IP Library › Granted Patent US 12,133,540
Granted Patent B2
US 12,133,540 · App. 17/464,747 · Granted Nov 5, 2024

Solvent based de-oiling for plant based protein extraction

Inventors: Michael A Spinelli (Moseley, VA); Krisan Singh (Midlothian, VA); Reinhold Brand (Henrico, VA)
Assignee: Tate & Lyle Solutions USA LLC
A23J1/144A23J3/14A23L11/32B01D11/0288A23V2002/00A23V2250/548A23V2300/10A23V2300/14A23V2300/31A23V2300/38
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Quick Facts
Patent No.
US 12,133,540
App. No.
17/464,747
Granted
Nov 5, 2024
Kind
B2
Abstract

A method provides for removing oil content from a source material and extracting protein from the source material prior to generating a protein concentrate, including decorticating the source material, the source material having a protein and an oil content therein, the decorticating to remove a cortex from the source material. The method includes creating a flour from the source material having the cortex removed therefrom, removing at least a portion of the oil content from the flour by generating a solvent mixture by mixing the flour with a solvent and extracting a de-oiled flour from the solvent mixture, including oil and sugars extracted from the flour. The solvent may include supercritical CO2, subcritical CO2, ethanol, or a combination thereof. The method includes drying the de-oiled flour using at least one dryer and extracting a protein concentrate from the de-oiled flour.

Claims (57)

1. A method for removing oil content from a source material and extracting protein from the source material prior to generating a protein concentrate, the method comprising:

decorticating the source material, the source material having a protein and an oil content therein, the decorticating removing a cortex from the source material;

creating a flour from the source material having the cortex removed therefrom;

removing at least a portion of the oil content from the flour by generating a solvent mixture by mixing the flour with a first solvent including supercritical carbon dioxide;

extracting a de-oiled flour from the solvent mixture, including extracting at least a portion of the first solvent from the solvent mixture, the portion of the first solvent extracted from the solvent mixture including oil and sugars extracted from the flour;

drying the de-oiled flour using at least one dryer; and

extracting a protein concentrate from the de-oiled flour.

2. The method of claim 1 , wherein the removing the at least a portion of the oil content further comprises:

mixing the flour with a second solvent including an alcohol.

3. The method of claim 2 , wherein the removing the at least a portion of the oil content further comprises:

mixing the flour with the first solvent in a first phase and mixing the flour with the second solvent in a second phase.

4. The method of claim 2 , wherein the alcohol is ethanol.

5. The method of claim 1 further comprising:

feeding the first solvent extracted from the solvent mixture, in combination with the extracted oil and sugars, to a solvent recycling unit.

6. The method of claim 1 , wherein the source material is at least one of: chickpeas and fava beans.

7. A method for removing oil content from a source material and extracting protein from the source material prior to generating a protein concentrate, the method comprising:

decorticating the source material, the source material having a protein and an oil content therein, the decorticating removing a cortex from the source material;

creating a flour from the source material having the cortex removed therefrom;

removing at least a portion of the oil content from the flour by generating a solvent mixture by mixing the flour with a first solvent including subcritical carbon dioxide;

extracting a de-oiled flour from the solvent mixture, including extracting at least a portion of the first solvent from the solvent mixture, the portion of the first solvent extracted from the solvent mixture including oil and sugars extracted from the flour;

drying the de-oiled flour using at least one dryer; and

extracting a protein concentrate from the de-oiled flour.

8. The method of claim 7 , wherein the removing the at least a portion of the oil content further comprises:

mixing the flour with a second solvent including an alcohol.

9. The method of claim 8 , wherein the removing the at least a portion of the oil content further comprises:

mixing the flour with the first solvent in a first phase and mixing the flour with the second solvent in a second phase.

10. The method of claim 8 , wherein the alcohol is ethanol.

11. The method of claim 7 further comprising:

feeding the first solvent extracted from the solvent mixture, in combination with the extracted oil and sugars, to a solvent recycling unit.

12. The method of claim 7 , wherein the source material is at least one of: chickpeas and fava beans.

13. A method for removing oil content from a source material and extracting protein from the source material prior to generating a protein concentrate, the method comprising:

decorticating the source material, the source material having a protein and an oil content therein, the decorticating removing a cortex from the source material;

creating a flour from the source material having the cortex removed therefrom;

removing at least a portion of the oil content from the flour by generating a solvent mixture by mixing the flour with a first solvent including carbon dioxide and mixing the flour with a second solvent including an alcohol;

extracting a de-oiled flour from the solvent mixture, including extracting at least a portion of the first solvent from the solvent mixture and at least a portion of the second solvent from the solvent mixture, including oil and sugars extracted from the flour;

drying the de-oiled flour using at least one dryer; and

extracting a protein concentrate from the de-oiled flour.

14. The method of claim 13 , wherein the removing the at least a portion of the oil content further comprises:

mixing the flour with the first solvent in a first phase and mixing the flour with the second solvent in a second phase.

15. The method of claim 13 , wherein the alcohol is ethanol and the carbon dioxide is at least one of: supercritical carbon dioxide and subcritical carbon dioxide.

16. The method of claim 13 further comprising:

feeding at least one of the first solvent and the second solvent extracted from the solvent mixture to a solvent recycling unit.

17. The method of claim 13 , wherein the source material is at least one of:

chickpeas and fava beans.

18. A method for removing oil content from a source material and extracting protein from the source material prior to generating a protein concentrate, the method comprising:

decorticating the source material, the source material having a protein and an oil content therein, the decorticating removing a cortex from the source material;

creating a flour from the source material having the cortex removed therefrom;

removing at least a portion of the oil content from the flour by generating a solvent mixture by mixing the flour with a solvent;

extracting a de-oiled flour from the solvent mixture, including extracting at least a portion of the solvent from the solvent mixture, the portion of the solvent extracted from the solvent mixture including oil and sugars extracted from the flour;

drying the de-oiled flour using at least one dryer; and

extracting a protein concentrate from the de-oiled flour.

19. The method of claim 18 , wherein the solvent includes a supercritical gas.

20. The method of claim 18 , wherein the solvent includes a subcritical gas.

21. The method of claim 20 , wherein the subcritical gas is subcritical carbon dioxide.

22. The method of claim 18 , wherein the solvent includes ethanol.

23. The method of claim 18 , wherein the solvent includes ethanol in water.

24. The method of claim 18 , wherein the solvent includes a combination of at least two of: supercritical carbon dioxide, subcritical carbon dioxide, a supercritical gas other than carbon dioxide, a subcritical gas other than carbon dioxide, ethanol, and water.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 12, 2022
From: NUTRIATI INC.
To: TATE & LYLE SOLUTIONS USA LLC
Reel/Frame 060050/0266 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 24, 2021
From: SPINELLI, MICHAEL A; SINGH, KRISAN; BRAND, REINHOLD
To: NUTRIATI, INC.
Reel/Frame 057588/0024 →
Continuity (7)
Continuation In Part 16805930 · Mar 2, 2020
Continuation 15886534 · Feb 1, 2018
Continuation In Part 15014882 · Feb 3, 2016
Continuation In Part 14997744 · Jan 18, 2016
Continuation In Part 14694341 · Apr 23, 2015
Provisional Application 62453151 · Feb 1, 2017
Related Publication 20220000142A1 · Jan 6, 2022