IP Library › Granted Patent US 12,467,662
Granted Patent B2
US 12,467,662 · App. 17/861,044 · Granted Nov 11, 2025

Integrated dilution refrigerators

Inventors: Corban I. Tillemann-Dick (Denver, CO); Kyle J. Thompson (Boulder, CO); John Ogando Dos Santos Allan (Boulder, CO)
Assignee: Maybell Quantum Industries, Inc.
F25B9/12F25B9/10F25B9/145F25B25/005F25D19/006H05K7/208B33Y80/00F25B2500/13H05K7/20827
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Quick Facts
Patent No.
US 12,467,662
App. No.
17/861,044
Granted
Nov 11, 2025
Kind
B2
Abstract

A dilution refrigerator is provided. The dilution refrigerator includes a plurality of thermal stages configured to be cooled to a plurality of temperatures. A coldest thermal stage of the plurality of thermal stages is disposed above warmer thermal stages of the plurality of thermal stages such that the coldest thermal stage is positioned furthest from a floor supporting the dilution refrigerator.

Claims (47)

1 . A dilution refrigerator comprising:

a plurality of thermal stages configured to be cooled to a plurality of temperatures, wherein:

a coldest thermal stage of the plurality of thermal stages is disposed above warmer thermal stages of the plurality of thermal stages such that the coldest thermal stage is positioned furthest from a floor supporting the dilution refrigerator; and

a still configured to provide cooling by distilling 3 He vapor from a 3 He— 4 He mixture, wherein:

the still comprises a pumping port comprising a pipe entering the still through a surface of the still other than a surface of the still furthest from the floor,

the pipe enters the still through a surface of the still closest to the floor, and

the pipe is coupled to a trap, comprising:

a p-trap; and

a superleak configured to remove superfluid 4 He from the p-trap.

2 . The dilution refrigerator of claim 1 , further comprising:

a de-mixing chamber disposed above and thermally coupled to the coldest thermal stage;

a mixing chamber disposed further from the floor than the de-mixing chamber; and

a fountain pump configured to transport 4 He from the de-mixing chamber to the mixing chamber.

3 . The dilution refrigerator of claim 2 , further comprising a heat exchanger configured to cool 4 He as the 4 He is transported from the de-mixing chamber to the mixing chamber.

4 . The dilution refrigerator of claim 2 , further comprising:

a first impedance stage configured to cool a 3 He— 4 He mixture;

a heat exchange stage configured to cool the 3 He— 4 He mixture prior to passing through the first impedance stage; and

the still is configured to distill 3 He from the 3 He— 4 He mixture received from the first impedance stage.

5 . The dilution refrigerator of claim 1 , wherein the pipe comprises a barrier configured to prevent a liquid 4 He film from creeping into an outlet of the pipe.

6 . The dilution refrigerator of claim 5 , wherein the barrier comprises one or more knife edges on the outlet of the pipe.

7 . The dilution refrigerator of claim 5 , wherein the barrier comprises a ring barrier on an exterior surface of the pipe.

8 . The dilution refrigerator of claim 5 , wherein the barrier comprises a ring barrier on an interior surface of the pipe.

9 . The dilution refrigerator of claim 5 , wherein the barrier comprises a heater.

10 . The dilution refrigerator of claim 1 , further comprising:

at least one inner radiation shield;

an outer vacuum chamber housing the at least one inner radiation shield and the plurality of thermal stages; and

a hole disposed in a portion of a surface of the outer vacuum chamber, the hole extending through the at least one inner radiation shield and disposed adjacent to the coldest thermal stage such that the hole is configured to provide access to the coldest thermal stage of the dilution refrigerator through the hole and while the outer vacuum chamber houses the plurality of thermal stages.

11 . The dilution refrigerator of claim 10 , wherein the hole is disposed proximate a top surface of the outer vacuum chamber.

12 . The dilution refrigerator of claim 10 , wherein the hole comprises a hermetic opening.

13 . The dilution refrigerator of claim 10 , wherein the hole comprises a hinged door.

14 . The dilution refrigerator of claim 10 ,

wherein the outer vacuum chamber is configured to fit within a container configured to integrate with commercial server rack infrastructure.

15 . The dilution refrigerator of claim 14 , wherein the container is a 19-inch server rack.

16 . The dilution refrigerator of claim 10 , further comprising a door or a panel configured to seal the hole in the surface of the outer vacuum chamber during operation of the dilution refrigerator.

17 . The dilution refrigerator of claim 1 , further comprising a pulse tube configured to cool a thermal stage of the plurality of thermal stages to approximately 4 K.

18 . A dilution refrigerator comprising:

a plurality of thermal stages configured to be cooled to a plurality of temperatures, wherein:

a coldest thermal stage of the plurality of thermal stages is disposed above warmer thermal stages of the plurality of thermal stages such that the coldest thermal stage is positioned furthest from a floor supporting the dilution refrigerator;

a de-mixing chamber disposed above and thermally coupled to the coldest thermal stage;

a mixing chamber disposed further from the floor than the de-mixing chamber;

a fountain pump configured to transport 4 He from the de-mixing chamber to the mixing chamber;

a first impedance stage configured to cool a 3 He/ 4 He mixture;

a heat exchange stage configured to cool the 3 He/ 4 He mixture prior to passing through the first impedance stage; and

a still configured to distill 3 He from the 3 He/ 4 He mixture received from the first impedance stage,

wherein the heat exchange stage is configured to cool the 3 He/ 4 He mixture by returning cold 3 He to the still from the mixing chamber.

19 . The dilution refrigerator of claim 18 , wherein the still is configured to provide cooling by distilling 3 He vapor from the 3 He/ 4 He mixture and the still comprises a pumping port comprising a pipe entering the still through a surface of the still other than a surface of the still furthest from the floor.

20 . The dilution refrigerator of claim 19 , wherein the pipe enters the still through a surface of the still closest to the floor.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 22, 2024
From: TILLEMANN-DICK, CORBAN I.; THOMPSON, KYLE J.; OGANDO DOS SANTOS ALLAN, JOHN
To: MAYBELL QUANTUM INDUSTRIES, INC.
Reel/Frame 066532/0111 →
Continuity (3)
Provisional Application 63319248 · Mar 11, 2022
Provisional Application 63219795 · Jul 8, 2021
Related Publication 20230010920A1 · Jan 12, 2023
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