IP Library › Granted Patent US 10,329,178
Granted Patent B2
US 10,329,178 · App. 15/908,844 · Granted Jun 25, 2019

Chelating base product for use in water-based system treatments

Inventors: David Nicholas (Gulf Breeze, FL); Reid Henry Bowman (Fort Collins, CO); Freddie L. Singleton (Fruit Cove, FL)
Assignee: EARTH SCIENCE LABORATORIES
C02F1/683C02F1/50C05C3/00C05D5/00C05D9/00C05D9/02C05G3/0064C02F1/505C02F1/68C02F2101/10C02F2103/42C02F2303/02C02F2303/04
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Quick Facts
Patent No.
US 10,329,178
App. No.
15/908,844
Granted
Jun 25, 2019
Kind
B2
Abstract

A base product fluid is produced by adding anhydrous liquid ammonia and a first portion of sulfuric acid to water in a process line to form a mixed fluid. The mixed fluid may be cooled and a second portion of sulfuric acid may be added to the mixed fluid to form the base product fluid. The base product fluid may include a molecular compound that is a chelating compound. The molecular compound may have the formula: ((NH 4 ) 2 SO 4 ) a .(H 2 SO 4 ) b .(H 2 O) c .(NH 4 HSO 4 ) x . In the formula, a may be between 1 and 5, b may be between 1 and 5, c may be between 1 and 5, and x may be between 1 and 10.

Claims (12)

1. A base product fluid comprising a molecular cluster compound which is a combination of ammonium sulfate, ammonium bisulfate, sulfuric acid, and water;

wherein the molecular cluster compound comprises 1 to 5 molecules of ammonium sulfate, 1 to 10 molecules of ammonium bisulfate, 1 to 5 molecules of sulfuric acid, and 1 to 5 molecules of water.

2. The base product fluid of claim 1 , wherein the molecular cluster compound comprises a mass percentage of hydrogen between about 3% and 6%, a mass percentage of nitrogen between about 10% and about 15%, a mass percentage of sulfur between about 25% and about 30%, and a mass percentage of oxygen between about 52% and about 60%.

3. The base product fluid of claim 2 , wherein the molecular cluster compound comprises a mass percentage of hydrogen between about 4% and 5%, a mass percentage of nitrogen between about 11% and about 15%, a mass percentage of sulfur between about 26% and about 28%, and a mass percentage of oxygen between about 53% and about 57%.

4. The base product fluid of claim 3 , wherein the molecular cluster compound comprises a mass percentage of hydrogen of about 4.7%, a mass percentage of nitrogen of about 14.8%, a mass percentage of sulfur of about 26.5%, and a mass percentage of oxygen of about 54%.

5. The base product fluid of claim 1 , wherein the molecular cluster compound is a chelating agent.

6. The base product fluid of claim 1 , wherein the molecular cluster compound comprises 1 to 3 molecules of ammonium sulfate, 1 to 6 molecules of ammonium bisulfate, 1 to 3 molecules of sulfuric acid, and 1 to 3 molecules of water.

7. The base product fluid of claim 6 , wherein the molecular cluster compound comprises 1 molecule of ammonium sulfate, 1 to 6 molecules of ammonium bisulfate, 1 molecule of sulfuric acid, and 1 molecule of water.

8. A base product fluid comprising a molecular cluster compound which is a combination of ammonium sulfate, ammonium bisulfate, sulfuric acid, and water; wherein the molecular cluster compound consists of a mass percentage of hydrogen between about 3% and 6%, a mass percentage of nitrogen between about 10% and about 15%, a mass percentage of sulfur between about 25% and about 30%, and a mass percentage of oxygen between about 52% and about 60%.

9. The base product fluid of claim 8 , wherein the molecular cluster compound consists of a mass percentage of hydrogen between about 4% and 5%, a mass percentage of nitrogen between about 11% and about 15%, a mass percentage of sulfur between about 26% and about 28%, and a mass percentage of oxygen between about 53% and about 57%.

10. The base product fluid of claim 9 , wherein the molecular cluster compound consists of a mass percentage of hydrogen of about 4.7%, a mass percentage of nitrogen of about 14.8%, a mass percentage of sulfur of about 26.5%, and a mass percentage of oxygen of about 54%.

11. The base product fluid of claim 8 , wherein the molecular cluster compound is a chelating agent.

Assignments (4)
SECURITY INTEREST Recorded Sep 3, 2026
From: SEPRO CORPORATION
To: VARAGON CAPITAL PARTNERS AGENT, LLC, AS ADMINISTRATIVE AGENT
Reel/Frame 075890/0044 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 4, 2026
From: EARTH SCIENCE LABORATORIES, INC.
To: SEPRO CORPORATION
Reel/Frame 074852/0166 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE'S NAME INSIDE THE ASSIGNMENT DOCUMENT AND ON THE COVER SHEET PREVIOUSLY RECORDED AT REEL: 045071 FRAME: 0418. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Aug 4, 2021
From: NICHOLAS, DAVID; BOWMAN, REID HENRY; SINGLETON, FREDDIE L.
To: EARTH SCIENCE LABORATORIES, INC.
Reel/Frame 057138/0920 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 1, 2018
From: NICHOLAS, DAVID; BOWMAN, REID HENRY; SINGLETON, FREDDIE L.
To: EARTH SCIENCE LABORATORIES
Reel/Frame 045071/0418 →
Continuity (3)
Continuation 15184523 · Jun 16, 2016
Provisional Application 62182191 · Jun 19, 2015
Related Publication 20180186668A1 · Jul 5, 2018