IP Library Granted Patent US 12,257,629
Granted Patent B2
US 12,257,629 · App. 17/315,607 · Granted Mar 25, 2025

Apparatus and methods for sintering

Inventors: Kurt Heikkila (Marine on the Saint Croix, MN); Rodney Williams (Stacy, MN)
Assignee: Tundra Compoistes, LLC
B22F3/003F27B9/36F27B21/00F27D11/06F27D11/12B33Y40/20F27D2099/0015F27D2099/0028
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Quick Facts
Patent No.
US 12,257,629
App. No.
17/315,607
Granted
Mar 25, 2025
Kind
B2
Abstract

Disclosed is an apparatus and methods for sintering particulate to make a workpiece.

Claims (15)

1. A furnace for sintering a workpiece, the furnace comprising:

a) at least one inductor coil;

b) at least one hollow cylindrical susceptor enclosing a process tube and an infrared heating zone containing a reducing atmosphere, the susceptor comprising a material capable of absorbing electromagnetic energy from the coil to generate radiant infrared heat and to shield the heating zone from incident RF heat;

c) at least one insulating layer surrounding the susceptor; and

d) a supply of power for said coil;

wherein the process tube in the furnace is horizontally configured to maintain a flow of the reducing atmosphere to aid in sintering and remove volatiles from the furnace; the inductor coils are energized sufficiently to progressively raise the temperature of the susceptor to heat the heating zone by radiant infrared heat to an effective temperature of 800 to 1500° C. and the sintering temperature within the heating zone comprises a uniform heat distribution.

2. The furnace of claim 1 wherein the incident RF heating mechanism is a current induced in the susceptor producing IR heating in the substantial absence of an eddy current heating in the workpiece.

3. The furnace of claim 1 wherein the susceptor cylinder has a wall thickness of 0.5 to 2 centimeters.

4. The furnace of claim 3 wherein the ratio of the outside diameter of the susceptor to the susceptor wall thickness is greater than 4 but less than 12.

5. The furnace of claim 1 wherein the heating of the heat zone is by infrared heat and not by a current induced by radio frequency energy.

6. The furnace of claim 1 wherein the furnace has a construction consisting essentially of the inductor coil, the insulation layer, the susceptor and the process tube with heating zone therein.

7. The furnace of claim 6 wherein the insulating layer is a ceramic insulator.

8. The furnace of claim 1 wherein the coil is water cooled.

9. The furnace of claim 1 wherein the process tube comprises a silicon carbide coating.

10. The furnace of claim 1 wherein the susceptor comprises graphite.

Continuity (2)
Provisional Application 62959168 · Jan 9, 2020
Related Publication 20230234127A1 · Jul 27, 2023
References Cited (65)
US 3656910A · Ferment · 1972 [cited by applicant]
US 3680625A · Hein et al. · 1972 [cited by applicant]
US 3696223A · Metcalf et al. · 1972 [cited by applicant]
US 3739067A · Stahr et al. · 1973 [cited by applicant]
US 4174462A · Pearce · 1979 [cited by applicant]
US 4231796A · Clark et al. · 1980 [cited by applicant]
US 4263336A · Thompson et al. · 1981 [cited by applicant]
US 4608473A · Paek · 1986 [cited by examiner]
US 4720615A · Dunn · 1988 [cited by applicant]
US 4741748A · Lane et al. · 1988 [cited by applicant]
US 4818833A · Formanack et al. · 1989 [cited by applicant]
US 5072087A · Apte et al. · 1991 [cited by applicant]
US 5157232A · Pfaffmann · 1992 [cited by applicant]
US 5198489A · Sterzel et al. · 1993 [cited by applicant]
US 5502743A · Conochie et al. · 1996 [cited by applicant]
US 5641920A · Hens et al. · 1997 [cited by applicant]
US 5713979A · Nicholson · 1998 [cited by examiner]
US 5808282A · Apte et al. · 1998 [cited by applicant]
US 5860055A · Hesse et al. · 1999 [cited by applicant]
US 6271509B1 · Dalton · 2001 [cited by applicant]
US 6361597B1 · Takase et al. · 2002 [cited by applicant]
US 6528771B1 · Matsen et al. · 2003 [cited by applicant]
US 6724803B2 · Miller et al. · 2004 [cited by applicant]
US 7110430B2 · Lazor · 2006 [cited by applicant]
US 7113535B2 · Tenzek et al. · 2006 [cited by applicant]
US 7153594B2 · Kejzelman et al. · 2006 [cited by applicant]
US 7625420B1 · Kodas et al. · 2009 [cited by applicant]
US 8236420B2 · Skarman et al. · 2012 [cited by applicant]
US 8247249B2 · Strittmatter · 2012 [cited by examiner]
US 9364775B2 · Chamyvelumani et al. · 2016 [cited by applicant]
US 9457403B2 · Holcomb · 2016 [cited by applicant]
US 10273567B2 · Isaac · 2019 [cited by applicant]
US 20010045426A1 · Eberhardt et al. · 2001 [cited by applicant]
US 20020148829A1 · Fishman · 2002 [cited by applicant]
US 20060193978A1 · Toth · 2006 [cited by applicant]
US 20080267251A1 · Gerszewski et al. · 2008 [cited by applicant]
US 20100282166A1 · Fukuda · 2010 [cited by examiner]
US 20110068700A1 · Fan · 2011 [cited by applicant]
US 20110168700A1 · Ripley · 2011 [cited by applicant]
US 20120104665A1 · ter Maat et al. · 2012 [cited by applicant]
US 20170175234A1 · Jennett · 2017 [cited by examiner]
US 20180051931A1 · Fornoff et al. · 2018 [cited by applicant]
US 20180104740A1 · Yamamoto et al. · 2018 [cited by applicant]
US 20180117676A1 · Lindroos et al. · 2018 [cited by applicant]
US 20200292235A1 · Hauptmann · 2020 [cited by applicant]
DE 2630819A1 · 1977 [cited by applicant]
EP 0640060A1 · 1995 [cited by applicant]
EP 640060B1 · 1996 [cited by applicant]
EP 0743289A1 · 1996 [cited by applicant]
EP 2993434A1 · 2016 [cited by applicant]
WO 9311655A1 · 1993 [cited by applicant]
WO 9631090A1 · 1996 [cited by applicant]
WO 2005046290A1 · 2005 [cited by applicant]
WO 2016177935A1 · 2016 [cited by applicant]
WO 2018098435A1 · 2018 [cited by applicant]
Capus Joesph, M. et al., Sintering, Advances in Powder Metallurgy and Particulate Materials, 1992, vol. 3, pp. 1-14, Metal Powder Industries Federation, Princeton, NJ, USA. [cited by applicant]
Capus, Joesph, The New Benefits of Binder Lubricants, pp. 11-12, Nov./Dec. 2011, metal-powder.net, Elsevier Ltd. [cited by applicant]
Catamold Feedstock for Metal Injection Molding: Processing—Properties—Applications, Technical Information BASF AG, May 2003, pp. 1-13, BASF AG. [cited by applicant]
Fox, Richard T., Optimization of Metal Injection Molding Experimental Design, The International Journal of Powder Metallurgy, 1990, pp. 233-243, vol. 26, No. 3. [cited by applicant]
German, R.M., Prediction of Sintered Density for Bimodal Powder Mixtures, May 1992, pp. 1455-1465, vol. 23A. [cited by applicant]
German, Randall, M., The Role of Particle Packing Density in Powder Injection Molding, Reviews of Powder Metallurgy and Physical Ceramics pp. 81-110, 5, Elsevier, England, May 1992. [cited by applicant]
Gonzalez-Gutierrez, Joamin et. al., Powder INjection Molding of Metal and Ceramic Parts, Center for Experimental Mechanics, pp. 65-88, University of Ljubljana, Ljubljana, Slovenia, Mar. 2008. [cited by applicant]
Nakamura Hidefumi et al., Effect of a slight addition of Zr on the sintering behaviour of water-atomised 316L stainless steel powder, Mar. 2011, pp. 60-67, vol. 5 No. 1, Powder Injection Moulding International. [cited by applicant]
Tudbury Chester A., Basics of Induction Heating,, 1960, 1-132, vol. 1, Pillar Induction, Brookfield, WI, USA. [cited by applicant]
Yih, Pay et al., Powder Metallurgy Fabrication OF Metal Matrix Composites Using Coated Fillers, International Journal of Powder Metallurgy, 1995, pp. 335-340, vol. 31, No. 4. [cited by applicant]