IP Library › Granted Patent US 12,571,090
Granted Patent B2
US 12,571,090 · App. 18/139,246 · Granted Mar 10, 2026

Method for cleaning a vacuum system used in the manufacture of OLED devices, method for vacuum deposition on a substrate to manufacture OLED devices, and apparatus for vacuum deposition on a substrate to manufacture OLED devices

Inventors: Jose Manuel Dieguez-Campo (Hanau, DE); Stefan Keller (Mainaschaff, DE); Jae Won Lee (Aschaffenburg, DE); Takashi Anjiki (Kyoto, JP); Dieter Haas (San Jose, CA)
Assignee: Applied Materials, Inc.
C23C14/564B08B3/08B08B7/0035B08B7/04B08B9/08C23C14/12C23C14/24C23C14/566H10K71/164H10K71/166B08B2209/08
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Quick Facts
Patent No.
US 12,571,090
App. No.
18/139,246
Granted
Mar 10, 2026
Kind
B2
Abstract

The present disclosure provides a method for cleaning a vacuum system used in the manufacture of OLED devices. The method includes performing pre-cleaning for cleaning at least a portion of the vacuum system, and performing plasma cleaning using a remote plasma source.

Claims (33)

1 . A method for cleaning a vacuum system, comprising:

pre-cleaning a chamber of the vacuum system at a first pressure within the chamber;

reducing the pressure within the chamber from the first pressure to a second pressure to establish a technical vacuum; and

plasma cleaning the chamber using a remote plasma source, wherein plasma cleaning the chamber is performed at the second pressure within the chamber.

2 . The method of claim 1 , wherein the plasma cleaning is a final cleaning procedure before operating the vacuum system.

3 . The method of claim 1 , wherein the chamber comprises a vacuum chamber.

4 . The method of claim 3 , wherein plasma cleaning the chamber comprises cleaning one or more inner walls of the vacuum chamber.

5 . The method of claim 1 , wherein plasma cleaning the chamber comprises cleaning one or more components inside the chamber.

6 . The method of claim 5 , wherein the one or more components are selected from the group consisting of mechanical components, moveable components, drives, valves, and any combination thereof.

7 . The method of claim 1 , wherein the method further comprises plasma cleaning one or more mask devices used during a deposition process.

8 . The method of claim 1 , wherein the method is performed after a maintenance procedure of the vacuum system or portions of the vacuum system.

9 . The method of claim 1 , wherein plasma cleaning the chamber comprises plasma cleaning one or more chambers of the vacuum system selected from the group consisting of a load lock chamber, a cleaning chamber, a vacuum deposition chamber, a vacuum processing chamber, a transfer chamber, a routing module, and any combination thereof.

10 . The method of claim 1 , wherein plasma cleaning the chamber comprises using a plasma of pure oxygen or oxygen mixtures with nitrogen or argon.

11 . The method of claim 1 , wherein pre-cleaning the chamber comprises a wet chemical cleaning process.

12 . The method of claim 1 , wherein the second pressure is about 10 −2 mbar or less.

13 . The method of claim 1 , wherein plasma cleaning the chamber provides a cleanliness level or 10 −9 grams/cm 2 when measured using a standard gas chromatography-mass spectrometry (GCMS) procedure.

14 . A method for vacuum deposition on a substrate, comprising:

pre-cleaning a chamber of the vacuum system at a first pressure within the chamber;

reducing the pressure within the chamber from the first pressure to a second pressure to establish a technical vacuum;

plasma cleaning the chamber using a remote plasma source, wherein plasma cleaning the chamber is performed at the second pressure within the chamber; and

depositing one or more layers of material on a substrate.

15 . The method of claim 14 , wherein plasma cleaning the chamber comprises using a plasma of pure oxygen or oxygen mixtures with nitrogen or argon.

16 . The method of claim 14 , wherein pre-cleaning the chamber comprises a wet chemical cleaning process.

17 . The method of claim 14 , wherein the second pressure is about 10 −2 mbar or less.

18 . The method of claim 14 , wherein plasma cleaning the chamber provides a cleanliness level or 10 −9 grams/cm 2 when measured using a standard gas chromatography-mass spectrometry (GCMS) procedure.

19 . An apparatus for vacuum deposition on a substrate, comprising:

a vacuum chamber;

a remote plasma source connected to the vacuum chamber; and

a controller connected to the remote plasma source to perform a plasma cleaning as a final cleaning procedure, wherein the controller is configured to implement a method for cleaning a vacuum system, the method comprising:

pre-cleaning a chamber of the vacuum system at a first pressure within the chamber,

reducing the pressure within the chamber from the first pressure to a second pressure to establish a technical vacuum, and

plasma cleaning the chamber using a remote plasma source, wherein plasma cleaning the chamber is performed at the second pressure within the chamber.

20 . The method of claim 19 , wherein the second pressure is about 10 −2 mbar or less.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2023
From: ANJIKI, TAKASHI; HAAS, DIETER
To: APPLIED MATERIALS, INC.
Reel/Frame 063843/0368 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2023
From: APPLIED MATERIALS GMBH & CO. KG
To: APPLIED MATERIALS, INC.
Reel/Frame 063843/0392 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2023
From: DIEGUEZ-CAMPO, JOSE MANUEL; KELLER, STEFAN; LEE, JAE WON
To: APPLIED MATERIALS GMBH & CO.KG
Reel/Frame 063843/0400 →
Continuity (2)
Continuation 16318052
Related Publication 20230256483A1 · Aug 17, 2023
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