IP Library › Granted Patent US 12,637,735
Granted Patent B2
US 12,637,735 · App. 18/661,231 · Granted May 26, 2026

Methods and systems for leaching a metal-bearing material

Inventor: Sarah Lyons (Vail, AZ)
Assignee: FREEPORT MINERALS CORPORATION
C22B3/165C22B1/16C22B3/22C22B15/0008C22B15/0067C22B15/0086
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Quick Facts
Patent No.
US 12,637,735
App. No.
18/661,231
Granted
May 26, 2026
Kind
B2
Abstract

Methods for recovering a metal value from a metal-bearing material are provided. The method comprises agglomerating the metal-bearing material with an agglomeration solution comprising a raffinate, an oxidant, and citric acid or salts thereof to form an agglomerated metal-bearing material; leaching the agglomerated metal-bearing material with a leaching solution comprising the raffinate and the citric acid or salts thereof to produce a pregnant leaching solution and a leached material; re-oxidizing the leached material with a curing solution comprising the raffinate and the oxidant; and recovering the metal value from the pregnant leach solution to produce the raffinate.

Claims (23)

1 . A method for extracting a metal value from a metal-bearing material, comprising:

leaching the metal-bearing material with a leaching solution comprising a raffinate, an oxidant, and citric acid or salts thereof, to produce a first leached material and a first pregnant leach solution, wherein the metal-bearing material comprises the metal value and wherein the oxidant is hydrogen peroxide; and

recovering the metal value from the first pregnant leach solution to produce the metal value and the raffinate;

wherein the metal value is copper.

2 . The method of claim 1 , wherein the first leached material further comprises ferrous (Fe 2+ ) and ferric ions (Fe 3+ ).

3 . The method of claim 2 , further comprising:

curing the first leached material with a curing solution to re-oxidize the ferrous (Fe 2+ ) ions to ferric (Fe 3+ ) ions and produce a cured leached material, wherein the curing solution comprises the raffinate and the oxidant, and wherein the cured leached material comprises the metal value;

leaching the cured leached material with the leaching solution to produce a second leached material and a second pregnant leach solution; and

recovering the metal value from the second pregnant leach solution.

4 . The method of claim 3 , wherein the curing solution further comprises citric acid or salts thereof.

5 . The method of claim 3 , wherein the curing solution comprises a concentration of hydrogen peroxide in a range of about 8% by weight to about 30% by weight.

6 . The method of claim 3 , wherein the curing solution further comprises a concentration of citric acid or salts thereof in the range of about 2 grams per liter to about 10 grams per liter.

7 . The method of claim 3 , wherein the leaching comprises a heap leach operation and the curing comprises a trickle-down cure.

8 . The method of claim 3 , wherein the curing and the leaching may comprise a cycle.

9 . The method of claim 8 , wherein the cycle may be repeated before the step of recovering.

10 . The method of claim 1 , further comprising agglomerating the metal-bearing material with an agglomeration solution before the leaching, wherein the agglomeration solution comprises the raffinate, the oxidant, and citric acid or salts thereof.

11 . The method of claim 10 , wherein the agglomeration solution comprises a concentration of hydrogen peroxide in a range of about 1% to about 6% by weight.

12 . The method of claim 10 , wherein the agglomeration solution comprises a concentration of citric acid or salts thereof in a range of about 2 grams per liter to about 10 grams per liter.

13 . The method of claim 1 , wherein the leaching solution comprises a concentration of citric acid or salts thereof in a range of about 0.1 g/l to about 20 g/l.

14 . The method of claim 1 , wherein the leaching solution comprises a concentration of hydrogen peroxide in a range of about 8% by weight.

15 . The method of claim 1 , wherein the metal-bearing material comprises a primary or secondary copper sulfide, or mixtures thereof.

16 . The method of claim 1 , wherein the leaching comprises a heap leach operation further comprising subsurface injection of the leaching solution into a heap of the heap leach operation.

17 . The method of claim 1 , wherein the leaching solution further comprises a concentration of added air and/or oxygen.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 30, 2024
From: LYONS, SARAH
To: FREEPORT MINERALS CORPORATION
Reel/Frame 067566/0068 →
Continuity (3)
Continuation 17945451 · Sep 15, 2022
Provisional Application 63246046 · Sep 20, 2021
Related Publication 20240301529A1 · Sep 12, 2024
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