IP Library › Granted Patent US 12,748,357
Granted Patent B2
US 12,748,357 · App. 18/350,309 · Granted Sep 29, 2026

Toner

Inventors: Naoya Isono (Shizuoka, JP); Kenji Ookubo (Shizuoka, JP); Masaya Komuro (Shizuoka, JP)
Assignee: CANON KABUSHIKI KAISHA
G03G9/0825G03G9/08711G03G9/08773
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Quick Facts
Patent No.
US 12,748,357
App. No.
18/350,309
Granted
Sep 29, 2026
Kind
B2
Abstract

A toner comprising a toner particle comprising: a toner base particle comprising a binder resin; and an organosilicon polymer at a surface of the toner base particle, wherein protruded portions constituted from the organosilicon polymer are present at the surface of the toner base particle, when a protruded portion having a height of 30 to 200 nm among the protruded portions is defined as a protrusion x, and the protrusion x is observed in a specific condition using a scanning electron microscope, an average aspect ratio of the protrusion x is 1.3 or more, and when shape measurements of a specific region of the surface of the toner particle are carried out using an atomic force microscope and measured data obtained by observing the protruded portions at the surface of the toner particle is subjected to surface roughness analysis, an average angle of inclination Δa is 1.0 to 2.0°.

Claims (16)

1 . A toner, comprising:

a toner particle comprising a toner base particle;

the toner base particle comprising a binder resin;

the toner base particle having an organosilicon polymer at a surface thereof; and

protruded portions constituted by the organosilicon polymer being present at the surface of the toner base particle, wherein

an average aspect ratio of protrusion x is 1.3 or more when protrusion x is a protruded portion having a height of 30 to 200 nm among the protruded portions and is observed in a normal direction from the surface of the toner particle using a scanning electron microscope, and

an average angle of inclination Δa is 1.0 to 2.0° when shape measurements of a region measuring 1 μm 2 at the surface of the toner particle are carried out using an atomic force microscope and measured data obtained by observing the protruded portions at the surface of the toner particle is subjected to surface roughness analysis.

2 . The toner according to claim 1 , wherein a density Spd of protruded portions having peak heights of at least ¾ of Sp is 17 to 93 protruded portions/μm 2 when Sp (nm) is a maximum peak height of the protruded portions in the surface roughness analysis.

3 . The toner according to claim 2 , wherein Spd is 25 to 65 protruded portions/μm 2 .

4 . The toner according to claim 1 , wherein the toner base particle comprises an organosilicon compound segment, and

the normalized intensity of silicon ions (m/z=28) is 0.0008 to 0.0800 obtained by measuring the toner base particle using time of flight secondary ion mass spectrometry.

5 . The toner according to claim 1 , wherein (Sc/S) is 0.40 to 0.70 when S is a total area of the surface of the toner particle and Sc is an area of those regions of the surface of the toner particle where the surface of the toner base particle is coated with the organosilicon polymer.

6 . The toner according to claim 1 , wherein the binder resin comprises a styrene acrylic resin having a monomer unit represented by Formula (1):

where R 1 denotes a hydrogen atom or a methyl group, and m denotes an integer of 10 to 22.

7 . The toner according to claim 1 , wherein the binder resin comprises a structure represented by Formula (3)

where L 2 denotes —COO(CH 2 ) n —, n denotes an integer of 1 to 10, a carbonyl group in L 2 bonds to a carbon atom having R 2 in the main chain, and R 2 denotes a hydrogen atom or a methyl group.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 21, 2023
From: ISONO, NAOYA; OOKUBO, KENJI; KOMURO, MASAYA
To: CANON KABUSHIKI KAISHA
Reel/Frame 064334/0038 →
Priority Claims (1)
JP 2022-113902 · Jul 15, 2022 · national
Continuity (1)
Related Publication 20240019792A1 · Jan 18, 2024
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