IP Library Granted Patent US 10,680,189
Granted Patent B2
US 10,680,189 · App. 15/989,854 · Granted Jun 9, 2020

Materials for organic light emitting diodes

Inventors: Chuanjun Xia (Lawrenceville, NJ); Bin Ma (Plainsboro, NJ); David Zenan Li (Princeton, NJ); Bert Alleyne (Newtown, PA); Alan DeAngelis (Pennington, NJ); James Fiordeliso (Yardley, PA); Vadim Adamovich (Yardley, PA)
Assignee: UNIVERSAL DISPLAY CORPORATION
H01L51/0085C07F15/0033
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Quick Facts
Patent No.
US 10,680,189
App. No.
15/989,854
Granted
Jun 9, 2020
Kind
B2
Abstract

Compounds are provided that comprise a ligand having a 5-substituted 2-phenylquinoline. In particular, the 2-phenylquinoline may be substituted with a cycloalkyl containing group at the 5-position. These compounds may be used in organic light emitting devices, in particular as red emitters in the emissive layer of such devices, to provide devices having improved properties.

Claims (40)

1. A compound comprising a ligand L having the formula:

wherein each of R 5 , R 6 , and R 7 is independently selected from the group consisting of hydrogen, deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl;

wherein R 4 is selected from the group consisting of isopropyl, isobutyl, and t-butyl; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

2. The compound of claim 1 , wherein M is Ir.

3. The compound of claim 1 , wherein the compound has the formula Ir(L) m (L′) 3-m

wherein L′ is an ancillary ligand; and

wherein m is 1, 2, or 3.

4. The compound of claim 3 , wherein L′ is a monoanionic bidentate ligand.

5. The compound of claim 3 , wherein the compound has the formula

and

wherein R 1 , R 2 , and R 3 are independently selected from the group consisting of hydrogen, deuterium, alkyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl.

6. The compound of claim 5 , wherein each of R 1 and R 3 are a branched alkyl with branching at a position further than the α position to the carbonyl group.

7. The compound of claim 5 , wherein each of R 5 , R 6 and R 7 are independently selected from methyl and hydrogen, and at least one of R 5 , R 6 and R 7 is methyl.

8. The compound of claim 5 , wherein each of R 5 and R 7 is methyl, and R 6 is hydrogen.

9. The compound of claim 5 , wherein each of R 5 and R 6 is methyl, and R 7 is hydrogen.

10. The compound of claim 5 , wherein each of R 5 , R 6 and R 7 is methyl.

11. The compound of claim 1 , wherein R 4 is isopropyl.

12. The compound of claim 1 , wherein R 4 is isobutyl.

13. The compound of claim 1 , wherein R 4 is t-butyl.

14. The compound of claim 1 , wherein the compound is selected from the group consisting of:

15. The compound of claim 1 , wherein the compound is selected from the group consisting of:

16. The compound of claim 1 , wherein the compound is selected from the group consisting of:

17. A first device comprising an organic light emitting device, comprising:

an anode;

a cathode; and

an organic layer, disposed between the anode and the cathode, comprising a compound comprising a ligand L having the formula:

wherein each of R 5 , R 6 , and R 7 is independently selected from the group consisting of hydrogen, deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl;

wherein R 4 is selected from the group consisting of isopropyl, isobutyl, and t-butyl; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

18. The first device of claim 17 , wherein the organic layer is an emissive layer and the compound is an emissive dopant.

19. The first device of claim 18 , wherein the organic layer further comprises a host.

20. A consumer product comprising an organic light emitting device, comprising:

an anode;

a cathode; and

an organic layer, disposed between the anode and the cathode, comprising a compound comprising a ligand L having the formula:

wherein each of R 5 , R 6 , and R 7 is independently selected from the group consisting of hydrogen, deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl;

wherein R 4 is selected from the group consisting of isopropyl, isobutyl, and t-butyl; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

21. The consumer product of claim 20 , wherein the consumer product is selected from the group consisting of a flat panel display, a computer monitor, a television, a billboard, lights for interior or exterior illumination and/or signaling, a heads up display, a fully transparent display, a flexible display, a laser printer, a telephone, a cell phone, a personal digital assistant (PDA), a laptop computer, a digital camera, a camcorder, a viewfinder, a micro-display, a vehicle, an area wall, theater or stadium screen, or a sign.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 29, 2018
From: XIA, CHUANJUN; MA, BIN; LI, DAVDI ZENAN; ALLEYNE, BERT; DEANGELIS, ALAN; FIORDELISO, JAMES; ADAMOVICH, VADIM
To: UNIVERSAL DISPLAY CORPORATION
Reel/Frame 045923/0207 →
Continuity (3)
Continuation 13932546 · Jul 1, 2013
Continuation In Part 13006016 · Jan 13, 2011
Related Publication 20180277775A1 · Sep 27, 2018
Cited By (2)
US 12,495,662 US 12,622,128