IP Library › Granted Patent US 10,131,715
Granted Patent B2
US 10,131,715 · App. 14/778,323 · Granted Nov 20, 2018

Cellulose particulate material

Inventors: David Hepworth (Burntisland, GB); Eric Whale (Burntisland, GB)
Assignee: CELLUCOMP LIMITED
C08B15/00A23L29/262A23L33/24A61K8/0241A61K8/731A61K8/97A61Q19/00C04B18/248C04B24/383C04B28/02C08H8/00C08L1/02C08L97/02C09D5/024C09D7/43C09D101/02C09D197/02D21H17/02D21H17/24D21H17/25D21H21/14A23V2002/00A61K2800/10A61K2800/412C08L2205/18Y02W30/97
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Quick Facts
Patent No.
US 10,131,715
App. No.
14/778,323
Granted
Nov 20, 2018
Kind
B2
Abstract

The invention relates to plant-derived cellulose-containing particles useful as rheology modifiers and to a process for preparing cellulose-containing particles from plant material, which process involves treating said plant material with a peroxide reagent. The process can be controlled to produce cellulose-containing particle having a viscosity up to about 7500 or 8000 cps.

Claims (25)

1. Plant-derived cellulose particulate material comprising

less than 30 wt % extractable glucose; and

extractable xylose in an amount of at least 0.8 wt %, and wherein the cellulose particulate material increases viscosity of an aqueous composition greater than 2500 cps when added at a concentration of 1 wt %.

2. Plant-derived cellulose particulate material according to claim 1 , comprising less than 60 wt % cellulose.

3. Plant-derived cellulose particulate material according to claim 1 , wherein the plant material is derived from sugar beet.

4. Plant-derived cellulose particulate material according to claim 1 , having a non-carbohydrate content of 20 to 50% by dry weight.

5. Plant-derived cellulose particulate material according to claim 1 , wherein the cellulose particulate material comprises particles having a mean major dimension of from 1 to 250 μm.

6. Plant-derived cellulose particulate material according to claim 1 , wherein the cellulose particulate material comprises a plurality of particles having a water-holding capacity in the range of 90 to 99.5% by weight.

7. Plant-derived cellulose particulate material according to claim 1 , wherein the cellulose particulate material comprises particles having a cellulose content of from 40 to 60 wt %, a mean major dimension of 10 to 70 μm and wherein the cellulose particulate material increases viscosity of an aqueous composition up to 5000 cps when added at a concentration of 1 wt %.

8. A process for preparing cellulose-containing particulate material from a herbaceous plant material, the process comprising the steps of:

(i) contacting the herbaceous plant material with a peroxide reagent and water to form a mixture;

(ii) heating the mixture to a temperature of from 30 to 110° C. and maintaining said mixture at a temperature of from 30 to 110° C. until the pH of the mixture has dropped by from about 1 to 2 pH units; and

(iii) isolating the cellulose-containing particulates,

wherein the cellulose containing particulate material contains less than 30 wt % extractable glucose, extractable xylose in an amount of at least 0.8 wt %, and wherein the particulate material increases viscosity of an aqueous composition greater than 2500 cps when added at a concentration of 1 wt %.

9. The process according to claim 8 , wherein the herbaceous plant material comprises greater than 30% by volume of parenchymal cell material.

10. The process according to claim 8 , wherein the herbaceous plant material comprises less than about 10 wt % lignocellulose.

11. The process according to claim 8 , wherein the herbaceous plant material is a root vegetable.

12. The process according to claim 8 , wherein the contacting step includes mechanically treating the herbaceous plant material so that it comprises particles with a major dimension of less than 10 mm.

13. The process according to claim 8 , wherein the heating step involves mechanically homogenizing the mixture while the mixture is being maintained at said temperature.

14. The process according to claim 8 , wherein heating the mixture comprises heating to a temperature of from 70 and 100° C. and maintaining at a temperature of from 70 and 100° C.

15. The process according to claim 8 , wherein the process is carried out in the absence of an alkali or acid reagent and wherein the process is carried out in the absence of a pH-modifying additive.

16. The process according to claim 8 , further comprising contacting the cellulose-containing particulates with an oxidant.

17. Plant-derived cellulose particulate material according to claim 1 , wherein the cellulose particulate material comprises extractable xylose in an amount of at least 1.5 wt %.

18. Plant-derived cellulose particulate material according to claim 1 , wherein the cellulose particulate material comprises hemicellulose less than 2 wt %.

19. The process according to claim 8 , wherein the cellulose-containing particulate material comprises extractable xylose in an amount of at least 1.5 wt % and hemicellulose less than 2 wt %.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 18, 2015
From: HEPWORTH, DAVID; WHALE, ERIC
To: CELLUCOMP LIMITED
Reel/Frame 036640/0338 →
Priority Claims (1)
GB 1304939.0 · Mar 18, 2013 · national
Continuity (1)
Related Publication 20160168273A1 · Jun 16, 2016
Cited By (3)
US 12,263,184 US 12,269,903 US 12,589,058