IP Library Granted Patent US 11,773,333
Granted Patent B2
US 11,773,333 · App. 15/908,944 · Granted Oct 3, 2023

Zeolitic catalytic conversion of alcohols to hydrocarbons

Inventors: Chaitanya K. Narula (Knoxville, TN); Brian H. Davison (Knoxville, TN); Martin Keller (Knoxville, TN)
Assignee: UT-BATTELLE, LLC
C10G3/49B01J29/061B01J29/072B01J29/076B01J29/46B01J29/48B01J35/023B01J35/04B01J37/0246C07C1/22C10G3/45C12P7/06C12P7/08C12P7/10C12P7/16B01J29/143B01J29/146B01J29/163B01J29/166B01J29/68B01J29/69B01J29/7615B01J29/7661B01J29/7669B01J29/7692B01J29/7815B01J29/7861B01J29/7869B01J29/7892B01J2229/183B01J2229/186C10G2300/1011C10G2300/1014C10G2300/4006C10G2400/02C10G2400/04C10G2400/08Y02E50/10Y02P30/20
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Quick Facts
Patent No.
US 11,773,333
App. No.
15/908,944
Granted
Oct 3, 2023
Kind
B2
Abstract

A method for converting an alcohol to a hydrocarbon, the method comprising contacting said alcohol with a metal-loaded zeolite catalyst at a temperature of at least 100° C. and up to 550° C., wherein said alcohol can be produced by a fermentation process, said metal is a positively-charged metal ion, and said metal-loaded zeolite catalyst is catalytically active for converting said alcohol to said hydrocarbon.

Claims (19)

1. A method for converting ethanol in an aqueous solution in a concentration of no more than about 20% (vol/vol) to a product comprising aromatic hydrocarbons, the method comprising contacting said ethanol in aqueous solution with a gallium or indium loaded ZSM-5 zeolite catalyst at a temperature of 300° C. to 550° C. and pressure of 1-5 atm to convert said ethanol into said product comprising aromatic hydrocarbons, wherein a combined concentration of alcohols in said aqueous solution is no more than about 20% (vol/vol).

2. The method of claim 1 , wherein said combined concentration of alcohols is no more than about 10% (vol/vol).

3. The method of claim 1 , wherein said ethanol is produced by a fermentation process.

4. The method of claim 3 , wherein said ethanol is a component of a fermentation stream when contacted with said gallium or indium loaded ZSM-5 zeolite catalyst.

5. The method of claim 3 , wherein said fermentation process produces said ethanol from a biomass source.

6. The method of claim 5 , wherein said biomass source is comprised of lignocellulosic matter.

7. The method of claim 3 , wherein said fermentation process produces said ethanol from a plant-based source of sugars.

8. The method of claim 1 , wherein said temperature is at least 350° C. and up to 550° C.

9. The method of claim 1 , wherein said temperature is at least 400° C. and up to 550° C.

10. The method of claim 1 , wherein said aromatic hydrocarbon is a mixture of hydrocarbon compounds, wherein said mixture is useful as a fuel or as a blendstock component of a fuel.

11. The method of claim 10 , wherein said mixture of hydrocarbon compounds substantially corresponds to a petrochemical fraction.

12. The method of claim 11 , wherein said petrochemical fraction substantially corresponds to a fuel selected from gasoline, kerosene, diesel, and jet propellant.

13. The method of claim 11 , wherein said method further comprises distilling said mixture of hydrocarbon compounds to obtain a fraction of said mixture of hydrocarbon compounds.

14. The method of claim 1 , wherein said method is integrated with a fermentation process, wherein said fermentation process produces said ethanol as a component of a fermentation stream, and said fermentation stream is contacted with said gallium or indium loaded ZSM-5 zeolite catalyst.

15. The method of claim 1 , wherein said method is integrated with a biomass reactor that includes a fermentation process, wherein said fermentation process produces said ethanol as a component of a fermentation stream, and said fermentation stream is contacted with said gallium or indium loaded ZSM-5 zeolite catalyst.

16. The method of claim 1 , wherein said ethanol is produced from a biomass source.

17. The method of claim 16 , wherein said biomass source is comprised of lignocellulosic matter.

18. The method of claim 16 , wherein said biomass source is comprised of starch or sugar.

19. The method of claim 1 , wherein the aqueous solution of ethanol is passed through a boiler configured to retain solids prior to transfer to the gallium or indium loaded ZSM-5 zeolite catalyst.

Continuity (5)
Continuation 15357039 · Nov 21, 2016
Continuation 14293248 · Jun 2, 2014
Continuation 14123363
Provisional Application 61497256 · Jun 15, 2011
Related Publication 20180187091A1 · Jul 5, 2018