IP Library Granted Patent US 12,655,057
Granted Patent B2
US 12,655,057 · App. 19/341,229 · Granted Jun 16, 2026

Glass-ceramic articles with increased resistance to fracture and methods for making the same

Inventors: Carol Ann Click (Corning, NY); Indrajit Dutta (Horseheads, NY); James Howard Edmonston (Durham, NC); Michael S Fischer (Brockport, NY); Qiang Fu (Painted Post, NY); Ozgur Gulbiten (Painted Post, NY); Jill Marie Hall (Elmira, NY); Mathieu Gerard Jacques Hubert (Corning, NY); Dhananjay Joshi (Rockville, MD); Andrew Peter Kittleson (Honeoye Falls, NY); Rohit Rai (Lexington, MA); John Robert Saltzer, Jr. (Beaver Dams, NY); Charlene Marie Smith (Corning, NY); Matthew Daniel Trosa (Horseheads, NY); Matthew Artus Tuggle (Seattle, WA); James Clark Walck, Jr. (Sayre, PA); Alana Marie Whittier (Painted Post, NY); Zheming Zheng (Horseheads, NY)
Assignee: CORNING INCORPORATED
C03C10/0036C03B32/02C03C4/0092C03C10/0027C03C3/097C03C10/0054C03C21/002C03C2203/52C03C2214/20
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Quick Facts
Patent No.
US 12,655,057
App. No.
19/341,229
Granted
Jun 16, 2026
Kind
B2
Abstract

A glass-ceramic article having one or more crystalline phases; a residual glass phase; a compressive stress layer extending from a first surface to a depth of compression (DOC); a maximum central tension greater than 70 MPa; a stored tensile energy greater than 22 J/m 2 ; a fracture toughness greater than 1.0 MPa√m; and a haze less than 0.2.

Claims (58)

1 . A glass-ceramic article, comprising:

a residual glass phase that is less than or equal to 50 wt % of the glass-ceramic article;

a composition of the glass-ceramic article, based on 100 mol % of the glass-ceramic article, comprising:

greater than or equal to 1.7 mol % ZrO 2 ;

from 60 mol % to 72 mol % SiO 2 ;

from 0 mol % to 6 mol % Al 2 O 3 ;

from 24 mol % to 32 mol % Li 2 O;

from 0 mol % to 2 mol % B 2 O 3 ;

from 0 mol % to 2 mol % Na 2 O; and

from 0 mol % to 2 mol % K 2 O,

wherein the glass-ceramic article comprises a molar ratio Li 2 O (mol %)/R 2 O (mol %) from greater than or equal to 0.85 to less than or equal to 1.00, where R 2 O is a total amount of Li 2 O, Na 2 O, and K 2 O;

a first surface of the glass-ceramic article; and

a compressive stress layer extending from the first surface of the glass-ceramic article to a depth of compression,

wherein the glass-ceramic article has a maximum central tension greater than 90 MPa.

2 . The glass-ceramic article of claim 1 , further comprising a stored tensile energy greater than 22 J/m 2 .

3 . The glass-ceramic article of claim 2 , wherein the stored tensile energy is no more than 100 J/m 2 .

4 . The glass-ceramic article of claim 3 , wherein the depth of compression is at least 0.05 mm and no more than 0.6 mm.

5 . The glass-ceramic article of claim 4 , further comprising a thickness of the glass-ceramic article, wherein the thickness is at least 0.2 mm and no more than 4 mm.

6 . The glass-ceramic article of claim 5 , wherein the ZrO 2 is greater than or equal to 1.7 mol % and less than or equal to 4.5 mol % ZrO 2 .

7 . The glass-ceramic article of claim 6 , wherein the molar ratio Li 2 O (mol %)/R 2 O (mol %) is from greater than or equal to 0.95 to less than or equal to 0.99.

8 . The glass-ceramic article of claim 7 , further comprising P 2 O 5 from 0.7 mol % to 2.2 mol %.

9 . The glass-ceramic article of claim 1 , further comprising a haze less than 0.2.

10 . The glass-ceramic article of claim 9 , further comprising a fracture toughness greater than 1.0 MPa√m.

11 . The glass-ceramic article of claim 1 , wherein the haze is less than 0.18.

12 . The glass-ceramic article of claim 1 , further comprising average transmittance of the glass-ceramic article at or exceeding 85% per mm over a wavelength range from 450 nm to 600 nm, including surface reflection losses of light.

13 . The glass-ceramic article of claim 1 , wherein the composition comprises from 65 mol % to 72 mol % SiO 2 .

14 . A glass-ceramic article, comprising:

a residual glass phase that is less than or equal to 50 wt % of the glass-ceramic article;

a composition of the glass-ceramic article, based on 100 mol % of the glass-ceramic article, comprising:

greater than or equal to 1.7 mol % ZrO 2 ;

from 60 mol % to 72 mol % SiO 2 ;

from 0 mol % to 6 mol % Al 2 O 3 ;

from 24 mol % to 32 mol % Li 2 O;

from 0 mol % to 2 mol % B 2 O 3 ;

from 0 mol % to 2 mol % Na 2 O; and

from 0 mol % to 2 mol % K 2 O,

wherein the glass-ceramic article comprises a molar ratio Li 2 O (mol %)/R 2 O (mol %) from greater than or equal to 0.85 to less than or equal to 1.00, where R 2 O is a total amount of Li 2 O, Na 2 O, and K 2 O;

a first surface of the glass-ceramic article;

a compressive stress layer extending from the first surface of the glass-ceramic article to a depth of compression; and

a stored tensile energy greater than 22 J/m 2 .

15 . The glass-ceramic article of claim 14 , wherein the stored tensile energy is no more than 100 J/m 2 .

16 . The glass-ceramic article of claim 14 , further comprising a haze less than 0.2.

17 . A glass-ceramic article, comprising:

a residual glass phase that is less than or equal to 50 wt % of the glass-ceramic article;

a composition of the glass-ceramic article, based on 100 mol % of the glass-ceramic article, comprising:

greater than or equal to 1.7 mol % ZrO 2 ;

from 60 mol % to 72 mol % SiO 2 ;

from 0 mol % to 6 mol % Al 2 O 3 ;

from 24 mol % to 32 mol % Li 2 O;

from 0 mol % to 2 mol % B 2 O 3 ;

from 0 mol % to 2 mol % Na 2 O; and

from 0 mol % to 2 mol % K 2 O,

wherein the glass-ceramic article comprises a molar ratio Li 2 O (mol %)/R 2 O (mol %) from greater than or equal to 0.85 to less than or equal to 1.00, where R 2 O is a total amount of Li 2 O, Na 2 O, and K 2 O;

a first surface of the glass-ceramic article;

optical retardance at room temperature of less than 40 nm per mm of thickness measured using a grey-field polariscope GFP-1400 photoelastic stress measurement system.

18 . The glass-ceramic article of claim 17 , further comprising a first surface of the glass-ceramic article, and a compressive stress layer extending from the first surface of the glass-ceramic article to a depth of compression, wherein the depth of compression is at least 0.05 mm and no more than 0.6 mm.

19 . The glass-ceramic article of claim 18 , further comprising a thickness of the glass-ceramic article, wherein the thickness is at least 0.2 mm and no more than 4 mm.

20 . The glass-ceramic article of claim 19 , further comprising a stored tensile energy greater than 22 J/m 2 ; and a haze less than 0.2.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 26, 2025
From: CLICK, CAROL ANN; DUTTA, INDRAJIT; EDMONSTON, JAMES HOWARD; FISCHER, MICHAEL S; FU, QIANG; GULBITEN, OZGUR; HALL, JILL MARIE; HUBERT, MATHIEU GERARD JACQUES; JOSHI, DHANANJAY; KITTLESON, ANDREW PETER; RAI, ROHIT; SALTZER, JOHN ROBERT, JR.; SMITH, CHARLENE MARIE; TROSA, MATTHEW DANIEL; TUGGLE, MATTHEW ARTUS; WALCK, JAMES CLARK, JR.; WHITTIER, ALANA MARIE; ZHENG, ZHEMING
To: CORNING INCORPORATED
Reel/Frame 072388/0401 →
Continuity (4)
Continuation 16512953 · Jul 16, 2019
Provisional Application 62736682 · Sep 26, 2018
Provisional Application 62698532 · Jul 16, 2018
Related Publication 20260022057A1 · Jan 22, 2026
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