IP Library Granted Patent US 12,247,295
Granted Patent B2
US 12,247,295 · App. 18/238,794 · Granted Mar 11, 2025

Platinum nanoparticle deposition on a series of UiO metal-organic frameworks

Inventors: Hannah Marie Ashberry (Alexandria, VA); Albert Epshteyn (Potomac, MD); James A. Ridenour (Arlington, VA); William A. Maza (Silver Spring, MD); Olga Baturina (Burke, VA)
Assignee: The Government of the United States of America, as represented by the Secretary of the Navy
C23C22/02
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Quick Facts
Patent No.
US 12,247,295
App. No.
18/238,794
Granted
Mar 11, 2025
Kind
B2
Abstract

Deposition of Pt nanoparticles on UiO metal organic frameworks via solvothermal reduction is achieved by reducing Pt acetylacetonate (Pt(acac) 2 ) in a UiO-66 and N,N-dimethylformamide (DMF) mixture at, for example, 130° C. for 18 hrs. Modification of reaction temperature and time can control the size of the Pt nanoparticles.

Claims (11)

1. A method of depositing platinum nanoparticles onto a metal organic framework (MOF), the method comprising:

providing a MOF in N,N-dimethylformamide (DMF); and

contacting the MOF with platinum acetylacetonate at a temperature between 100° C. and 180° C., thereby depositing platinum nanoparticles onto the MOF.

2. The method of claim 1 , wherein said MOF is UiO-66.

3. The method of claim 1 , wherein said temperature is between 120° C. and 150° C.

4. The method of claim 1 , wherein said depositing is accomplished as a single reaction to produce said platinum nanoparticles deposited onto the MOF without a need for additional steps.

5. A method of depositing platinum nanoparticles onto a metal organic framework (MOF), the method consisting essentially of:

providing a MOF in N,N-dimethylformamide (DMF); and

contacting the MOF with platinum acetylacetonate at a temperature between 100° C. and 180° C., thereby depositing platinum nanoparticles onto the MOF.

6. The method of claim 4 , wherein said MOF is UiO-66.

7. The method of claim 4 , wherein said temperature is between 120° C. and 150° C.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2023
From: EPSHTEYN, ALBERT; ASHBERRY, HANNAH MARIE; RIDENOUR, JAMES A.; BATURINA, OLGA; MAZA, WILLIAM A.
To: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY
Reel/Frame 064724/0193 →
Continuity (2)
Provisional Application 63374131 · Aug 31, 2022
Related Publication 20240068106A1 · Feb 29, 2024
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