IP Library Granted Patent US 12,594,539
Granted Patent B2
US 12,594,539 · App. 18/793,533 · Granted Apr 7, 2026

Liquid dispersion compositions, uses and method of making the same

Inventors: Steven Edward Brown (Oak Ridge, NC); Paul Sevier McClellan, Jr. (Hickory, NC); Bradlee Watts Gustavesen (Upton, MA); Jason Randall (Granite Falls, NC)
Assignee: Chase Corporation
B01J20/261B01J20/28026B01J20/3214B01J20/327
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Quick Facts
Patent No.
US 12,594,539
App. No.
18/793,533
Granted
Apr 7, 2026
Kind
B2
Abstract

This disclosure relates to liquid dispersion compositions that are suitable to provide absorbent materials (e.g., an absorbent coating), and methods of preparing the compositions and absorbent materials thereof.

Claims (56)

1 . A liquid dispersion composition comprising a granular superabsorbent polymer dispersed in a liquid medium, wherein:

the granular superabsorbent polymer is present in the composition from about 10% to about 80% by weight; and

the liquid medium comprises at least two liquid components, wherein at least one of the liquid components is insoluble with the other liquid components, and the liquid medium comprises a first liquid component and a second liquid component.

2 . The liquid dispersion composition of claim 1 , wherein the granular superabsorbent polymer comprises an acrylate polymer.

3 . The liquid dispersion composition of any one of claim 1 , wherein the insolubility of the at least one liquid component with the other liquid components is determined by Hansen solubility parameters, wherein the relative energy difference (RED) of the at least one liquid component and the other liquid components is equal to or greater than 1.

4 . The liquid dispersion composition of claim 1 , wherein the first liquid component comprises a silicon-containing liquid, a hydrocarbon liquid, or a fluorocarbon liquid.

5 . The liquid dispersion composition of claim 4 , wherein the silicon-containing liquid comprises a silicone, organo-silicone, silane, siloxane, or organosilane.

6 . The liquid dispersion composition of claim 4 , wherein the hydrocarbon liquid is paraffinic oil or polyisobutene.

7 . The liquid dispersion composition of claim 1 , wherein the second liquid component comprises a surface active agent, a polyol, an ester, an alkylene glycol, water, an alcohol, or a combination thereof.

8 . The liquid dispersion composition of claim 1 , wherein the liquid dispersion composition comprises one or more surface active agents.

9 . The liquid dispersion composition of claim 8 , wherein the liquid dispersion composition comprises at least one surface active agent that is different from the first liquid component and the second liquid component.

10 . The liquid dispersion composition of claim 9 , wherein the at least one surface active agent that is different from the first liquid component or the second liquid component is present in the composition from about 0.01% to about 50% by weight, about 0.1% to about 10% by weight, about 0.1% to about 5% by weight, or about 0.5% to about 2% by weight.

11 . The liquid dispersion composition of claim 8 , wherein at least one of the one or more surface active agents is a polysorbate.

12 . The liquid dispersion composition of claim 1 , further comprising one or more additives.

13 . The liquid dispersion composition of claim 12 , wherein the one or more additives comprise polyethylene glycol.

14 . The liquid dispersion composition of claim 1 , wherein the liquid dispersion composition has a water absorption capacity of at least about 10 grams of water per gram of liquid dispersion composition, at least about 20 grams of water per gram of liquid dispersion composition, or at least about 50 grams of water per gram of liquid dispersion composition.

15 . The liquid dispersion composition of claim 1 , wherein the liquid dispersion composition forms an oil-in-oil emulsion, suspension, oil-in-water emulsion, water-in-oil emulsion, or a combination thereof.

16 . The liquid dispersion composition of claim 15 , wherein the liquid dispersion composition forms a multiphase emulsion.

17 . The liquid dispersion composition of claim 1 , wherein the granular superabsorbent polymer is present in the composition from about 30% to about 70% by weight, about 40% to about 65% by weight, or about 40% to about 50% by weight.

18 . The liquid dispersion composition of claim 1 , wherein the first liquid component is present in the composition from about 0.1% to about 99% by weight, about 1% to about 99% by weight, about 1% to about 10% by weight, about 10% to about 80% by weight, about 20% to about 60% by weight, about 25% to about 45% by weight, or about 50% to about 60% by weight.

19 . The liquid dispersion composition of claim 1 , wherein the second liquid component is present in the composition from about 0.1% to about 99% by weight, about 1% to about 99% by weight, about 5% to about 99% by weight, about 75% to about 99% by weight, about 0.1% to about 10% by weight, or about 0.5% to about 5% by weight.

20 . The liquid dispersion composition of claim 1 , comprising:

about 40 wt. % to about 80 wt. % of the granular superabsorbent polymer;

about 1 wt. % to about 99 wt. % of the first liquid component, wherein the first liquid component comprises a nonpolar liquid component;

about 5 wt. % to about 99 wt. % of the second liquid component, wherein the second liquid component comprises a polar liquid component;

about 0.01 wt. % to about 50 wt. % of the at least one surface active agent that is different from the first liquid component or the second liquid component.

21 . The liquid dispersion composition of claim 1 , comprising:

about 30 wt. % to about 70 wt. % of the granular superabsorbent polymer;

about 5 wt. % to about 95 wt. % of the first liquid component;

about 0.5 wt. % to about 95 wt. % of the second liquid component, wherein the second liquid component comprises a polyol; and

about 0.5 wt. % to about 20 wt. % of the at least one surface active agent that is different from the first liquid component or the second liquid component.

22 . The liquid dispersion composition of claim 1 , wherein the liquid dispersion composition is enclosed within one or more containers.

23 . A liquid dispersion composition comprising:

about 25 wt. % to about 75 wt. % of a granular superabsorbent polymer, wherein the granular superabsorbent polymer comprises an acrylate polymer;

about 0.5 wt. % to about 90 wt. % of a polyol; and

about 0.2 wt. % to about 20 wt. % of one or more surface active agents.

24 . A method of preparing an absorbent coating comprising:

providing a liquid dispersion composition comprising a granular superabsorbent polymer dispersed in a liquid medium, wherein:

the granular superabsorbent polymer is present in the composition from about 10% to about 80% by weight; and

the liquid medium comprises two or more liquid components, wherein at least one of the liquid components is insoluble with the other liquid components; and

applying the liquid dispersion composition to a substrate.

25 . An absorbent coating formed by the method of claim 24 .

26 . A substrate coated with a liquid dispersion composition comprising a granular superabsorbent polymer dispersed in a liquid medium, wherein:

the granular superabsorbent polymer is present in the composition from about 10% to about 80% by weight; and

the liquid medium comprises two or more liquid components, wherein at least one of the liquid components is insoluble with the other liquid components.

27 . A liquid dispersion composition comprising a granular superabsorbent polymer dispersed in a liquid medium, wherein:

the granular superabsorbent polymer is present in the composition from about 30% to about 95% by weight; and

the liquid medium comprises at least two liquid components, wherein at least one of the liquid components is insoluble with the other liquid components, and the liquid medium comprises a first liquid component and a second liquid component.

28 . The liquid dispersion composition of claim 27 , comprising:

about 30 wt. % to about 95 wt. % of the granular superabsorbent polymer;

about 20 wt. % to about 60 wt. % of the first liquid component, wherein the first liquid component comprises a hydrocarbon liquid; and

about 0.1 wt. % to about 10 wt. % of the second liquid component, wherein the second liquid component comprises a surface active agent.

29 . The liquid dispersion composition of claim 27 , comprising:

about 30 wt. % to about 90 wt. % of the granular superabsorbent polymer;

about 10 wt. % to about 60 wt. % of the first liquid component, wherein the first liquid component comprises a nonpolar liquid component;

about 1 wt. % to about 30 wt. % of the second liquid component, wherein the second liquid component comprises a surface active agent.

Assignments (3)
RELEASE OF SECURITY INTEREST IN PATENT COLLATERAL, RECORDED ON NOVEMBER 17, 2023 AT REEL 065597, FRAME 0771 Recorded Apr 22, 2025
From: ANTARES CAPITAL LP, AS COLLATERAL AGENT
To: CHASE CORPORATION; NEPTCO INCORPORATED; NUCERA SOLUTIONS LLC; STEWART SUPERABSORBENTS, LLC
Reel/Frame 070906/0753 →
GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded Apr 22, 2025
From: CHASE CORPORATION; NEPTCO INCORPORATED; NUCERA SOLUTIONS LLC; STEWART SUPERABSORBENTS, LLC
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 070909/0765 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 18, 2024
From: BROWN, STEVEN EDWARD; MCCLELLAN, PAUL SEVIER, JR.; GUSTAVESEN, BRADLEE WATTS; RANDALL, JASON
To: CHASE CORPORATION
Reel/Frame 068940/0765 →
Continuity (6)
Provisional Application 63647221 · May 14, 2024
Provisional Application 63575508 · Apr 5, 2024
Provisional Application 63559023 · Feb 28, 2024
Provisional Application 63534280 · Aug 23, 2023
Provisional Application 63530916 · Aug 4, 2023
Related Publication 20250041827A1 · Feb 6, 2025
References Cited (28)
US 4598119A · Volk · 1986 [cited by applicant]
US 9149789B2 · Holt · 2015 [cited by applicant]
US 20090151963A1 · Sortwell · 2009 [cited by applicant]
US 20160272769A1 · Holt · 2016 [cited by applicant]
US 20210129505A1 · Mishra et al. · 2021 [cited by applicant]
US 20210130070A1 · Zhu et al. · 2021 [cited by applicant]
US 20210130752A1 · Mishra et al. · 2021 [cited by applicant]
US 20210380446A1 · Holt · 2021 [cited by applicant]
US 20220387227A1 · Kreisel et al. · 2022 [cited by applicant]
US 20230096385A1 · Ferracane et al. · 2023 [cited by applicant]
US 20230234028A1 · Collias et al. · 2023 [cited by applicant]
US 20230363954A1 · Ehrnsperger et al. · 2023 [cited by applicant]
EP 0726028A2 · 1996 [cited by applicant]
KR 20220021303A · 2022 [cited by examiner]
WO WO9640849A1 · 1996 [cited by applicant]
Kim et al. English machine translation of KR 20220021303 A. (Year: 2022). [cited by examiner]
International Search Report and Written Opinion in International Appln. No. PCT/US2024/040766, mailed on Jan. 9, 2025, 25 pages. [cited by applicant]
Invitation to Pay Fees in International Appln. No. PCT/US2024/040766, mailed on Nov. 12, 2024, 20 pages. [cited by applicant]
Atascientific.com [online], “Basic principles of particle size analysis,” 2014, retrieved on Apr. 23, 2024, retrieved from URL<https://www.atascientific.com.au/wp-content/uploads/2017/02/AN020710-Basic-Principles-Partic… [cited by applicant]
Brunauer et al., “Adsorption of Gases in Multimolecular Layers,” Journal of the American Chemical Society, 1938, 60(2):309-319 (abstract only). [cited by applicant]
Burgess et al., “Particle Size Analysis: AAPS Workshop Report, Cosponsored by the Food and Drug Administration and the United States Pharmacopeia,” AAPS Journal, 2004, 6(3):1-12. [cited by applicant]
Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density, Particle Technology Series (POTS, vol. 16), 1st ed., 2004, 365 pages (abstract only). [cited by applicant]
Handbook of Pharmaceutical Excipients, 6th edition Pharmaceutical Press, London, England, 2009, 917 pages (abstract only). [cited by applicant]
Hansen Solubility Parameters: A User's Handbook, Second Edition, CRC Press, 2007, 546 pages (abstract only). [cited by applicant]
Hansen-solubility.com [online], “Welcome to the official site of HSP and HSPiP,” available on or before Jun. 21, 2023, retrieved on Apr. 23, 2024, retrieved from URL<https://www.hansen-solubility.com/>, 4 pages. [cited by applicant]
Methods and Application of Particle Size Analysis, Cambridge University Press, 1rst Ed., 368 pages (abstract only). [cited by applicant]
Modern Superabsorbent Polymer Technology, Wiley, Nov. 1997, 304 pages (abstract only). [cited by applicant]
Thommes et al., “Physisorption of gases, with special reference to the evaluation of surface area and pore size distribution (IUPAC Technical Report),” Pure and Applied Chemistry, Jul. 2, 2015, 87(9-10):1051-1069. [cited by applicant]