IP Library Granted Patent US 11,160,761
Granted Patent B2
US 11,160,761 · App. 16/086,198 · Granted Nov 2, 2021

Silica microcapsules and methods of preparing same

Inventors: John Brahms (Morris Plains, NJ); Ronald Gabbard (Farmingdale, NJ); Feng Geng (Fort Worth, TX); Julie Ann Wieland (Edison, NJ); Li Xu (Edison, NJ); Lewis Michael Popplewell (Morganville, NJ)
Assignee: International Flavors & Fragrances Inc.
A61K9/4825A21D2/02A21D2/165A23G4/064A23L27/72A23L27/74A23P10/35A61K8/11A61K9/4816B01J13/08B01J13/206A23V2002/00
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Quick Facts
Patent No.
US 11,160,761
App. No.
16/086,198
Granted
Nov 2, 2021
Kind
B2
Abstract

Disclosed is a microcapsule containing: (i) a microcapsule core having an active material, and (ii) a microcapsule wall formed of a first polymer and second polymer. The first polymer is a sol-gel polymer. The second polymer is gum arabic, purity gum ultra, gelatin, chitosan, xanthan gum, plant gum, carboxymethyl cellulose, sodium carboxymethyl guar gum, or a combination thereof. The weight ratio between the first and second polymer is 1:10 to 10:1. Also disclosed are processes for preparing the microcapsule and uses of the microcapsules in consumer products.

Claims (4)

1. A microcapsule comprising: (i) a microcapsule core containing an active material, and (ii) a microcapsule wall formed of a first polymer and second polymer, wherein the first polymer is a sol-gel polymer, the second polymer is gum arabic, purity gum ultra, gelatin, chitosan, xanthan gum, plant gum, carboxymethyl cellulose, sodium carboxymethyl guar gum, or a combination thereof, and the weight ratio between the first and second polymer is 1:10 to 10:1, wherein the microcapsule wall is single-layered containing a polymeric network of polymerized silica interlocked with a coacervate of the second polymer wherein the sol-gel polymer is a silica polymer and the second polymer is a combination of gelatin and gum Arabic, and the weight ratio between gum Arabic and gelatin is 1:5 to 5:1.

2. The microcapsule of claim 1 furthering comprising a dispersant selected from the group consisting of quillaja saponin, N-lauroyl-L-arginine ethyl ester, sorbitan esters, lecithins, lyso-lecithins, polyethoxylated sorbitan esters, polyglyceryl esters, fatty acid esters, gum arabic, pectin, carrageenan, chitosan, chondroitin sulfate, cellulose gum, modified starch, whey protein, pea protein, egg white protein, silk protein, gelatin of fish, proteins of porcine or bovine origin, ester gum, fatty acids, and combinations thereof.

3. The microcapsule of claim 1 , wherein the active material is a fragrance, pro-fragrance, flavor, malodor counteractive agent, anti-inflammatory agent, anesthetic, analgesic, anti-viral agent, anti-infectious agent, anti-acne agent, skin lightening agent, insect repellant, emollient, skin moisturizing agent, vitamin or derivative thereof, nanometer to micron size inorganic solid, polymeric or elastomeric particle, taste modulator, probiotic, cell, or combination thereof.

4. The microcapsule of claim 1 , wherein the microcapsule has a particle size in diameter of 1 to 250 μm, and the weight ratio of between the microcapsule wall and the microcapsule core 1:50 to 2:1.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 15, 2021
From: BRAHMS, JOHN; GABBARD, RONALD; GENG, FENG; WIELAND, JULIE ANN; XU, LI; POPPLEWELL, LEWIS MICHAEL
To: INTERNATIONAL FLAVORS & FRAGRANCES INC.
Reel/Frame 056867/0329 →
Continuity (3)
Provisional Application 62310381 · Mar 18, 2016
Provisional Application 62397651 · Sep 21, 2016
Related Publication 20200306197A1 · Oct 1, 2020
Cited By (5)
US 12,201,956 US 12,325,867 US 12,390,783 US 12,514,794 US 12,559,716