IP Library Granted Patent US 12,157,834
Granted Patent B2
US 12,157,834 · App. 17/009,961 · Granted Dec 3, 2024

Composition and method for polysilicon CMP

Inventors: Sarah Brosnan (St. Charles, IL); Brian Reiss (Woodridge, IL)
Assignee: CMC Materials LLC
C09G1/02B24B1/00B24B37/044C09G1/00C09G1/04C09G1/06C09K3/1454C09K3/1463H01L21/30625H01L21/3212
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Quick Facts
Patent No.
US 12,157,834
App. No.
17/009,961
Granted
Dec 3, 2024
Kind
B2
Abstract

A chemical mechanical polishing composition for polishing a substrate having a polysilicon layer includes a water based liquid carrier, a silica abrasive, an amino acid or guanidine derivative containing polysilicon polishing accelerator, and an alkali metal salt. The composition includes less than about 500 ppm tetraalkylammonium salt and has a pH in a range from about 10 to about 11.

Claims (17)

1. A chemical mechanical polishing composition for polishing a substrate containing a polysilicon layer, the composition comprising:

a water based liquid carrier;

about 0.1 to about 3 weight percent silica abrasive particles dispersed in the liquid carrier;

about 0.05 to about 1 weight percent of a polysilicon accelerator, wherein the polysilicon accelerator is arginine, trimethylglycine, guanidine carbonate, or a mixture thereof;

an alkali metal salt;

wherein the composition further comprising about 0.01 to about 1 weight percent of a potassium salt and further comprising about 0.01 to about 0.5 weight percent of a heterocyclic amine;

wherein the composition has a pH in a range from about 10 to about 11, wherein the composition further comprises about 0.05 to about 0.5 weight percent of an amino phosphonic acid compound; and

wherein the composition comprises less than about 500 ppm by weight tetraalkylammonium salts, and wherein the composition further comprises about 0.03 to about 0.3 weight percent of potassium bicarbonate.

2. The composition of claim 1 , comprising from about 0.2 to about 1.5 weight percent of the silica abrasive particles.

3. The composition of claim 1 , comprising from about 0.1 to about 0.5 weight percent of the polysilicon accelerator.

4. The composition of claim 1 , wherein the polysilicon accelerator is a guanidine derivative.

5. The composition of claim 1 , wherein the heterocyclic amine is a triazole compound.

6. The composition of claim 1 , wherein the amino phosphonic acid compound is amino trimethylene phosphonic acid.

7. The composition of claim 1 further comprising:

from about 0.03 to about 0.3 weight percent of potassium bicarbonate; and

wherein the polysilicon accelerator is arginine, and wherein the amino phosphonic acid compound is amino trimethylene phosphonic acid.

8. The composition of claim 1 , wherein the composition comprises less than about 10 ppm tetraalkylammonium salts.

Assignments (7)
CHANGE OF NAME Recorded Nov 8, 2023
From: CMC MATERIALS, INC.
To: CMC MATERIALS LLC
Reel/Frame 065517/0783 →
SECURITY INTEREST Recorded Jul 8, 2022
From: CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 060615/0001 →
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
RELEASE OF SECURITY INTEREST Recorded Jul 6, 2022
From: JPMORGAN CHASE BANK, N.A.
To: CABOT MICROELECTRONICS CORPORATION; QED TECHNOLOGIES INTERNATIONAL, INC.; FLOWCHEM LLC; KMG ELECTRONIC CHEMICALS, INC.; KMG-BERNUTH, INC.; MPOWER SPECIALTY CHEMICALS LLC; SEALWELD (USA), INC.; INTERNATIONAL TEST SOLUTIONS, LLC; CMC MATERIALS, INC.
Reel/Frame 060592/0260 →
SECURITY AGREEMENT Recorded Jul 2, 2021
From: CMC MATERIALS, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 056752/0645 →
CHANGE OF NAME Recorded Jan 13, 2021
From: CABOT MICROELECTRONICS CORPORATION
To: CMC MATERIALS, INC.
Reel/Frame 054980/0681 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 2, 2020
From: BROSNAN, SARAH; REISS, BRIAN
To: CABOT MICROELECTRONICS CORPORATION
Reel/Frame 053669/0957 →
Continuity (2)
Provisional Application 62895838 · Sep 4, 2019
Related Publication 20210062043A1 · Mar 4, 2021