IP Library › Granted Patent US 10,544,240
Granted Patent B2
US 10,544,240 · App. 15/778,985 · Granted Jan 28, 2020

Ethylene polymer, stretched molded article, microporous membrane and fiber

Inventor: Kenya Tanaka (Tokyo, JP)
Assignee: Asahi Kasei Kabushiki Kaisha
C08F10/02C08J9/00B29C55/12B29K2023/0658B29K2995/004B29K2995/0063B29K2995/0088B29L2031/755
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Quick Facts
Patent No.
US 10,544,240
App. No.
15/778,985
Granted
Jan 28, 2020
Kind
B2
Abstract

The present invention provides an ethylene polymer having a viscosity average molecular weight of 100×10 4 or more and 1,000×10 4 or less, in which a ratio between an isothermal crystallization time at 125° C. and an isothermal crystallization time at 123° C. obtained under specific isothermal crystallization time measurement conditions is 3.5 or more and 10.0 or less, and a degree of crystallization obtained using a differential scanning calorimeter (DSC) is 40% or more and 75% or less.

Claims (21)

1. An ethylene polymer, having a viscosity average molecular weight of 100×10 4 or more and 1,000×10 4 or less,

wherein a ratio between an isothermal crystallization time at 125° C. and an isothermal crystallization time at 123° C. obtained under isothermal crystallization time measurement conditions is 3.5 or more and 10.0 or less,

a degree of crystallization obtained using a differential scanning calorimeter (DSC) is 40.0% or more and 75.0% or less, and

said isothermal crystallization time measurement conditions are

1) a temperature is held at 50° C. for 1 minute, and then increased to 180° C. at a temperature increase rate of 200° C./min;

2) the temperature is held at 180° C. for 5 minutes, and then decreased to 122° C. at a temperature decrease rate of 80° C./min;

3) the temperature is held at 122° C. for 5 minutes, and then increased to 180° C. at a temperature increase rate of 200° C./min;

4) the temperature is held at 180° C. for 5 minutes, and then decreased to 123° C. at a temperature decrease rate of 80° C./min;

5) the temperature is held at 123° C. for 10 minutes, and then increased to 180° C. at a temperature increase rate of 200° C./min, wherein the isothermal crystallization time at 123° C. is measured, assuming that a time of reaching 123° C. is a point of origin, 0 min;

6) the temperature is held at 180° C. for 5 minutes, and then decreased to 124° C. at a temperature decrease rate of 80° C./min;

7) the temperature is held at 124° C. for 15 minutes, and then increased to 180° C. at a temperature increase rate of 200° C./min;

8) the temperature is held at 180° C. for 5 minutes, and then decreased to 125° C. at a temperature decrease rate of 80° C./min; and

9) the temperature is held at 125° C. for 30 minutes, and then increased to 180° C. at a temperature increase rate of 200° C./min, wherein the isothermal crystallization time at 125° C. is measured, assuming that a time of reaching 125° C. is a point of origin, 0 min.

2. The ethylene polymer according to claim 1 , wherein a difference between a melting point at a first melting peak (Tm1) and a melting point at a second melting peak (Tm2) obtained using the differential scanning calorimeter (DSC) is 0° C. or more and less than 10° C.

3. The ethylene polymer according to claim 1 , wherein a difference between a melting start temperature at a first melting peak and a melting start temperature at a second melting peak obtained using the differential scanning calorimeter (DSC) is 5.0° C. or more.

4. The ethylene polymer according to claim 1 , wherein a total content of Ti and Al is 1.0 ppm or more and 30.0 ppm or less.

5. The ethylene polymer according to claim 1 , wherein a content of chlorine is 30 ppm or less.

6. The ethylene polymer according to claim 1 , wherein a total content of hydrocarbon components respectively having 16 and 18 carbon atoms extracted with hexane is 200 ppm or less.

7. A stretched molded article, comprising the ethylene polymer according to claim 1 .

8. A microporous membrane, comprising the ethylene polymer according to claim 1 .

9. A fiber, comprising the ethylene polymer according to claim 1 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 21, 2018
From: TANAKA, KENYA
To: ASAHI KASEI KABUSHIKI KAISHA
Reel/Frame 046637/0946 →
Priority Claims (1)
JP 2017-018676 · Feb 3, 2017 · national
Continuity (1)
Related Publication 20190359740A1 · Nov 28, 2019
Cited By (1)
US 12,454,609