IP Library Granted Patent US 9,533,921
Granted Patent B2
US 9,533,921 · App. 14/293,248 · Granted Jan 3, 2017

Zeolitic catalytic conversion of alochols to hydrocarbons

Inventors: Chaitanya K. Narula (Knoxville, TN); Brian H. Davison (Knoxville, TN); Martin Keller (Knoxville, TN)
Assignee: UT-BATTELLE, LLC.
C07C1/22B01J29/061B01J29/072B01J29/076B01J29/46B01J29/48B01J35/023B01J35/04B01J37/0246C10G3/45C10G3/49C12P7/06C12P7/08C12P7/10C12P7/16B01J29/143B01J29/146B01J29/163B01J29/166B01J29/68B01J29/69B01J29/7615B01J29/7661B01J29/7669B01J29/7692B01J29/7815B01J29/7861B01J29/7869B01J29/7892B01J2229/183B01J2229/186C10G2300/1011C10G2300/1014C10G2300/4006C10G2400/02C10G2400/04C10G2400/08Y02E50/10Y02E50/16Y02E50/17Y02P30/20
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Quick Facts
Patent No.
US 9,533,921
App. No.
14/293,248
Granted
Jan 3, 2017
Kind
B2
Abstract

A method for converting an alcohol to a hydrocarbon, the method comprising contacting said alcohol with a metal-loaded zeolite catalyst at a temperature of at least 100° C. and up to 550° C., wherein said alcohol can be produced by a fermentation process, said metal is a positively-charged metal ion, and said metal-loaded zeolite catalyst is catalytically active for converting said alcohol to said hydrocarbon.

Claims (20)

1. A method for converting an alcohol to a hydrocarbon product containing comprising no more than 20% C 2 hydrocarbon compounds, the method comprising contacting said alcohol with a vanadium-loaded ZSM-5 zeolite catalyst at a temperature of at least 250° C. and up to 350° C. and at a liquid hourly space velocity of up to 5 hr −1 , wherein said alcohol can be produced by a fermentation process and is selected from ethanol, butanol, isobutanol, or combination thereof and is a component of an aqueous solution in a concentration of no more than about 20%.

2. The method of claim 1 , wherein said alcohol comprises ethanol.

3. The method of claim 1 , wherein said concentration is no more than about 10%.

4. The method of claim 1 , wherein said alcohol is produced by a fermentation process.

5. The method of claim 4 , wherein said alcohol is a component of a fermentation stream when contacted with said vanadium-loaded ZSM-5 zeolite catalyst.

6. The method of claim 1 , wherein said vanadium-loaded ZSM-5 zeolite catalyst comprises V-ZSM5.

7. The method of claim 1 , wherein said hydrocarbon product is a mixture of hydrocarbon compounds, wherein said mixture is useful as a fuel or as a blendstock component of a fuel.

8. The method of claim 7 , wherein said mixture of hydrocarbon compounds is comprised of hydrocarbon compounds containing at least four carbon atoms.

9. The method of claim 7 , wherein said mixture of hydrocarbon compounds substantially corresponds to a petrochemical fraction.

10. The method of claim 1 , wherein said method is integrated with a fermentation process, wherein said fermentation process produces said alcohol as a component of a fermentation stream, and said fermentation stream is contacted with said vanadium-loaded ZSM-5 zeolite catalyst.

11. The method of claim 1 , wherein said method is integrated with a biomass reactor that includes a fermentation process, wherein said fermentation process produces said alcohol as a component of a fermentation stream, and said fermentation stream is contacted with said vanadium-loaded ZSM-5 zeolite catalyst.

12. The method of claim 9 , wherein said method further comprises distilling said mixture of hydrocarbon compounds to obtain a fraction of said mixture of hydrocarbon compounds.

13. The method of claim 1 , wherein said alcohol is produced from a biomass source.

14. The method of claim 13 , wherein said biomass source comprises lignocellulosic matter.

15. The method of claim 4 , wherein said fermentation process produces said alcohol from a biomass source.

16. The method of claim 15 , wherein said biomass source comprises lignocellulosic matter.

17. The method of claim 1 wherein the alcohol comprises n-butanol or isobutanol.

18. The method of claim 13 , wherein said biomass source of comprises starch or sugar.

19. The method of claim 4 , wherein said fermentation process produces said alcohol from a plant-based source of sugars.

20. The method of claim 1 , wherein said liquid hourly space velocity is up to 3 hr −1 .

Continuity (3)
Continuation 14123363
Provisional Application 61497256 · Jun 15, 2011
Related Publication 20140273146A1 · Sep 18, 2014