IP Library › Granted Patent US 12,221,443
Granted Patent B2
US 12,221,443 · App. 17/859,015 · Granted Feb 11, 2025

Crystalline forms of diazabicyclooctane derivative and production process thereof

Inventors: Takao Abe (Kanagawa, JP); Takeshi Furuuchi (Kanagawa, JP); Yoshiaki Sakamaki (Kanagawa, JP); Nakako Mitsuhashi (Kanagawa, JP); Yumiko Saito (Kanagawa, JP)
Assignee: MEIJI SEIKA PHARMA CO., LTD.
C07D471/08A61K31/439A61K45/06C07B2200/13
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Quick Facts
Patent No.
US 12,221,443
App. No.
17/859,015
Granted
Feb 11, 2025
Kind
B2
Abstract

A crystalline form I of a compound represented by Formula (VII-1): having characteristic peaks appearing at lattice spacing (d) of 7.34, 5.66, 5.53, 5.30, 5.02, 4.66, 4.37, 4.28, 4.06, 3.68, 3.62, 3.47, 3.36, 3.30, 3.16, 3.11, 3.03, 2.99 and 2.50 Å in the powder X-ray diffraction pattern.

Claims (23)

1. A crystalline form II of a compound represented by Formula (VII-1):

having characteristic peaks appearing at lattice spacing (d) of 9.46, 5.62, 5.23, 5.10, 5.00, 4.91, 4.67, 4.45, 4.29, 3.96, 3.78, 3.71, 3.52, 3.24, 3.18, 3.10, 3.02, 2.88, 2.81, 2.77, 2.67, 2.50 and 2.45 Å in the powder X-ray diffraction pattern.

2. A process for producing the crystalline form II according to claim 1 , comprising adjusting the temperature of a solution of a compound represented by the Formula (VII-1) between 10 to 15° C., adding isopropanol and stirring.

3. A pharmaceutical composition comprising a pharmaceutically effective amount of the crystalline form II according to claim 1 and a pharmaceutically acceptable carrier.

4. A pharmaceutical composition comprising the crystalline form II according to claim 1 , a β-lactam antibiotic selected from the group consisting of ampicillin, amoxicillin, piperacillin, ticarcillin, flomoxef, cefotaxime, ceftriaxone, ceftazidime, cefepime, ceftaroline, ceftolozane, imipenem, meropenem, biapenem, doripenem, ertapenem and aztreonam, and optionally a pharmaceutically acceptable carrier.

5. A method for treating a bacterial infection which comprises administering to a subject in need thereof the crystalline form II of a compound according to claim 1 , and a β-lactam antibiotic selected from the group consisting of ampicillin, amoxicillin, piperacillin, ticarcillin, flomoxef, cefotaxime, ceftriaxone, ceftazidime, cefepime, ceftaroline, ceftolozane, imipenem, meropenem, biapenem, doripenem, ertapenem and aztreonam, in combination.

6. A pharmaceutical composition comprising a mixture of at least two crystalline forms of a compound represented by the following Formula (VII-1):

and optionally a pharmaceutically acceptable carrier,

wherein the at least two crystalline forms comprise:

a crystalline form I of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 7.34, 5.66, 5.53, 5.30, 5.02, 4.66, 4.37, 4.28, 4.06, 3.68, 3.62, 3.47, 3.36, 3.30, 3.16, 3.11, 3.03, 2.99 and 2.50 Å in the powder X-ray diffraction pattern; and

any one crystalline form selected from the group consisting of:

a crystalline form II of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 9.46, 5.62, 5.23, 5.10, 5.00, 4.91, 4.67, 4.45, 4.29, 3.96, 3.78, 3.71, 3.52, 3.24, 3.18, 3.10, 3.02, 2.88, 2.81, 2.77, 2.67, 2.50 and 2.45 Å in the powder X-ray diffraction pattern;

a crystalline form III of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 8.32, 6.10, 5.98, 5.51, 5.16, 5.07, 4.85, 4.70, 4.61, 4.35, 4.20, 4.06, 4.00, 3.95, 3.77, 3.73, 3.65, 3.42, 3.39, 3.36, 3.26, 3.23, 3.13, 3.09, 2.99, 2.81 and 2.52 Å in the powder X-ray diffraction pattern; and

a crystalline form IV of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 7.88, 6.41, 5.20, 4.67, 4.50, 4.02, 3.81, 3.75, 3.70, 3.62, 3.38, 3.23, 3.20, and 2.74 Å in the powder X-ray diffraction pattern.

7. A pharmaceutical composition comprising a mixture of at least two crystalline forms of a compound represented by the following Formula (VII-1):

a β-lactam antibiotic selected from the group consisting of ampicillin, amoxicillin, piperacillin, ticarcillin, flomoxef, cefotaxime, ceftriaxone, ceftazidime, cefepime, ceftaroline, ceftolozane, imipenem, meropenem, biapenem, doripenem, ertapenem and aztreonam,

and optionally a pharmaceutically acceptable carrier,

wherein the at least two crystalline forms comprise:

a crystalline form I of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 7.34, 5.66, 5.53, 5.30, 5.02, 4.66, 4.37, 4.28, 4.06, 3.68, 3.62, 3.47, 3.36, 3.30, 3.16, 3.11, 3.03, 2.99 and 2.50 Å in the powder X-ray diffraction pattern; and

any one crystalline form selected from the group consisting of:

a crystalline form II of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 9.46, 5.62, 5.23, 5.10, 5.00, 4.91, 4.67, 4.45, 4.29, 3.96, 3.78, 3.71, 3.52, 3.24, 3.18, 3.10, 3.02, 2.88, 2.81, 2.77, 2.67, 2.50 and 2.45 Å in the powder X-ray diffraction pattern;

a crystalline form III of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 8.32, 6.10, 5.98, 5.51, 5.16, 5.07, 4.85, 4.70, 4.61, 4.35, 4.20, 4.06, 4.00, 3.95, 3.77, 3.73, 3.65, 3.42, 3.39, 3.36, 3.26, 3.23, 3.13, 3.09, 2.99, 2.81 and 2.52 Å in the powder X-ray diffraction pattern; and

a crystalline form IV of the compound represented by the Formula (VII-1), having characteristic peaks appearing at lattice spacing (d) of 7.88, 6.41, 5.20, 4.67, 4.50, 4.02, 3.81, 3.75, 3.70, 3.62, 3.38, 3.23, 3.20, and 2.74 Å in the powder X-ray diffraction pattern.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 7, 2022
From: ABE, TAKAO; FURUUCHI, TAKESHI; SAKAMAKI, YOSHIAKI; MITSUHASHI, NAKAKO; SAITO, YUMIKO
To: MEIJI SEIKA PHARMA CO., LTD.
Reel/Frame 060417/0058 →
Priority Claims (1)
JP 2013-211242 · Oct 8, 2013 · national
Continuity (4)
Division 16793843 · Feb 18, 2020
Continuation 16148774 · Oct 1, 2018
Continuation 15027956
Related Publication 20220348578A1 · Nov 3, 2022
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