IP Library › Granted Patent US 10,265,320
Granted Patent B2
US 10,265,320 · App. 15/164,324 · Granted Apr 23, 2019

Amino, amido and heterocyclic compounds as modulators of rage activity and uses thereof

Inventors: Ann Marie Schmidt (Franklin Lakes, NJ); Ravichandran Ramasamy (Ardsley, NY); Alexander Shekhtman (Glenmont, NY); Vivek Rai (Allahabad, IN); Michaele B. Manigrasso (New York, NY)
Assignees: The Research Foundation for The State University of New York; New York Universirty
A61K31/5377A61K31/137A61K31/167A61K31/185A61K31/353A61K31/357A61K31/403A61K31/4045A61K31/4184A61K31/426A61K31/427A61K31/44A61K31/4439A61K31/454A61K31/47A61K31/4985A61K31/505A61K31/506A61K31/52C07D213/75C07D239/42C07D277/28C07D319/20
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Quick Facts
Patent No.
US 10,265,320
App. No.
15/164,324
Granted
Apr 23, 2019
Kind
B2
Abstract

Amino, amido, and heterocyclic compounds are disclosed. The compounds may be prepared as pharmaceutical compositions, and may be used for the prevention and treatment of a variety of conditions in mammals including humans, including by way of non-limiting example, diabetes complications, inflammation, and neurodegeneration, obesity, cancer, ischemia/reperfusion injury, cardiovascular disease and other diseases related to RAGE activity.

Claims (177)

1. A method for treating or ameliorating in a mammal a disease or condition that is causally related to RAGE activity in vivo, which comprises administering to the mammal an effective disease-treating or condition-treating amount of a compound according to formula A-Ia or A-Ib:

wherein

L 1 is —NH—, —CH 2 —NH—, —CH 2 —CH 2 —NH—, —CO—NH— or —CO—NH-L 2 -CO—NH—; and Cy is substituted or unsubstituted aryl or substituted or unsubstituted heteroaryl; or

L 1 is a bond and Cy is

R 1 is H, substituted or unsubstituted C 1 -C 6 alkyl, substituted or unsubstituted C 1 -C 6 alkoxy, or halo;

each R 2 is independently selected from substituted or unsubstituted alkyl, substituted or unsubstituted alkoxy, substituted or unsubstituted acyl, substituted or unsubstituted acylamino, substituted or unsubstituted alkylamino, substituted or unsubstituted alkythio, substituted or unsubstituted alkoxycarbonyl, substituted or unsubstituted alkylarylamino, substituted or unsubstituted amino, substituted or unsubstituted arylalkyl, substituted sulfinyl, substituted sulfanyl, unsubstituted aminosulfonyl, substituted or unsubstituted alkylsulfonyl, substituted or unsubstituted arylsulfonyl, azido, substituted or unsubstituted carbamoyl, carboxyl, cyano, substituted or unsubstituted aryl, substituted or unsubstituted heteroaryl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted dialkylamino, halo, nitro, and thiol; or two adjacent R 1 and R 2 groups may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring;

R 3 is H, or substituted or unsubstituted C 1 -C 6 alkyl;

the subscript n is 0, 1, 2, or 3;

L 2 is C 1 -C 3 alkylene;

X is CH or N; Y is O or NR 5 ;

R 4 is substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, or substituted or unsubstituted heteroaryl;

R 5 is H or substituted or unsubstituted alkyl; and * represents an attachment point; or a pharmaceutically acceptable salt, solvate or prodrug thereof;

and stereoisomers, isotopic variants and tautomers thereof;

and wherein the disease or condition is diabetes.

2. The method according to claim 1 , wherein the compound is according to formula A-II, A-III, A-IV, A-V, A-VI, A-VII:

wherein Cy, X, Y, R 1 , R 2 , R 3 , R 4 , and n are as in claim 1 .

3. The method according to claim 1 , wherein the compound is according to formula A-XIVa, A-XIVb, or A-XIVd:

4. The method according to claim 1 , wherein the compound is according to A-XV:

5. The method according to claim 1 , wherein the compound is according to formula A-XVIa or A-XVIb:

6. The method according to claim 1 , wherein the compound is according to formula A-XXa or A-XXb:

7. The method according to claim 1 , wherein the compound is according to formula A-XIVa, A-XIVb, A-XIVd, A-XV, A-XVIb, or A-XXa:

8. The method according to claim 1 , wherein the compound is any one of the compounds listed in Table 1, or Table 2 below:

TABLE 1

Compd #

Structure

CB-1

CB-6

CB-7

CB-8

CB-13

CB-14

CD-1

CD-21

TABLE 2

ID

STRUCTURE

201

202

203

204

205

206

207

208

209

210

211

212

213

214

215

216

217

218

219

220

221

222

223

224

225

226

227

228

229

230

231

232

233

234

235

236

237

238

239

240

241

242

243

244

245

246

247

248

249

250

251

252

253

254

255

256

257

258

259

260

261

262

263

264

265

266

267

268

269

270

271

272

273

274

275

276

277

278

279

280

281

282

283

284

285

286

287

288

289

290

291

.

9. The method according to claim 1 , wherein R 1 is independently selected from H, halo, substituted or unsubstituted C 1 -C 6 alkyl, and substituted or unsubstituted C 1 -C 6 alkoxy; and each R 2 is independently selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, methylthio, and substituted or unsubstituted C 1 -C 6 alkoxy.

10. The method according to claim 2 , wherein R 1 is independently selected from H, halo, substituted or unsubstituted C 1 -C 6 alkyl, and substituted or unsubstituted C 1 -C 6 alkoxy; and each R 2 is independently selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, methylthio, and substituted or unsubstituted C 1 -C 6 alkoxy.

11. The method according to claim 1 , wherein Cy is:

a) phenyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, carboxy, carbalkoxy, and substituted or unsubstituted C 1 -C 6 alkoxy;

b) pyridyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, and substituted or unsubstituted C 1 -C 6 alkoxy;

c) substituted or unsubstituted pyrrolyl, imidazolyl, triazolyl, thienyl, furanyl, thiazolyl, or oxazolyl; or

d) substituted or unsubstituted thiazolyl.

12. The method according to claim 1 , wherein Cy is thiazolyl, substituted with difluorophenyl.

13. The method according to claim 1 , wherein the compound is according to formula A-VIIIa, A-VIIIb, A-VIIId, A-IX, A-Xa, or A-Xb :

wherein Cy, and R 1 are as in claim 1 .

14. The method according to claim 13 , wherein Cy is:

a) phenyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, carboxy, carbalkoxy, and substituted or unsubstituted C 1 -C 6 alkoxy;

b) pyridyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, and substituted or unsubstituted C 1 -C 6 alkoxy;

c) substituted or unsubstituted pyrrolyl, imidazolyl, triazolyl, thienyl, furanyl, thiazolyl, or oxazolyl; or

d) substituted or unsubstituted thiazolyl.

15. The method according to claim 13 , wherein Cy is thiazolyl, substituted with difluorophenyl.

16. The method according to claim 13 , wherein R 1 is independently selected from H, halo, amino, substituted amino, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, and substituted or unsubstituted C 1 -C 6 alkoxy.

17. The method according to claim 1 , wherein the compound is according to formula A-XIa, A-XIb, A-XId, A-XII, A-XIIa, or A-XIIIb:

wherein Cy is as in claim 1 .

18. The method according to claim 17 , wherein Cy is:

a) phenyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, carboxy, carbalkoxy, and substituted or unsubstituted C 1 -C 6 alkoxy;

b) pyridyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, and substituted or unsubstituted C 1 -C 6 alkoxy;

c) substituted or unsubstituted pyrrolyl, imidazolyl, triazolyl, thienyl, furanyl, thiazolyl, or oxazolyl; or

d) substituted or unsubstituted thiazolyl.

19. The method according to claim 17 , wherein Cy is thiazolyl, substituted with difluorophenyl.

20. The method according to claim 1 , wherein the compound is according to formula A-XVIIIa or A-XVIIIb:

wherein R 1 is halo, amino, substituted amino, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, or substituted or unsubstituted C 1 -C 6 alkoxy; R 4 is substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, or substituted or unsubstituted heteroaryl; and Y is O, NH, or N—Me.

21. A method for treating or ameliorating in a mammal a disease or condition that is causally related to RAGE activity in vivo, which comprises administering to the mammal an effective disease-treating or condition-treating amount of a compound according to formula A-Ia:

wherein

L 1 is —NH—, —CH 2 —NH—, —CH 2 —CH 2 —NH—, —CO—NH— or —CO—NH-L 2 -CO—NH—; and Cy is substituted or unsubstituted aryl or substituted or unsubstituted heteroaryl; or

L 1 is a bond and Cy is

R 1 is H, substituted or unsubstituted C 1 -C 6 alkyl, substituted or unsubstituted C 1 -C 6 alkoxy, or halo;

each R 2 is independently selected from substituted or unsubstituted alkyl, substituted or unsubstituted alkoxy, substituted or unsubstituted acyl, substituted or unsubstituted acylamino, substituted or unsubstituted alkylamino, substituted or unsubstituted alkythio, substituted or unsubstituted alkoxycarbonyl, substituted or unsubstituted alkylarylamino, substituted or unsubstituted amino, substituted or unsubstituted arylalkyl, substituted sulfinyl, substituted sulfanyl, unsubstituted aminosulfonyl, substituted or unsubstituted alkylsulfonyl, substituted or unsubstituted arylsulfonyl, azido, substituted or unsubstituted carbamoyl, carboxyl, cyano, substituted or unsubstituted aryl, substituted or unsubstituted heteroaryl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted dialkylamino, halo, nitro, and thiol; or two adjacent R 1 and R 2 groups may join together to form a substituted or unsubstituted carbocyclic or heterocyclic ring;

the subscript n is 0, 1, 2, or 3;

L 2 is C 1 -C 3 alkylene;

X is CH or N; Y is O or NR 5 ;

R 4 is substituted or unsubstituted alkyl, substituted or unsubstituted cycloalkyl, substituted or unsubstituted aryl, or substituted or unsubstituted heteroaryl;

R 5 is H or substituted or unsubstituted alkyl; and * represents an attachment point; or a pharmaceutically acceptable salt, solvate or prodrug thereof;

and stereoisomers, isotopic variants and tautomers thereof;

and wherein the disease or condition is diabetes.

22. The method according to claim 21 , wherein the compound is according to formula A-VI:

wherein Cy, R 1 , R 2 , and n are as in claim 21 .

23. The method according to claim 22 , wherein R 1 is independently selected from H, halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, and substituted or unsubstituted C 1 -C 6 alkoxy; and each R 2 is independently selected from halo, amino, substituted amino, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, methylthio, and substituted or unsubstituted C 1 -C 6 alkoxy.

24. The method according to claim 22 , wherein Cy is:

a) phenyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, carboxy, carbalkoxy, and substituted or unsubstituted C 1 -C 6 alkoxy;

b) pyridyl substituted with one or more groups selected from halo, substituted or unsubstituted C 1 -C 6 alkyl, CN, OH, —NHAc, Cl, —SMe, and substituted or unsubstituted C 1 -C 6 alkoxy;

c) substituted or unsubstituted pyrrolyl, imidazolyl, triazolyl, thienyl, furanyl, thiazolyl, or oxazolyl; or

d) substituted or unsubstituted thiazolyl.

25. The method according to claim 22 , wherein Cy is thiazolyl, substituted with difluorophenyl.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 2, 2016
From: SCHMIDT, ANN MARIE; RAMASAMY, RAVICHANDRAN; MANIGRASSO, MICHAELE B.; RAI, VIVEK
To: NEW YORK UNIVERSITY
Reel/Frame 040200/0134 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 2, 2016
From: SHEKHTMAN, ALEXANDER
To: THE RESEARCH FOUNDATION FOR THE STATE UNIVERSITY OF NEW YORK
Reel/Frame 040200/0454 →
Continuity (4)
Division 14503919 · Oct 1, 2014
Provisional Application 61885183 · Oct 1, 2013
Provisional Application 61885176 · Oct 1, 2013
Related Publication 20160263125A1 · Sep 15, 2016
Cited By (1)
US 12,234,231