IP Library Granted Patent US 12,187,621
Granted Patent B2
US 12,187,621 · App. 17/409,893 · Granted Jan 7, 2025

Sustainable calcium hydroxide production for green cement

Inventors: Bu Wang (Madison, WI); Raghavendra Ragipani (Madison, WI); Robert Phillip Anex (Madison, WI); Thatcher Wiley Root (Madison, WI)
Assignee: Wisconsin Alumni Research Foundation
C01F11/12C04B7/424C04B2103/001
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Quick Facts
Patent No.
US 12,187,621
App. No.
17/409,893
Granted
Jan 7, 2025
Kind
B2
Abstract

A method of making a composition of matter comprising calcium hydroxide. The method includes the steps of contacting a calcium-containing molecule with an aqueous solution of a water-soluble salt having ammonium cation and a counter-anion, under conditions effective to yield a compound containing calcium and the counter-anion; and reacting the compound comprising calcium and the counter-anion with ammonia and water under conditions to yield calcium hydroxide.

Claims (7)

1. A method of making a composition of matter comprising calcium hydroxide, the method comprising:

(a) contacting a feedstock comprising a material selected from the group consisting of crystalline, amorphous, or hydrated phases of calcium silicate, calcium aluminate, calcium aluminosilicate, and combinations thereof with an aqueous solution comprising a water-soluble salt comprising ammonium cation and a counter-anion, for a time, and at a temperature, pH, and pressure effective to yield a compound comprising calcium and the counter-anion; and

(b) reacting at least a portion of the compound comprising calcium and the counter-anion with ammonia and water for a time, and at a temperature, pH, and pressure effective to yield calcium hydroxide.

2. The method of claim 1 , wherein the water-soluble salt comprising ammonium cation and a counter-anion is selected from the group consisting of ammonium halide, ammonium acetate, ammonium phosphate, ammonium oxalate, and ammonium lactate.

3. The method of claim 1 , wherein the water-soluble salt comprising ammonium cation and a counter-anion is ammonium chloride or ammonium acetate.

4. The method of claim 1 , wherein step (b) yields calcium hydroxide and ammonium halide and further comprising:

(c) recycling at least a portion of the ammonium halide formed in step (b) and using it as the water-soluble salt comprising ammonium cation and a counter-anion.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2023
From: ANEX, ROBERT; WANG, BU; RAGIPANI, RAGHAVENDRA; ROOT, THATCHER
To: WISCONSIN ALUMNI RESEARCH FOUNDATION
Reel/Frame 063461/0496 →
CONFIRMATORY LICENSE Recorded Oct 14, 2021
From: UNIVERSITY OF WISCONSIN-MADISON
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 057813/0664 →
Continuity (2)
Provisional Application 63069936 · Aug 25, 2020
Related Publication 20220081311A1 · Mar 17, 2022
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