IP Library › Granted Patent US 10,096,684
Granted Patent B2
US 10,096,684 · App. 15/391,186 · Granted Oct 9, 2018

Metal oxide film and semiconductor device

Inventors: Yasuharu Hosaka (Tochigi, JP); Toshimitsu Obonai (Tochigi, JP); Yukinori Shima (Gunma, JP); Masami Jintyou (Tochigi, JP); Daisuke Kurosaki (Tochigi, JP); Takashi Hamochi (Tochigi, JP); Junichi Koezuka (Tochigi, JP); Kenichi Okazaki (Tochigi, JP); Shunpei Yamazaki (Tokyo, JP)
Assignee: Semiconductor Energy Laboratory Co., Ltd.
H01L29/24C03C17/245C04B35/01C04B35/453C04B35/62218C23C14/08C23C14/5853H01L29/7869C03C2217/23C03C2218/151C04B2235/3217C04B2235/3225C04B2235/3284C04B2235/3286C04B2235/3293C04B2235/787C04B2235/96
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Quick Facts
Patent No.
US 10,096,684
App. No.
15/391,186
Granted
Oct 9, 2018
Kind
B2
Abstract

A metal oxide film includes indium, M, (M is Al, Ga, Y, or Sn), and zinc and includes a region where a peak having a diffraction intensity derived from a crystal structure is observed by X-ray diffraction in the direction perpendicular to the film surface. Moreover, a plurality of crystal parts is observed in a transmission electron microscope image in the direction perpendicular to the film surface. The proportion of a region other than the crystal parts is higher than or equal to 20% and lower than or equal to 60%.

Claims (26)

1. A metal oxide film comprising:

indium;

M which is Al, Ga, Y, or Sn; and

zinc,

wherein a peak having a diffraction intensity derived from a crystal structure is observed by X-ray diffraction in a direction perpendicular to a surface of the metal oxide film,

wherein a plurality of crystal parts is observed in a transmission electron microscope image in the direction perpendicular to the surface of the metal oxide film, and

wherein a proportion of a region other than the plurality of crystal parts is higher than or equal to 20% and lower than or equal to 60%.

2. The metal oxide film according to claim 1 , wherein the plurality of crystal parts has a higher proportion of crystal parts in which c-axes are aligned in a thickness direction than crystal parts aligned in other directions.

3. The metal oxide film according claim 1 ,

wherein in a second image obtained in such a manner that a first image that is an image obtained by subjecting a cross-sectional TEM image to fast Fourier transform is subjected to inverse fast Fourier transform after mask treatment by which a periodic region remains, the proportion of the remaining area subtracted from an original image is more than or equal to 20% and less than 60%.

4. The metal oxide film according to claim 1 ,

wherein when electron diffraction with a probe diameter of 50 nm or more is performed on a slice of the metal oxide film having a thickness of greater than or equal to 10 nm and less than or equal to 50 nm in the direction perpendicular to its cross section, a first electron diffraction pattern that includes a ring-like diffraction pattern and two first spots overlapping with the ring-like diffraction pattern is observed, and

wherein when electron diffraction with a probe diameter of greater than or equal to 0.3 nm and less than or equal to 5 nm is performed thereon, a second electron diffiaction pattern that includes the two first spots and a plurality of second spots distributed in a circumferential direction is observed.

5. The metal oxide film according to claim 4 ,

wherein the two first spots are symmetric with respect to a center,

wherein an angle between a first straight line and the direction of a normal vector of the surface of the metal oxide film is more than or equal to 0° and less than or equal to 10°, and

wherein the first straight line passes through the center and a point at which the luminance of the two first spots is the highest.

6. The metal oxide film according to claim 5 ,

wherein in the first electron diffraction pattern, the luminance of the ring-like diffraction pattern is lower than that of the two first spots at a point of intersection of the ring-like diffiaction pattern and a second straight line that intersects with the first straight line.

7. The metal oxide film according to claim 6 ,

wherein the luminance of the two first spots is greater than 1 time and less than or equal to 9 times the luminance of the ring-like diffraction pattern at the point of intersection of the ring-like diffraction pattern and the second straight line.

8. A semiconductor device comprising:

a semiconductor layer;

a gate insulating layer; and

a gate,

wherein the semiconductor layer includes the metal oxide film according to claim 1 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 5, 2017
From: HOSAKA, YASUHARU; OBONAI, TOSHIMITSU; SHIMA, YUKINORI; JINTYOU, MASAMI; KUROSAKI, DAISUKE; HAMOCHI, TAKASHI; KOEZUKA, JUNICHI; OKAZAKI, KENICHI; YAMAZAKI, SHUNPEI
To: SEMICONDUCTOR ENERGY LABORATORY CO., LTD.
Reel/Frame 042597/0099 →
Priority Claims (2)
JP 2015-257710 · Dec 29, 2015 · national
JP 2016-125478 · Jun 24, 2016 · national
Continuity (1)
Related Publication 20170186843A1 · Jun 29, 2017
Cited By (3)
US 12,363,955 US 12,378,656 US 12,490,470