IP Library Granted Patent US 12,480,142
Granted Patent B2
US 12,480,142 · App. 18/210,805 · Granted Nov 25, 2025

Processes for separating whole stillage

Inventor: Jason Bootsma (Wichita, KS)
Assignee: POET Grain (Octane), LLC
C12P7/10B01D17/0217B01D33/00C11B1/10C12M47/10C12P7/14C12P7/6409C12P19/02C12P19/14C12M45/04C12M47/06C12N9/2437C12P2201/00
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,480,142
App. No.
18/210,805
Granted
Nov 25, 2025
Kind
B2
Abstract

Improved processes and systems for recovering products from a corn fermentation mash. In some examples, a process recovers an oil product, a protein meal product, and a fiber product from a slurry. A process includes the following steps: introducing the slurry into a device with a flexible screen and mechanical agitation to produce a filtrate and a fibrous solid stream; and introducing the filtrate into a three-phase centrifuge to produce an oil stream, a high protein solids stream, and a water with solubles stream. The flexible screen includes a washing nozzle. The slurry is whole stillage from an ethanol process. The three-phase centrifuge is a three-phase decanter. The filtrate is heated before introducing into the three-phase centrifuge. The filtrate is optionally evaporated before introducing into the three-phase centrifuge.

Claims (43)

1 . A process for recovering an oil product, a protein meal product, and a corn fiber product from corn pieces comprising:

introducing the corn pieces into an ethanol production process to produce a whole stillage;

introducing the whole stillage into a filtration device comprising a flexible screen and a mechanical agitation mechanism to produce a filtrate and a fibrous solid stream;

introducing the filtrate into a three-phase centrifuge to produce the oil product, a high protein solids stream, and a solubles stream;

dewatering the fibrous solid stream to produce a wet fibrous stream;

drying the high protein solids stream to produce the protein meal product;

evaporating the solubles stream to produce a condensed solubles stream;

mixing the wet fibrous stream and the condensed solubles stream to produce a mixture;

drying the mixture to produce the corn fiber with solubles product; and

recycling at least a portion of the filtrate to the whole stillage.

2 . The process of claim 1 , wherein:

the filtration device comprises a washing nozzle housed inside the flexible screen and positioned to provide counter-current washing of solids in the

filtration device;

and

the filtration device does not comprise a conveying element.

3 . The process of claim 1 , wherein the three-phase centrifuge is a three-phase decanter.

4 . The process of claim 1 , wherein the fibrous solid stream is washed and dewatered to produce additional filtrate.

5 . The process of claim 1 , wherein the filtrate is heated before introduction into the three-phase centrifuge.

6 . The process of claim 1 , wherein the filtrate is evaporated before introduction into the three-phase centrifuge.

7 . A process for separating at least a protein meal product from whole stillage, wherein the process comprises:

separating a first stream and a second stream from whole stillage, wherein the first stream is a fiber rich stream;

separating at least a portion of the second stream via one or more separators into at least a protein rich stream and a clarified stillage;

removing water from the protein rich stream to form at least a protein rich product stream and a water stream; and

recycling at least a portion of the water stream to the whole stillage.

8 . The process of claim 7 , wherein the whole stillage is separated via one or more pressure screens, one or more centrifuges, one or more paddle screens, one or more fiber filters, one or more rotary drum screens, one or more rotary vacuum drum filters, one or more brush strainers, one or more vibratory separators, one or more centrifugal screeners, one or more linear motion screens, one or more vacu-deck screens, and combinations thereof.

9 . The process of claim 7 , wherein the whole stillage is separated via one or more fiber filters, wherein each fiber filter comprises:

a flexible screen; and

a mechanical agitation mechanism to produce the fiber rich stream and a filtrate as the second stream, wherein the flexible screen is coupled to the filter device via one or more elastic supports.

10 . The process of claim 7 , wherein the whole stillage is separated via one or more fiber filters, wherein each fiber filter comprises:

a flexible screen;

a rotor positioned inside the flexible screen;

one or more paddles coupled to the rotor, wherein each paddle pulses the whole stillage radially outward against the flexible screen; and

flighting coupled to the rotor, wherein the flighting conveys solids present in the whole stillage toward a discharge outlet of the fiber filter to form the fiber rich stream.

11 . The process of claim 10 , wherein the flexible screen comprises a flexible, filtering sleeve, and wherein the whole stillage flows into the flexible, filtering sleeve so that the second stream flows through openings in the flexible, filtering sleeve and separates from the whole stillage.

12 . The process of claim 11 , wherein the flexible, filtering sleeve comprises polymer fabric.

13 . The process of claim 11 , wherein the fiber filter is configured to permit the flexible, filtering sleeve to expand and contract along a longitudinal axis of the flexible, filtering sleeve.

14 . The process of claim 11 , wherein the rotor rotates in a manner that pulses whole stillage radially outward against the flexible, filtering sleeve.

15 . The process of claim 7 , wherein the one or more separators comprise one or more two-phase centrifuges.

16 . The process of claim 7 , wherein removing water from the protein rich stream to form at least a protein rich product stream and a water stream comprises separating the protein rich stream into the protein rich product stream and the water stream via one or more decanter centrifuges.

17 . The process of claim 7 , further comprising removing water from the protein rich product stream via one or more dryers to form a dried protein rich product.

18 . The process of claim 7 , further comprising separating a water stream from the fiber rich stream via one or more centrifuges.

19 . The process of claim 9 , wherein the filter device comprises a washing nozzle inside the flexible screen positioned for counter-current washing of solids contained in the filter device.

20 . The process of claim 9 , wherein the whole stillage is from an ethanol process.

Assignments (3)
CHANGE OF NAME Recorded Jul 13, 2023
From: FLINT HILLS RESOURCES GRAIN, LLC
To: POET GRAIN (OCTANE), LLC
Reel/Frame 064270/0877 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2023
From: FLINT HILLS RESOURCES, LP
To: FLINT HILLS RESOURCES GRAIN, LLC
Reel/Frame 064198/0783 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 7, 2023
From: BOOTSMA, JASON
To: FLINT HILLS RESOURCES, LP
Reel/Frame 064180/0778 →
Continuity (8)
Continuation 16734422 · Jan 6, 2020
Continuation In Part 16102835 · Aug 14, 2018
Division 15604507 · May 24, 2017
Continuation In Part 15529025
Continuation In Part 15529014
Provisional Application 62324159 · Apr 18, 2016
Provisional Application 62260181 · Nov 25, 2015
Related Publication 20230332189A1 · Oct 19, 2023
References Cited (276)
US 1198774A · Salisbury · 1916 [cited by examiner]
US 2446913A · Erlich · 1948 [cited by applicant]
US 2478937A · Neithamer · 1949 [cited by applicant]
US 2698826A · Peltzer · 1955 [cited by applicant]
US 3538551A · Joa · 1970 [cited by applicant]
US 3761027A · Mendoza · 1973 [cited by applicant]
US 4056636A · Muller · 1977 [cited by applicant]
US 4361651A · Keim · 1982 [cited by applicant]
US 4565330A · Katoh · 1986 [cited by applicant]
US 5195684A · Radzins · 1993 [cited by applicant]
US 5250182A · Bento et al. · 1993 [cited by applicant]
US 5662810A · Willgohs · 1997 [cited by applicant]
US 5795477A · Herman et al. · 1998 [cited by applicant]
US 6106673A · Walker · 2000 [cited by applicant]
US 6117321A · Johnston · 2000 [cited by applicant]
US 6230995B1 · Niemi et al. · 2001 [cited by applicant]
US 6475132B2 · Zettier · 2002 [cited by applicant]
US 6509180B1 · Verser et al. · 2003 [cited by applicant]
US 6962722B2 · Dawley et al. · 2005 [cited by applicant]
US 7083954B2 · Jakel et al. · 2006 [cited by applicant]
US 7101691B2 · Kinley et al. · 2006 [cited by applicant]
US 7300680B2 · Prevost et al. · 2007 [cited by applicant]
US 7384010B2 · Horigane et al. · 2008 [cited by applicant]
US 7497955B2 · Scheimann et al. · 2009 [cited by applicant]
US 7507562B2 · Verser et al. · 2009 [cited by applicant]
US 7572353B1 · Vander Griend · 2009 [cited by applicant]
US 7601858B2 · Cantrell et al. · 2009 [cited by applicant]
US 7608729B2 · Winsness et al. · 2009 [cited by applicant]
US 7699255B2 · Kapper · 2010 [cited by applicant]
US 7829680B1 · Sander et al. · 2010 [cited by applicant]
US 7842484B2 · Lewis · 2010 [cited by applicant]
US 7857608B2 · Fabbricante et al. · 2010 [cited by applicant]
US 7858140B2 · Paustian et al. · 2010 [cited by applicant]
US 7886996B2 · Horigane et al. · 2011 [cited by applicant]
US 7888082B2 · Verser et al. · 2011 [cited by applicant]
US 7915458B2 · Bruckmayer · 2011 [cited by applicant]
US 7919289B2 · Lewis · 2011 [cited by applicant]
US 7935370B1 · Prevost et al. · 2011 [cited by applicant]
US 7954734B2 · Hata · 2011 [cited by applicant]
US 8017365B1 · Rein et al. · 2011 [cited by applicant]
US 8093023B1 · Prevost et al. · 2012 [cited by applicant]
US 8103385B2 · Macharia et al. · 2012 [cited by applicant]
US 8126606B2 · Hung · 2012 [cited by applicant]
US 8168037B2 · Winsness · 2012 [cited by applicant]
US 8192627B2 · Gallop et al. · 2012 [cited by applicant]
US 8236086B2 · Janssen et al. · 2012 [cited by applicant]
US 8236977B2 · Woods et al. · 2012 [cited by applicant]
US 8257951B2 · Prevost et al. · 2012 [cited by applicant]
US 8449728B2 · Redford · 2013 [cited by applicant]
US 8454802B2 · Redford · 2013 [cited by applicant]
US 8524473B2 · Hammond et al. · 2013 [cited by applicant]
US 8563282B2 · Galvez, III et al. · 2013 [cited by applicant]
US 8597917B2 · Medoff et al. · 2013 [cited by applicant]
US 8603786B2 · Redford · 2013 [cited by applicant]
US 8679353B2 · Winsness · 2014 [cited by applicant]
US 8702819B2 · Bootsma · 2014 [cited by applicant]
US 8722372B2 · Kiuchi et al. · 2014 [cited by applicant]
US 8722911B2 · Bleyer et al. · 2014 [cited by applicant]
US 8735544B1 · Prevost et al. · 2014 [cited by applicant]
US 8748141B2 · Lewis et al. · 2014 [cited by applicant]
US 8778433B2 · Lee · 2014 [cited by applicant]
US 8813973B2 · Lee et al. · 2014 [cited by applicant]
US 8927239B2 · Allen et al. · 2015 [cited by applicant]
US 8956460B2 · Ahmed et al. · 2015 [cited by applicant]
US 8962059B1 · Froderman et al. · 2015 [cited by applicant]
US 8986551B2 · Kohl et al. · 2015 [cited by applicant]
US 9012191B2 · Lee · 2015 [cited by applicant]
US 9012668B2 · Winsness · 2015 [cited by applicant]
US 9029126B2 · Bleyer et al. · 2015 [cited by applicant]
US 9040270B2 · Prevost et al. · 2015 [cited by applicant]
US 9061987B2 · Bootsma · 2015 [cited by applicant]
US 9108140B2 · Winsness · 2015 [cited by applicant]
US 9114114B2 · Anderson et al. · 2015 [cited by applicant]
US 9150790B2 · Thorn et al. · 2015 [cited by applicant]
US 9169498B2 · Woods et al. · 2015 [cited by applicant]
US 9212334B2 · Cantrell et al. · 2015 [cited by applicant]
US 9290728B2 · Bootsma · 2016 [cited by applicant]
US 9320990B2 · Winsness · 2016 [cited by applicant]
US 9328311B2 · Jenkins et al. · 2016 [cited by applicant]
US 9340767B2 · Narendranath · 2016 [cited by applicant]
US 9353332B2 · Lewis et al. · 2016 [cited by applicant]
US 9375731B2 · Dieker et al. · 2016 [cited by applicant]
US 9376504B2 · Dieker et al. · 2016 [cited by applicant]
US 9388475B2 · Lee · 2016 [cited by applicant]
US 9516891B1 · Roa-Espinosa · 2016 [cited by applicant]
US 9631161B2 · Sungail et al. · 2017 [cited by applicant]
US 9695381B2 · Lee · 2017 [cited by applicant]
US 9714267B2 · Emanuele et al. · 2017 [cited by applicant]
US 9718006B2 · Lee et al. · 2017 [cited by applicant]
US 9730463B1 · Roa-Espinosa · 2017 [cited by applicant]
US 9745540B2 · Sungail et al. · 2017 [cited by applicant]
US 9896643B2 · Redford · 2018 [cited by applicant]
US 9963671B2 · Williams et al. · 2018 [cited by applicant]
US 10059966B2 · Bootsma · 2018 [cited by applicant]
US 10093891B2 · Kohl et al. · 2018 [cited by applicant]
US 10113007B2 · Kohl · 2018 [cited by applicant]
US 10214559B2 · Modinger et al. · 2019 [cited by applicant]
US 10226774B2 · Franko · 2019 [cited by applicant]
US 10260031B2 · Gallop et al. · 2019 [cited by applicant]
US 10400201B2 · Yu · 2019 [cited by applicant]
US 10449469B2 · Lewis · 2019 [cited by applicant]
US 10465152B2 · Bootsma · 2019 [cited by applicant]
US 10683479B2 · Lucas · 2020 [cited by applicant]
US 10745643B2 · Gallop et al. · 2020 [cited by applicant]
US 10774303B2 · Dieker et al. · 2020 [cited by applicant]
US 10837029B2 · Bootsma · 2020 [cited by applicant]
US 10851327B2 · Urban et al. · 2020 [cited by applicant]
US 10875889B2 · Jakel · 2020 [cited by applicant]
US 10926267B2 · Hora et al. · 2021 [cited by applicant]
US 11028378B2 · Jump et al. · 2021 [cited by applicant]
US 11078500B2 · Hansen et al. · 2021 [cited by applicant]
US 11104873B2 · Bootsma · 2021 [cited by applicant]
US 11166478B2 · Lee · 2021 [cited by applicant]
US 11248197B2 · Bootsma · 2022 [cited by examiner]
US 11254955B2 · Bootsma · 2022 [cited by examiner]
US 11266166B2 · Gallop et al. · 2022 [cited by applicant]
US 11273455B2 · Xu · 2022 [cited by applicant]
US 11286509B2 · Bootsma · 2022 [cited by examiner]
US 11337442B2 · Lecocq et al. · 2022 [cited by applicant]
US 11485990B2 · Pohl et al. · 2022 [cited by applicant]
US 11713474B2 · Bootsma · 2023 [cited by examiner]
US 11718863B2 · Bootsma · 2023 [cited by examiner]
US 11730172B2 · Rindsig et al. · 2023 [cited by applicant]
US 11739352B1 · Carlson et al. · 2023 [cited by applicant]
US 20040087808A1 · Prevost et al. · 2004 [cited by applicant]
US 20040192896A1 · Finch · 2004 [cited by applicant]
US 20040234649A1 · Lewis et al. · 2004 [cited by applicant]
US 20050233030A1 · Lewis et al. · 2005 [cited by applicant]
US 20050239181A1 · Lewis et al. · 2005 [cited by applicant]
US 20060194296A1 · Hammond et al. · 2006 [cited by applicant]
US 20070031953A1 · Dunson, Jr. et al. · 2007 [cited by applicant]
US 20070036881A1 · Griffith · 2007 [cited by applicant]
US 20070141691A1 · Hirl · 2007 [cited by applicant]
US 20070148318A1 · Rubio et al. · 2007 [cited by applicant]
US 20070190626A1 · Wilkening et al. · 2007 [cited by applicant]
US 20070238691A1 · Thompson et al. · 2007 [cited by applicant]
US 20070254089A1 · Hickey et al. · 2007 [cited by applicant]
US 20080009048A1 · Bhargava et al. · 2008 [cited by applicant]
US 20080110577A1 · Winsness · 2008 [cited by applicant]
US 20080193991A1 · Allen et al. · 2008 [cited by applicant]
US 20080277264A1 · Sprague · 2008 [cited by applicant]
US 20090093027A1 · Balan et al. · 2009 [cited by applicant]
US 20090176289A1 · Friedmann · 2009 [cited by applicant]
US 20090250412A1 · Winsness et al. · 2009 [cited by applicant]
US 20090269817A1 · Lantero · 2009 [cited by applicant]
US 20090311397A1 · Whalen et al. · 2009 [cited by applicant]
US 20100055741A1 · Galvez, III · 2010 [cited by examiner]
US 20100159519A1 · Diner et al. · 2010 [cited by applicant]
US 20100199062A1 · Sancho-Dominguez et al. · 2010 [cited by applicant]
US 20100221804A1 · Veit et al. · 2010 [cited by applicant]
US 20100281765A1 · Schwartz · 2010 [cited by applicant]
US 20110003341A1 · Nojiri et al. · 2011 [cited by applicant]
US 20110086149A1 · Bootsma · 2011 [cited by applicant]
US 20110142788A1 · Sellier et al. · 2011 [cited by applicant]
US 20110143411A1 · Yuan et al. · 2011 [cited by applicant]
US 20120051980A1 · Gallop et al. · 2012 [cited by applicant]
US 20120064213A1 · Lee · 2012 [cited by examiner]
US 20120244590A1 · Lee · 2012 [cited by applicant]
US 20130165678A1 · Kohl et al. · 2013 [cited by applicant]
US 20130295661A1 · Roesch et al. · 2013 [cited by applicant]
US 20140024084A1 · Galvez, III et al. · 2014 [cited by applicant]
US 20140110512A1 · Lee · 2014 [cited by applicant]
US 20140155639A1 · Sticklen et al. · 2014 [cited by applicant]
US 20140178946A1 · Galvez, III et al. · 2014 [cited by applicant]
US 20140242251A1 · Bootsma · 2014 [cited by examiner]
US 20140273166A1 · Narendranath · 2014 [cited by applicant]
US 20140315259A1 · Woods · 2014 [cited by applicant]
US 20150024451A1 · Williams · 2015 [cited by applicant]
US 20150037857A1 · Redford · 2015 [cited by applicant]
US 20150056327A1 · Redford · 2015 [cited by applicant]
US 20150076078A1 · Gallop · 2015 [cited by applicant]
US 20150118727A1 · Escudero et al. · 2015 [cited by applicant]
US 20150147786A1 · Clarkson et al. · 2015 [cited by applicant]
US 20150152196A1 · Phanopoulos et al. · 2015 [cited by applicant]
US 20150152372A1 · Kohl et al. · 2015 [cited by applicant]
US 20150181911A1 · Redford · 2015 [cited by applicant]
US 20150181912A1 · Redford · 2015 [cited by applicant]
US 20150182882A1 · Gallop et al. · 2015 [cited by applicant]
US 20150299645A1 · Williams · 2015 [cited by applicant]
US 20160024406A1 · Javers et al. · 2016 [cited by applicant]
US 20160145650A1 · Lewis et al. · 2016 [cited by applicant]
US 20160222135A1 · Lee · 2016 [cited by applicant]
US 20170051322A1 · Bushong et al. · 2017 [cited by applicant]
US 20170107452A1 · Dasari et al. · 2017 [cited by applicant]
US 20170114293A1 · Jakel et al. · 2017 [cited by applicant]
US 20170166834A1 · Jakel · 2017 [cited by applicant]
US 20170166835A1 · Jakel · 2017 [cited by applicant]
US 20170226165A1 · Franko et al. · 2017 [cited by applicant]
US 20170253892A1 · Bootsma · 2017 [cited by applicant]
US 20170268024A1 · Bootsma et al. · 2017 [cited by applicant]
US 20180016602A1 · Franko et al. · 2018 [cited by applicant]
US 20180126302A1 · Gallop · 2018 [cited by applicant]
US 20180242626A1 · Froderman et al. · 2018 [cited by applicant]
US 20180355387A1 · Javers et al. · 2018 [cited by applicant]
US 20190119711A1 · Lee · 2019 [cited by applicant]
US 20190160470A1 · Hora et al. · 2019 [cited by applicant]
US 20190374883A1 · Gallop et al. · 2019 [cited by applicant]
US 20200113209A1 · Gallop et al. · 2020 [cited by applicant]
US 20200128855A1 · Gallop et al. · 2020 [cited by applicant]
US 20200139269A1 · Gallop et al. · 2020 [cited by applicant]
US 20200199062A1 · Franko et al. · 2020 [cited by applicant]
US 20200359657A1 · Gallop et al. · 2020 [cited by applicant]
US 20210002686A1 · Pohl et al. · 2021 [cited by applicant]
US 20210062122A1 · Franko et al. · 2021 [cited by applicant]
US 20210251256A1 · Gibbons et al. · 2021 [cited by applicant]
US 20220002762A1 · Botella-Franco et al. · 2022 [cited by applicant]
US 20220142200A1 · Gibbons et al. · 2022 [cited by applicant]
US 20220151260A1 · Janow et al. · 2022 [cited by applicant]
US 20220154114A1 · Bootsma · 2022 [cited by applicant]
US 20220186266A1 · Kreel · 2022 [cited by applicant]
US 20220298532A1 · Pal et al. · 2022 [cited by applicant]
US 20240263110A1 · Bootsma · 2024 [cited by applicant]
AU 2833395A · 1996 [cited by applicant]
EP 3831915A1 · 2021 [cited by applicant]
WO WO2005029974A1 · 2005 [cited by applicant]
WO WO2017059083A1 · 2017 [cited by applicant]
WO WO2017091760A1 · 2017 [cited by applicant]
WO WO2017091766A1 · 2017 [cited by applicant]
WO WO2018215965A1 · 2018 [cited by applicant]
WO WO2018217202A1 · 2018 [cited by applicant]
WO WO2018231371A1 · 2018 [cited by applicant]
WO WO2019226703A1 · 2019 [cited by applicant]
WO WO2019226704A1 · 2019 [cited by applicant]
WO WO2019226707A1 · 2019 [cited by applicant]
WO WO2020109268A1 · 2020 [cited by applicant]
WO WO2020178184A1 · 2020 [cited by applicant]
WO WO2020206058A1 · 2020 [cited by applicant]
WO WO2020261291A1 · 2020 [cited by applicant]
WO WO2021026201A1 · 2021 [cited by applicant]
A Lecture on Pressure Screening, James A. Olson, Mechanical Engineering Department, University of British Columbia, Aug. 21, 2003. [cited by applicant]
Abdel-Tawwab et al., “Evaluation of commercial live bakers' yeast, [cited by applicant]
About Harvesting Technology: Bringing Profitable Innovation for Ethanol Production, retrieved on Jun. 26, 2018 via http:/harvestingtech.com/#benefils, (11 pages). [cited by applicant]
Akinoso, R., et al. “Work Index and Milling Efficiency of Size Reduction of Maize Using Plate Mill”, Agricultural Engineering today, vol. 36, pp. 22-28, 2012. {Abstract). [cited by applicant]
Ankom, “Acid Detergent Fiber in Feeds—Filter Bag Technique (for A2000 and A2000I)”, ADF method, pp. 1-2, 2017. [cited by applicant]
AOAC International “AOAC 965.22-1966”, pp. 1, 1996. [cited by applicant]
Benedetti, A., et al., “X-ray diffraction methods to determine crystallinity and preferred orientation of lithium disilicate n Li—Zn-silicate glass-ceramic fibres”, Journal of Materials Science, vol. 18, pp. 1039-1048, … [cited by applicant]
Chatzifragkou et al., “Biorefinery strategies for upgrading distillers' dried grains with solubles (DOGS)”, Process Biochemistry, vol. 50, 2015, pp. 2194-2207. [cited by applicant]
Cheetham, et al., Variation in crystalline type with amylase content in maize starch granules: an X-ray powder diffraction study, Carbohydrate Polymers, vol. 36, pp. 277-284, 1998. [cited by applicant]
Disc Mill DM 400-Retsch, Powerful grinding and robust design, Aug. 19, 2015. [cited by applicant]
Ethanol Producers Talk Shop, pp. 1-3, Ron Kotrba, Aug. 1, 2006. [cited by applicant]
Flash Dryer, retrieved from https://www.gea.com/en/products/dryers-particle-processing/flash-dryers-coolers/flash-dryer.jsp, on Jun. 9, 2020, (11 pages). [cited by applicant]
“Flottweg Separation Technology,” Web page <https://www.flottweg.com/fileadmin/user_upload/data/pdf-downloads/Sedicanter-EN.pdf>, 12 pages, Aug. 10, 2016, retrieved from Internet Archive Wayback Machine<https://web.arch… [cited by applicant]
Fluid Quip-Ethanol Industry, Corn Wet Milling Process Description, website pp. 1-6, Aug. 19, 2015. [cited by applicant]
Hames, B., et al., “Determination of Protein Content in Biomass”, National Renewable Energy Laboratory, pp. 1-8, 2008. [cited by applicant]
Hunt, et al. “Corn Stillage as a Feedstuff for Broilers and Turkeys”, Applied Poultry Science, Inc., Research Report 1997, published online at http://japr.fass.org/contenl/6/3/310.full.pdf, (9 pages). [cited by applicant]
International Standard, IS013320, Particle size analysis-Laser diffraction methods, pp. 1-58, 2009. [cited by applicant]
Jakel, “Product Diversification: Proven Path Forward”, presented at the ACE conference which was held Aug. 15-17, 2017 in Omaha NE, (71 pages). [cited by applicant]
Kim et al., “Composition of corn dry-grind ethanol by-products: DDGS, wet cake, and thin stillage”, Science Direct, Bioresource Technology, vol. 99, pp. 5165-5176, 2008, (12 pages). [cited by applicant]
Kim et al., “Process simulation of modified dry grind ethanol plant with recycle of pretreated and enzymatically hydrolyzed distillers' grains”, Bioresource Technology, vol. 99, 2008, pp. 5177-5192. [cited by applicant]
Li, “Enzymes for Cellular Lysis or Protoplast Formation: Bacteria, Yeasts, and Plant”, published at https://cellculturedish.com/experts/shanghao-li/, A guest post by Shanghao Li, Ph.D. is Global Product Manager of Immun… [cited by applicant]
Nara, S., et al., “Studies on the Relationship Between Water-satured State and Crystallinity by the Diffraction Method or Moistened Potato Starch”, starch, vol. 35, Issue 12, pp. 407-410, 1983. (Abstract). [cited by applicant]
Nouroddini et al., “Stagewise Dilute-Acid Pretreatment and Enzyme Hydrolysis of Distillers' Grains and Com Fiber”, Appl Biochem Biotech, 159, pp. 553-567, 2009. [cited by applicant]
Particle Size Distributions of Ground Com and DDGS from Dry Grind Processing, Rausch et al., Transactions of the ASAE, vol. 48(1), pp. 273-277, 2005. [cited by applicant]
Pleasant Hill Grain, website catalog pp. 1-8, ABC Hansen Disc Mill, Aug. 9, 2015. [cited by applicant]
Rausch et al., “The Future of Coproducts From Corn Processing”, Applied Biochemistry and Biotechnology, vol. 128, pp. 47-86, 2006, (40 pages). [cited by applicant]
Ring Dryer, retrieved from https://www.gea.com/en/products/dryers-particle-processing/ring-dryers/ring-dryer.jsp, on Jun. 9, 2020, (12 pages). [cited by applicant]
Robert, “Industrial Glucose: Bridging the Biochemical GAP”, presented at the Renewable Chemicals Summit which was held Apr. 3-5, 2019 in Washington, DC, (20 pages). [cited by applicant]
Rosentrater, “Production and use of evolving corn-based fuel ethanol coproducts in the U.S” In: Biernat Editor): 11 Biofuels—Status and perspective, 2015, pp. 81-98. [cited by applicant]
Sluiter, A., et al., “Determination of Ash in Biomass”, National Renewable Energy Laboratory, pp. 1-8, 2005. [cited by applicant]
Sluiter, A., et al., “Determination of Extractives in Biomass”, National Renewable Energy Laboratory, pp. 1-12, 2005. [cited by applicant]
Sluiter, A., et al., “Determination of starch in solid biomass samples”, National Renewable Energy Laboratory, pp. 1-7, 2005. (Abstract). [cited by applicant]
Sluiter, A., et al., “Determination of Structural Carbohydrates and Lignin in Biomass”, National Renewable Energy Laboratory, pp. 1-18, 2012. [cited by applicant]
Sluiter, A., et al., “Determination of Total Solids in Biomass and Total Dissolved Solids in Liquid Process Samples”, National Renewable Energy Laboratory, pp. 1-9, 2008. [cited by applicant]
Svonja, “From Operating Ease to Operating Costs: Weighing Differences in DDGS Dryers”, retrieved from http://ethanolproducer.com/articles/3032/from-operating-ease-to-operating-costs-weighing-differences-in-ddgs-dryers, … [cited by applicant]
Thin Stillage Solids Separation System, retrieved on Jun. 26, 2018 via http://www.icminc.com/products/lhin-stillagesolids separation-system.html, (2 pages). [cited by applicant]
Wongsagonsup et al., “Effects of different mill types on ethanol production using uncooked dry-grind fermentation and characteristics of residual starch in distiller's dried grains (DOG)”, Cereal Chemistry, vol. 94, Feb… [cited by applicant]
Yamada et al., “Yeast ( [cited by applicant]
PCT/US2016/063657 International Search Report and Written Opinion, Feb. 7, 2017. [cited by applicant]
International Preliminary Report on Patentability Chapter I of the PCT that issued Jun. 7, 2018 in PCT/US2016/063657. [cited by applicant]
PCT/US2016/063666 International Search Report and Written Opinion, Mar. 27, 2017. [cited by applicant]
International Preliminary Report on Patentability Chapter I that issued Jun. 7, 2018 in PCT/US2016/063666. [cited by applicant]
International Search Report and Written Opinion received for PCT application No. PCT/US2017/034324, mailed on Aug. 14, 2017, 8 pages. [cited by applicant]
International Preliminary Report on Patentability Chapter I of the PCT that issued Dec. 5, 2019 in PCT/US2017/034324. [cited by applicant]
PCT/IB2018/053688, International Search Report and Written Opinion, Aug. 21, 2018. [cited by applicant]
International Preliminary Report on Patentability Chapter I of the PCT that issued Dec. 5, 2019 in PCT/IB2018/053688. [cited by applicant]
Rindsig et al., Utility U.S. Appl. No. 18/216,939, filed Jun. 30, 2023 (no attachment). [cited by applicant]