC.
Reel/Frame 066491/0167 →
Continuity (2)
Provisional Application 63324872 · Mar 29, 2022
Related Publication 20230313045A1 · Oct 5, 2023
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