IP Library Granted Patent US 12,266,733
Granted Patent B2
US 12,266,733 · App. 18/219,821 · Granted Apr 1, 2025

Methods for growing doped cesium lead halides

Inventors: Mercouri G. Kanatzidis (Wilmette, IL); Yihui He (Evanston, IL)
Assignee: Northwestern University
H01L31/085C30B11/003C30B29/12G01T1/24H01L31/0224H01L31/032
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Quick Facts
Patent No.
US 12,266,733
App. No.
18/219,821
Granted
Apr 1, 2025
Kind
B2
Abstract

Methods and devices for detecting incident radiation are provided. The methods and devices use high quality single-crystals of photoactive semiconductor compounds in combination with metal anodes and metal cathodes that provide for enhanced photodetector performance.

Claims (15)

1. A method of growing a doped CsPbX 3 single crystal, the method comprising:

forming a melt comprising CsX, PbX 2 , where X is Br or Cl, and a doping species comprising a dopant element from Group 13 or Group 17 of the periodic table; and

growing crystalline doped CsPbX 3 from the melt via vertical Bridgman growth.

2. The method of claim 1 , wherein X is Br.

3. The method of claim 2 , wherein the dopant species comprises PbI 2 or PbCl 2 .

4. The method of claim 2 , wherein the dopant species comprises TlBr.

5. The method of claim 2 , wherein the dopant species comprises Pb.

6. The method of claim 1 , wherein X is Cl.

7. The method of claim 6 , wherein the dopant species comprises PbBr 2 .

8. A method of growing a doped CsPbX 3 single crystal, the method comprising:

forming a melt comprising CsX, PbX 2 , where X is Br or Cl, and a doping species comprising Se; and

growing crystalline doped CsPbX 3 from the melt via vertical Bridgman growth.

9. A method of growing a doped CsPbX 3 single crystal, the method comprising:

forming a melt comprising CsX, PbX 2 , where X is Br or Cl, and a doping species comprising CsSnBr 3 ; and

growing crystalline doped CsPbX 3 from the melt via vertical Bridgman growth.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 10, 2023
From: KANATZIDIS, MERCOURI G.; HE, YIHUI
To: NORTHWESTERN UNIVERSITY
Reel/Frame 065168/0941 →
Continuity (4)
Continuation 17523141 · Nov 10, 2021
Continuation 16644404
Provisional Application 62555248 · Sep 7, 2017
Related Publication 20230378388A1 · Nov 23, 2023
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