IP Library Granted Patent US 11,997,918
Granted Patent B2
US 11,997,918 · App. 17/745,547 · Granted May 28, 2024

Organic electroluminescent materials and devices

Inventors: Chuanjun Xia (Lawrenceville, NJ); Bin Ma (Plainsboro, NJ); David Zenan Li (Princeton, NJ); Bert Alleyne (Newtown, PA); Alan Deangelis (Pennington, NJ); James Fiordeliso (Yardley, PA); Vadim Adamovich (Yardley, PA)
Assignee: UNIVERSAL DISPLAY CORPORATION
H10K85/342C07F15/0033
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Quick Facts
Patent No.
US 11,997,918
App. No.
17/745,547
Granted
May 28, 2024
Kind
B2
Abstract

Compounds are provided that comprise a ligand having a 5-substituted 2-phenylquinoline. In particular, the 2-phenylquinoline may be substituted with a cycloalkyl containing group at the 5-position. These compounds may be used in organic light emitting devices, in particular as red emitters in the emissive layer of such devices, to provide devices having improved properties.

Claims (52)

1. A compound comprising a ligand L having the formula:

wherein A is a 5-membered or 6-membered carbocyclic or heterocyclic ring;

wherein R A can represent tri or tetra substitutions;

wherein each of R A is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylalkyl, aryl and heteroaryl;

wherein at least one R A is a substituent other than alkyl or aryl;

wherein R B is alkyl having at least 2 carbon atoms; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

2. The compound of claim 1 , wherein A is phenyl.

3. The compound of claim 1 , wherein M is Ir.

4. The compound of claim 1 , wherein at least one R A is selected from the group consisting of silyl, alkoxy, amino, alkenyl, alkynyl, or heteroaryl.

5. The compound of claim 1 , wherein at least one R A is silyl or amino.

6. The compound of claim 1 , wherein the compound has the formula:

wherein L′ is an ancillary ligand; and

wherein m is 1, 2, or 3.

7. The compound of claim 6 , wherein L′ is a monoanionic bidentate ligand.

8. The compound of claim 6 , wherein L′ is

and wherein each of R 1 , R 2 , and R 3 is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, alkoxy, amino, alkenyl, alkynyl, arylalkyl, aryl and heteroaryl.

9. The compound of claim 6 , wherein the compound has the formula:

wherein each R 1 , R 2 , and R 3 is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl;

wherein each R 5 , R 6 , and R 7 is independently selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylalkyl, aryl and heteroaryl;

wherein R 4 is alkyl having at least 2 carbon atoms;

wherein at least one of R 5 , R 6 , or R 7 is not alkyl or aryl; and

wherein m is 1, 2, or 3.

10. The compound of claim 9 , wherein each of R 1 and R 3 is a branched alkyl with branching at a position further than the α position to the carbonyl group.

11. The compound of claim 9 , wherein at least one of R 5 , R 6 and R 7 is methyl.

12. The compound of claim 9 , wherein each of R 5 and R 7 is methyl.

13. The compound of claim 9 , wherein each of R 5 and R 6 is methyl.

14. The compound of claim 9 , wherein at least one of R 5 , R 6 and R 7 is not selected from the group consisting of deuterium, alkyl, and aryl.

15. The compound of claim 1 , wherein R B is an alkyl group having at least 4 carbon atoms.

16. The compound of claim 1 , wherein R B is an alkyl group having at least 3 carbon atoms.

17. A first device comprising an organic light emitting device, comprising:

an anode;

a cathode; and

an organic layer, disposed between the anode and the cathode, comprising a compound comprising a ligand L having the formula:

wherein A is a 5-membered or 6-membered carbocyclic or heterocyclic ring;

wherein R A can represent tri or tetra substitutions;

wherein each of R A is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylalkyl, aryl and heteroaryl;

wherein at least one R A is a substituent other than alkyl or aryl;

wherein R B is alkyl having at least 2 carbon atoms; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

18. The first device of claim 17 , wherein the organic layer is an emissive layer and the compound is an emissive dopant.

19. A consumer product comprising an organic light emitting device, comprising:

an anode;

a cathode; and

an organic layer, disposed between the anode and the cathode, comprising a compound comprising a ligand L having the formula:

wherein A is a 5-membered or 6-membered carbocyclic or heterocyclic ring;

wherein R A can represent tri or tetra substitutions;

wherein each of R A is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylalkyl, aryl and heteroaryl;

wherein at least one R A is a substituent other than alkyl or aryl;

wherein R B is alkyl having at least 2 carbon atoms; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

20. The consumer product of claim 19 , wherein the consumer product is one of a flat panel display, a computer monitor, a television, a billboard, a light for interior or exterior illumination and/or signaling, a heads up display, a fully transparent display, a flexible display, a laser printer, a telephone, a cell phone, a personal digital assistant (PDA), a laptop computer, a digital camera, a camcorder, a viewfinder, a vehicle, a wall, theater or stadium screen, and a sign.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 16, 2022
From: XIA, CHUANJUN; MA, BIN; LI, DAVID ZENAN; ALLEYNE, BERT; DEANGELIS, ALAN; FIORDELISO, JAMES; ADAMOVICH, VADIM
To: UNIVERSAL DISPLAY CORPORATION
Reel/Frame 059921/0993 →
Continuity (5)
Continuation 16861655 · Apr 29, 2020
Continuation 15989854 · May 25, 2018
Continuation 13932546 · Jul 1, 2013
Continuation In Part 13006016 · Jan 13, 2011
Related Publication 20220285632A1 · Sep 8, 2022