IP Library › Granted Patent US 12,214,420
Granted Patent B2
US 12,214,420 · App. 18/061,250 · Granted Feb 4, 2025

Spheroidal titanium metallic powders with custom microstructures

Inventors: Kamal Hadidi (Somerville, MA); Gregory M. Wrobel (North Andover, MA); Makhlouf Redjdal (Melrose, MA)
Assignee: 6K Inc.
B22F1/00B22F1/065B22F1/142B22F9/08B22F9/14B22F9/30H01J37/32192H05H1/26H05H1/30H05H1/42B22F2207/11B22F2998/10B22F2999/00
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Quick Facts
Patent No.
US 12,214,420
App. No.
18/061,250
Granted
Feb 4, 2025
Kind
B2
Abstract

Methodologies, systems, and devices are provided for producing metal spheroidal powder products. By utilizing a microwave plasma, control over spheriodization and resulting microstructure can be tailored to meet desired demands.

Claims (25)

1. A method of modifying a particle shape and a microstructure of a feedstock, the method comprising:

melting at least a surface portion of particles of feedstock comprising titanium in a plasma to spheroidize the particles; and

setting and applying cooling processing parameters to create spheroidized particles with a microstructure,

wherein the cooling process parameters comprise one or more of a cooling gas flow rate, a residence time of the feedstock, and a cooling gas composition, and

wherein the cooling processing parameters are selected to create at least two regions in the spheroidized particles, each region having a different microstructure or crystal structure, wherein the cooling processing parameters are selected to create an equiaxed microstructure in the spheroidized particles.

2. The method of claim 1 , wherein the particles of the feedstock have a particle size of no less than 1.0 micrometers and no more than 300 micrometers.

3. The method of claim 1 , wherein setting and applying the cooling processing parameters comprises controlling a cooling gas flow rate.

4. The method of claim 1 , wherein setting and applying the selected cooling processing parameters comprises controlling a cooling gas composition.

5. The method of claim 1 , wherein the at least two regions include a core portion and a skin portion.

6. The method of claim 5 , wherein the skin portion has a microstructure that is different from the microstructure of the feedstock.

7. A method of modifying a particle shape and a microstructure of a feedstock, the method comprising:

melting at least a surface portion of particles of the feedstock comprising titanium in a plasma to spheroidize the particles; and

setting and applying cooling processing parameters to create spheroidized particles with a microstructure,

wherein the cooling process parameters comprise one or more of a cooling gas flow rate, a residence time of the feedstock, and a cooling gas composition, and

wherein the cooling processing parameters are selected to create a martensitic microstructure, a Widmanstätten microstructure, and/or an equiaxed microstructure in the spheroidized particles.

8. The method of claim 7 , wherein the particles of the feedstock have a particle size of no less than 1.0 micrometers and no more than 300 micrometers.

9. The method of claim 7 , wherein setting and applying the selected cooling processing parameters comprises controlling a cooling gas flow rate.

10. The method of claim 7 , wherein setting and applying the selected cooling processing parameters comprises controlling a cooling gas composition.

11. The method of claim 7 , wherein the cooling processing parameters are selected to create a martensitic microstructure in the spheroidized particles.

12. The method of claim 7 , wherein the cooling processing parameters are selected to create a Widmanstätten microstructure in the spheroidized particles.

13. The method of claim 7 , wherein the cooling processing parameters are selected to create an equiaxed microstructure in the spheroidized particles.

14. The method of claim 7 , wherein the cooling processing parameters are selected to create at least two regions in the spheroidized particles.

15. The method of claim 14 , wherein each region has a different microstructure or crystal structure.

16. The method of claim 14 , wherein the at least two regions include a core portion and a skin portion.

17. The method of claim 16 , wherein the skin portion has a microstructure that is different from the microstructure of the feedstock.

Assignments (2)
CHANGE OF NAME Recorded Oct 4, 2024
From: AMASTAN TECHNOLOGIES INC.
To: 6K INC.
Reel/Frame 069119/0516 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2024
From: HADIDI, KAMAL; WROBEL, GREGORY; REDJDAL, MAKHLOUF
To: AMASTAN TECHNOLOGIES INC.
Reel/Frame 068800/0062 →
Continuity (5)
Continuation 17301880 · Apr 16, 2021
Continuation 16012370 · Jun 19, 2018
Continuation In Part 15381336 · Dec 16, 2016
Provisional Application 62268186 · Dec 16, 2015
Related Publication 20230211407A1 · Jul 6, 2023
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