IP Library Granted Patent US 12,339,073
Granted Patent B2
US 12,339,073 · App. 18/282,244 · Granted Jun 24, 2025

Method for monitoring a tube sheet of a heat exchanger

Inventors: Michael S. DeCourcy (King of Prussia, PA); Kishlay Tripathy (King of Prussia, PA)
Assignee: Arkema Inc.
F28F27/00F28D7/16F28D2021/0054F28F2200/00
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,339,073
App. No.
18/282,244
Granted
Jun 24, 2025
Kind
B2
Abstract

Shell-and-tube devices typically require regular maintenance. Described herein is an automated method for tracking the status of individual tubes during maintenance activities and recording status data for review and analysis. Status data may optionally be reported in real-time summary format and/or used to predict time-to-completion. The method minimizes omission errors and helps to reduce the expense of performing maintenance activities in shell-and-tube devices, including shell-and-tube reactors and heat exchangers.

Claims (52)

1. A method for monitoring a status of a shell and tube device during a particulate catalyst loading activity, the shell and tube device comprising a tube sheet comprising a plurality of tube ends arranged in a fixed pattern of rows (R) and columns (C), said method comprising the steps of:

a) placing a plurality of plugging plates on said tube sheet such that all of the plurality of tube ends are covered, each of the plurality of plugging plates comprising a disk recess for installing a colored indicator disk,

b) assigning a unique identifier to each of said plurality of plugging plates,

c) installing a plurality of colored indicator disks in the disk recesses, said plurality of colored indicator disks including at least one disk having a first color and at least one disk having a second color that is different than the first color,

d) positioning at least one digital camera such that at least a portion of the plurality of plugging plates lie within a field of view of the at least one digital camera,

e) acquiring an initial digital image (Di) of at least the portion of the plurality of plugging plates at an initial acquisition time (Ti),

f) determining an initial color of each of the plurality of colored indicator disks within said initial digital image (Di), and

g) creating an initial data record in a relational database for each of the plurality of plugging plates within said initial digital image (Di), said data record including:

i. the initial acquisition time (Ti),

ii. the unique identifier for the plugging plate, and

iii. the initial color for the colored disk at the initial acquisition time (Ti).

2. The method of claim 1 , wherein the unique identifier assigned to each of said plurality of tube ends is a set of Cartesian coordinates of the form (row, column).

3. The method of claim 1 , wherein steps e) through g) are performed multiple times.

4. The method of claim 1 further comprising illuminating the tube sheet with at least one light source that emits wavelengths of light within a visible light spectrum, an infrared spectrum, or an ultraviolet UV spectrum.

5. The method of claim 1 , wherein the at least one digital camera detects wavelengths of light selected from one or more of the visible light spectrum, the infrared spectrum, or the ultraviolet (UV) spectrum.

6. The method of claim 1 , wherein said tube sheet forms part of a heat exchanger, and said heat exchanger is one of a condenser, reboiler, preheater, boiler, superheater, quench exchanger, Transfer Line Exchanger (TLE), evaporator, waste heat boiler, recuperator, cross-exchanger and process heater.

7. The method of claim 1 , wherein said tube sheet forms part of a reaction system for producing either Hydrogen Cyanide or Nitrogen Oxides.

8. The method of claim 1 , wherein said tube sheet forms part of a nuclear power reactor.

9. The method of claim 1 further comprising the step of using at least a portion of the data recorded in the relational database to produce one or more of tables, graphs, spreadsheets, and color-coded summary graphics.

10. The method of claim 1 , wherein said shell and tube device is utilized to perform a chemical conversion, said chemical conversion selected from the group consisting of:

i. conversion of propylene to acrolein and/or acrylic acid;

ii. conversion of propane to acrolein and/or acrylic acid;

iii. conversion of glycerol to acrolein and/or acrylic acid;

iv. conversion of tert-butanol, isobutene, isobutane, isobutyraldehyde, isobutyric acid, or methyl tert-butyl ether to methacrolein and/or methacrylic acid;

V. conversion of acrolein to acrylic acid;

vi. conversion of methacrolein to methacrylic acid;

vii. conversion of o-xylene or naphthalene to phthalic anhydride;

viii. conversion of butadiene to maleic anhydride;

ix. conversion of n-butane to maleic anhydride;

X. conversion of indanes to anthraquinone;

xi. conversion of ethylene to ethylene oxide; and

xii. conversion of propylene to propylene oxide.

11. The method of claim 1 , wherein said shell and tube device is utilized to perform the oxychlorination of ethylene to 1,2-dichloroethane (EDC).

12. The method of claim 1 , further comprising the step of using one or more data records stored in the relational database to produce one or more of tables, graphs, spreadsheets, and color-coded summary graphics.

13. The method of claim 1 , further comprising the step of producing performance metrics for the maintenance activity, wherein the producing step comprises calculating and displaying the performance metrics in a table, graph, spreadsheet, or color-coded summary graphic.

14. The method of claim 1 , further comprising predicting time-to-completion of the maintenance activity.

15. The method of claim 1 , further comprising:

h) installing and/or removing a colored indicator disk on the one or more disk recesses,

i) acquiring a later digital image (Dx) of at least a portion of the plurality of plugging plates at a later acquisition time (Tx), wherein Tx>Ti,

j) determining the later color of each of the colored indicator disks within said later digital image (Dx),

k) creating a later data record in the relational database for each plugging plate within said later digital image (Dx), said later data record including:

i. the later acquisition time (Tx),

ii. the unique identifier for the plugging plate, and

iii. the later color for the colored indicator disk at later acquisition time (Tx), and

l. Repeating steps h) through k) until said catalyst loading activity is complete.

16. The method of claim 1 , wherein said shell-and-tube device is a shell-and-tube reactor, a tandem reactor, a single tube reactor, or a single-shell open interstage (SSOI) reactor.

17. The method of claim 15 , further comprising producing one or more of tables, graphs, spreadsheets, and color-coded summary graphics using one or more of the data records stored in the relational database.

18. The method of claim 15 , further comprising predicting a time-to-completion for the catalyst loading activity.

19. The method of claim 1 , further comprising the steps of:

measuring one or more workspace parameters,

recording workspace parameter measurements in the relational database, and

optionally, presenting said workspace parameter measurements on a visual display.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 25, 2023
From: DECOURCY, MICHAEL S.; TRIPATHY, KISHLAY
To: ARKEMA INC.
Reel/Frame 065009/0076 →
Continuity (2)
Provisional Application 63186931 · May 11, 2021
Related Publication 20240159482A1 · May 16, 2024
References Cited (36)
US 4222540A · King et al. · 1980 [cited by applicant]
US 4977529A · Gregg et al. · 1990 [cited by applicant]
US 6362875B1 · Burkley · 2002 [cited by applicant]
US 6960333B2 · Blanda, Jr. et al. · 2005 [cited by applicant]
US 6981404B2 · Johns et al. · 2006 [cited by applicant]
US 7115776B2 · Hammon et al. · 2006 [cited by applicant]
US 7115777B2 · Allmendinger et al. · 2006 [cited by applicant]
US 8063778B2 · Johns et al. · 2011 [cited by applicant]
US 9440903B2 · Decourcy et al. · 2016 [cited by applicant]
US 10168527B2 · Tripathy · 2019 [cited by applicant]
US 20070087311A1 · Garvey, III et al. · 2007 [cited by applicant]
US 20080045748A1 · Jinno et al. · 2008 [cited by applicant]
US 20090112367A1 · Decourcy et al. · 2009 [cited by applicant]
US 20100063304A1 · Olbert et al. · 2010 [cited by applicant]
US 20100097221A1 · Kreiner et al. · 2010 [cited by applicant]
US 20110144356A1 · Taheri et al. · 2011 [cited by applicant]
US 20120062691A1 · Fowler et al. · 2012 [cited by applicant]
US 20120097378A1 · Gianazza et al. · 2012 [cited by applicant]
US 20140184781A1 · Au et al. · 2014 [cited by applicant]
US 20140290368A1 · Guo et al. · 2014 [cited by applicant]
US 20160046498A1 · Caton et al. · 2016 [cited by applicant]
US 20160220974A1 · Schmidt · 2016 [cited by applicant]
US 20200003503A1 · Colombo et al. · 2020 [cited by applicant]
US 20200068125A1 · Michael et al. · 2020 [cited by applicant]
US 20210065356A1 · Fisher · 2021 [cited by examiner]
US 20210179375A1 · Okumura · 2021 [cited by examiner]
WO WO2009049031A1 · 2009 [cited by applicant]
WO WO2015002451A1 · 2015 [cited by applicant]
WO WO2018232508A1 · 2018 [cited by applicant]
MDPI “Monocular Stero Measurement Using High-Speed Catadioptric Tracking”; Shaopeng Hu et al; Sensors 2017, 17, 1839, doi: 10.3390/s17081839 pp. 1-29. [cited by applicant]
Feb. 2013 Problemy Eksploatacji—Maintenance Problems; “Multi-Mirror System for High-Speed Camera Monitoring Applications”; Garbacz et al; Institute for Sustainable Technologies—National Research Institute, Radom piotr. … [cited by applicant]
Sulzer Chemtech “Falling Film Melt Crystallization-Technology for Production of Glacial Acrylic Acid” ; [email protected]; pp. 1-2. [cited by applicant]
Sulzer Chemtech “Fractional Crystallization” 28.56.06.40-IV06-50; pp. 1-15. [cited by applicant]
The National Academies of Science Engineering Medicine—The National Academies Press; http://nap.edu/12896; “Seeing Photons: Progress and Limits of Visible and Infrared Sensor Arrays (2010)” [Book details 194 Pages ISBN … [cited by applicant]
Density—Product Overview—“The Occupany Analytics Platform for Connected Buildings” pp. 1-18. [cited by applicant]
Applied Industrial Catalysis, vol. 1—Chapter 9 “Oxychlorination of Ethylene”; J.S. Naworski and E.S. Velez pp. 239-273. [cited by applicant]