IP Library › Granted Patent US 10,604,660
Granted Patent B2
US 10,604,660 · App. 13/876,328 · Granted Mar 31, 2020

Wear resistant coating, article, and method

Inventors: David A. Smith (Bellefonte, PA); James B. Mattzela (State College, PA); Paul H. Silvis (Port Matilda, PA); Gary A. Barone (Bellefonte, PA); Martin E. Higgins (Bellefonte, PA)
Assignee: SILCOTEK CORP.
C09D5/00C23C16/0272C23C16/18C23C16/30C23C16/401C23C16/56C23C30/00Y10T428/265Y10T428/31612Y10T428/31663
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Quick Facts
Patent No.
US 10,604,660
App. No.
13/876,328
Granted
Mar 31, 2020
Kind
B2
Abstract

A wear coating is disclosed that includes a layer treated by a trifunctional organosilane. An article is also disclosed, the article having a surface to which the wear coating is applied. A method of applying the wear coating is also disclosed. In some embodiments, the organosilane is trimethylsilane and the wear coating is applied by chemical vapor deposition, followed by heat treating the wear coating in the presence of the trimethylsilane.

Claims (22)

1. An article having a wear coating comprising:

a layer treated by trimethylsilane applied to a surface of the article

wherein the wear coating is applied by chemical vapor deposition via thermal decomposition of dimethylsilane;

wherein constituents of the decomposed dimethylsilane are oxidized prior to trimethylsilane treatment.

2. The article of claim 1 , wherein the article is in reciprocating contact with a second article.

3. The article of claim 2 , wherein the article is a piston head or a piston cylinder.

4. The article of claim 1 , wherein the article is a drilling tool.

5. The article of claim 1 , wherein the surface is an interior surface of the article.

6. The article of claim 1 , wherein constituents of the decomposed dimethylsilane are functionalized.

7. The article of claim 1 , wherein the wear coating has a thickness of about 100 nm to about 10,000 nm.

8. The article of claim 1 , wherein the wear coating has a wear resistance between about 13×10 −5 mm 3 /Nm and about 0.5×10 −5 mm 3 /Nm upon application of a 0.5 N force via a standard 100 Cr6 ball and circular linear speed of 3.00 cm/s.

9. The article of claim 1 , wherein the wear coating has a coefficient of friction between about 0.58 and about 0.05.

10. The article of claim 1 , wherein the surface of the article to which the wear coating is applied is metal or metallic.

11. The article of claim 1 , wherein the wear coating has a thickness in the range of about 100 nm to about 10,000 nm, a wear resistance in the range of about 13×10 −5 mm 3 /Nm to about 0.5×10 −5 mm 3 /Nm upon application of a 0.5 N force via a standard 100 Cr6 ball and circular linear speed of 3.00 cm/s, and a coefficient of friction between about 0.58 and about 0.05.

12. The article of claim 1 , wherein the wear coating has a thickness of about 200 nm to about 5,000 nm.

13. The article of claim 1 , wherein the wear coating has a thickness of about 300 nm to about 1,500 nm.

14. The article of claim 1 , wherein the constituents of the decomposed dimethylsilane that are oxidized form an oxidized layer.

15. The article of claim 14 , wherein the oxidized layer extends for 1,600 Angstroms.

16. The article of claim 1 , wherein the thermal decomposition of the dimethylsilane is at a temperature between 400° C. and 500° C.

17. The article of claim 1 , wherein the surface of the article to which the wear coating is applied is ceramic.

18. The article of claim 1 , wherein the surface of the article to which the wear coating is applied is glass.

19. An article, comprising a dimethylsilane-based layer on the article, an oxidization of the dimethylsilane-based layer on the dimethylsilane-based layer, and a trimethylsilane-based treatment on the oxidation.

Continuity (3)
Provisional Application 61389777 · Oct 5, 2010
Provisional Application 61507650 · Jul 14, 2011
Related Publication 20130244025A1 · Sep 19, 2013
Cited By (5)
US 12,269,059 US 12,291,778 US 12,352,734 US 12,473,635 US 12,522,732