IP Library › Granted Patent US 12,259,656
Granted Patent B1
US 12,259,656 · App. 17/951,306 · Granted Mar 25, 2025

Method of fabricating structured membranes

Inventors: Elissa Williams (Greenbelt, MD); Kevin Denis (Crofton, MD); Hsiang-Yu Liu (Lanham, MD)
Assignee: United States of America as represented by the Administrator of NASA
G03F7/343G03F7/36B81C1/00531
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Quick Facts
Patent No.
US 12,259,656
App. No.
17/951,306
Granted
Mar 25, 2025
Kind
B1
Abstract

A structured membrane fabrication method begins with a membrane wafer on a substrate and at least one thin-film on the membrane wafer such that portions of the membrane wafer are exposed. The exposed portions of the membrane wafer and each thin-film are covered with an acetone-inert protectant. Portions of the protectant are etched through to the membrane wafer while each thin-film remains fully covered by the protectant. A handle is coupled to the protectant with a wax that dissolves in acetone. Portions of the substrate are then removed to define and expose a contiguous region of the membrane wafer adjacent to each thin-film and the portions of the protectant so-etched. The wax is exposed to acetone so that it dissolves. The contiguous region of the membrane wafer is then etched through at the portions of the protectant so-etched. The protectant is then removed.

Claims (51)

1. A method comprising the steps of:

providing a membrane wafer on a substrate;

providing at least one thin-film on said membrane wafer wherein portions of said membrane wafer are exposed;

covering said portions of said membrane wafer and each said thin-film with a protectant that is inert in acetone;

etching portions of said protectant through to said membrane wafer, wherein each said thin-film remains fully covered by said protectant;

coupling a handle to said protectant with a wax that dissolves in acetone;

removing portions of said substrate wherein a contiguous region of said membrane wafer is defined and exposed adjacent to each said thin-film and said portions of said protectant so-etched;

exposing said wax to acetone wherein said wax dissolves and said handle is uncoupled from said protectant;

etching through said contiguous region of said membrane wafer at said portions of said protectant so-etched; and

removing said protectant.

2. A method according to claim 1 , wherein said step of etching portions of said protectant comprises a plasma etching process.

3. A method according to claim 1 , wherein said step of removing portions of said substrate from is selected from the group consisting of ion etching processes, plasma etching processes, and wet etching processes.

4. A method according to claim 1 , wherein said step of etching through said contiguous region comprises an ion etching process.

5. A method according to claim 1 , wherein said step of removing said protectant comprises a plasma etching process.

6. A method according to claim 1 , wherein said membrane is selected from the group consisting of silicon, silicon oxide, silicon nitride, aluminum oxide, aluminum nitride, diamond, and combinations thereof.

7. A method according to claim 1 , wherein said thin-film is selected from the group consisting of metals and non-metals.

8. A method according to claim 1 , wherein said protectant comprises an anti-reflective coating.

9. A method according to claim 1 , wherein said handle comprises an optically-transparent glass.

10. A method comprising the steps of:

providing a membrane wafer on a substrate;

providing at least one metal film on said membrane wafer wherein portions of said membrane wafer are exposed;

covering said portions of said membrane wafer and each said metal film with a protectant that is inert in acetone;

etching portions of said protectant through to said membrane wafer, wherein each said metal film remains fully covered by said protectant;

covering said protectant with a wax that dissolves in acetone;

coupling an optically-transparent glass handle to said wax;

removing portions of said substrate wherein a contiguous region of said membrane wafer is defined and exposed adjacent to each said metal film and said portions of said protectant so-etched;

exposing said wax to acetone, wherein said wax dissolves and wherein said protectant is exposed;

etching through said contiguous region of said membrane wafer at said portions of said protectant so-etched; and

removing said protectant.

11. A method according to claim 10 , wherein said step of etching portions of said protectant comprises a plasma etching process.

12. A method according to claim 10 , wherein said step of removing portions of said substrate is selected from the group consisting of ion etching processes, plasma etching processes, and wet etching processes.

13. A method according to claim 10 , wherein said step of etching through said contiguous region comprises an ion etching process.

14. A method according to claim 10 , wherein said step of removing said protectant comprises a plasma etching process.

15. A method according to claim 10 , wherein said membrane is selected from the group consisting of silicon, silicon oxide, silicon nitride, aluminum oxide, aluminum nitride, diamond, and combinations thereof.

16. A method according to claim 10 , wherein said protectant comprises an anti-reflective coating.

17. A method comprising the steps of:

providing a membrane wafer on a substrate;

providing at least one metal film on said membrane wafer wherein portions of said membrane wafer are exposed;

covering said portions of said membrane wafer and each said metal film with an anti-reflective coating that is inert in acetone;

etching portions of said anti-reflective coating through to said membrane wafer, wherein each said metal film remains fully covered by said anti-reflective coating;

coupling a handle to said anti-reflective coating using a wax that dissolves in acetone;

removing portions of said substrate wherein a contiguous region of said membrane wafer is defined and exposed adjacent to each said metal film and said portions of said anti-reflective coating so-etched;

exposing said wax to acetone wherein said wax dissolves and said handle is uncoupled from said anti-reflective coating;

etching through said contiguous region of said membrane wafer at said portions of said anti-reflective coating so-etched; and

removing said anti-reflective coating.

18. A method according to claim 17 , wherein said step of etching portions of said anti-reflective coating comprises a plasma etching process.

19. A method according to claim 17 , wherein said step of removing portions of said substrate is selected from the group consisting of ion etching processes, plasma etching processes, and wet etching processes.

20. A method according to claim 17 , wherein said step of etching through said contiguous region comprises an ion etching process.

21. A method according to claim 17 , wherein said step of removing said anti-reflective coating comprises a plasma etching process.

22. A method according to claim 17 , wherein said membrane is selected from the group consisting of silicon, silicon oxide, silicon nitride, aluminum oxide, aluminum nitride, diamond, and combinations thereof.

23. A method according to claim 17 , wherein said handle comprises an optically-transparent glass.

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